Fluitec Mixer2018
Fluitec Mixer2018
Fluitec Mixer2018
It was back in 1993 when Fluitec launched its first static mixers in the
market.Today, Fluitec is a reliable partner for high quality products
whose know-how spans a wide range of mixing, heat transfer
and reaction tasks in the chemical, petrochemical, pharmaceutical,
environment and food industries.
View of the production shop – apparatus weighing up to 3.5 tons is The Fluitec management:
manufactured in-house Daniel Altenburger (Managing Director), Silvano Andreoli (Manager
Production), Alain Georg (Manager R&D), Tobias Vögeli (Manager Sales)
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www.fluitec.ch Contents
Dosing technology
Page 17
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Fluitec static mixers www.fluitec.ch
Static mixers are apparatus with fixed internal elements Mixing with static mixers
that mix the product flowing through them with the help
of kinetic energy only. Since maintenance and wear are There are basically two possible types of flow: turbulent
negligible, only a comparatively small space is required and laminar. In turbulent flow (Re > 2400), the fluid parti-
for installation and the apparatus is suited for a wide vis- cles move randomly in all directions. In laminar flow (Re
cosity range, static mixers are today a popular alterna- < 20), the fluid particles move in layers along straight,
tive for continuous and batch processes. parallel paths. The Reynolds number is a dimensionless
quantity that is defined as the ratio of inertial to viscous
Fluitec mixers are ideal for the following applications forces. It is the decisive parameter for the flow regime.
The Reynolds number can be represented as follows re-
ferred to the diameter D or the hydraulic diameter dh:
• Mixing of pumpable liquids
• Dispersion and emulsification of components Equation 1
which are insoluble in each other
• Mixing of reactive liquids
Determination of homogeneity
• Mixing and homogenising of polymer melts
The mixing efficiency of static mixers in laminar flow al-
• Contacting of gas and liquid
ways used to be analysed by forcing epoxy resins dyed
• Mixing of gases in various colours, which had been premixed with hard-
ener, into the mixing section and subsequently curing
• Heat transfer of viscous fluids
them. The hardened strand was cut into slices in order
• Laminar, uniform flow through to investigate what goes on inside the mixer. These slic-
tubes, e.g. residence time reactors es revealed a cross-section of the mixture. It could be
seen that the number of layers increases rapidly with the
The most diverse geometries are employed to achieve length of the mixer; the layer thickness simultaneously
a homogeneous mixture, depending on the application decreases while the homogeneity increases. Today, the
and the flow regime.The choice of mixer geometry is de- efficiency of a mixer geometry can be assessed very ac-
termined by the Reynolds number and the properties of curately with the help of CFD simulations. Real experi-
the fluids to be mixed. ments with epoxy resin are usually only carried out in or-
der to verify the simulation results.
The mixing processes which take place in Fluitec mixers
are defined, reproducible and optimised.Their high pro- The success of a mixing process can be quantified if a
ductivity and low energy consumption have a positive measure exists for the state of the mixture and this refer-
impact on both the capital investment and the operat- ence state can be derived from locally determined quan-
ing costs. Industrial plants can be reliably designed on tities (e.g. temperature, concentration, electrical con-
the basis of longstanding experience and the results of ductivity, laser induced fluorescence (LIF), photometric
pilot trials. The scale-up risk is reduced to a minimum in analysis (FIP), a CFD calculation, etc. If this data is avail-
this way. able for the cross-sectional area of flow, the mixture can
be evaluated according to statistical criteria. The meas-
ured values and measuring errors generally conform to
a Gaussian (normal) distribution.
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www.fluitec.ch Fluitec static mixers
Equation 4
Standard deviation
The standard deviation is a useful benchmark for the -0.5% +0.5% 0.0025
symmetrical distribution of measured values about the
weighted average and is usually formed from the square
root of the variance. -1% +1% 0.005
The maximum allowable deviation of individual mixture A mixture is normally described as homogeneous if the
samples, referred to the mean concentration, is repre- coefficient of variation COV is between 1 and 5% ( = 0.01
sented as follows: to 0.05).
Equation 3
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Fluitec static mixers www.fluitec.ch
Pressure drop In the laminar flow regime the Newton number is in-
versely proportional to the Reynolds number, i.e. NeRe
The pressure drop must be overcome by means of con- = constant.The following equation is thus used to calcu-
veying devices such as pumps, extruders or blowers. late the pressure drop with laminar flow
With Newtonian fluids, it can be described using the fol-
lowing equation for all flow regimes: Equation 6
Equation 5
1.0E+06
1.0E+05
CSE-X/8
1.0E+04 CSE-XC/6
Aquamix
Newton Number Ne
VORTIX
1.0E+03 New CSE-B
1.0E+02
1.0E+01
1.0E+00
Reynolds Number Re
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www.fluitec.ch Static mixers for laminar flow
The mixing quality of a soluble mixing process is largely Development of the new CSE-XC/6
dependent on the volume flow and viscosity ratios. It can
also be influenced by diffusion, the shear rate, the resi- Over a period of many years, various attempts were
dence time and the Froude number. made to improve the mixing intensity of the CSE-X mix-
er. The engineers at Fluitec considered the mixing pro-
X mixers have emerged during the last few years as by cesses in the static mixer from a different angle for this
far the most powerful and most popular of all known ba- purpose. The question they asked themselves was «Is
sic geometries, namely CSE-W, CSE and CSE-X. Thanks layer growth in the CSE-X mixer determined by the num-
to laser welding technology, Fluitec can meanwhile build ber of bars or is it the open ducts between the bars that
the CSE-X with any desired diameter – from very small to are responsible?»
very large – and using a wide range of materials.
If the open ducts are the culprit when it comes to lay-
Fluitec is continuing to develop and optimise the above er growth, they concluded, one remedy might be to re-
mixer geometries. The new «CSE-XC/6» mixer, which duce the number of bars from 8 to 6 and at the same time
combines a small pressure drop with high mixing effi- open the wall area of the mixer tube.The mixing element
ciency, the «mikromakro®» mixer technology and the would thus have the same number of ducts (openings)
«CSE-X-DS high performance mixer» are just a few re- but would be easier to manufacture and the mixing effi-
cent examples. From mixing and gasification through ciency ought to remain constant.
emulsification and homogenisation to mixing processes
Fluitec uses various types of mixer inspired by the basic geometry of the CSE-X
The new CSE-XC/6 is a The CSE-X/8 was the mikromakro® mixing The CSE-X-DS high per-
more advanced version number one universal could be described as formance mixer is an X
of the CSE-X/8. It reduces mixer for many years. In the targeted use of static mixer with additional
the pressure drop by up the meantime, it has been mixers with different ge- bars.These improve the
to 50% without compro- largely superseded by the ometries and diameters. mixing efficiency, resi-
mising mixing efficien- new CSE-X/6 owing to The macro mixer nor- dence time distribution
cy and can also mix high its relatively high energy mally serves to achieve and variable concentra-
or low-viscosity fluids consumption. However, good pre-distribution of tion range, though at the
without any problems. its geometry sometimes the product prior to fine expense of higher en-
This new mixer model has advantages and it distribution in the micro ergy consumption.This
has a narrower residence therefore remains the mixer. mixer type is therefore
time distribution than the system of choice in cer- only used to meet special
CSE-X/8. tain applications. requirements.
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Static mixers for laminar flow www.fluitec.ch
0.10
0.01
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20
relative mixer length (L/D)
Mixing of two epoxy resins in the new CSE-X (top) and CFD calculation
(bottom). The cut views along the mixing section show the rapid growth
of the layers.
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www.fluitec.ch Laminar mixing applications
Installation types
Mixer bars can be provided for various installation types.
Inserted
di
di
Sleeve design
di
di
di
Supporting ring
di
di
di
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Laminar mixing applications www.fluitec.ch
0.6
Laminar flow tube
• Viscosity ratios from 1 to 1’000‘000 and
H(θ)
0.5 Ideal flow tube (plug flow)
concentrations of up to 50%
CSE-X mixer / Bodenstein number = 120
0.4
0.0
0 0.5 1 1.5 2 2.5 3 3.5 4
θ = t/τ
Equation 8
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www.fluitec.ch Laminar mixing applications
1.0E+03
1.0E+01
1.0E+00
1.0E-01
1.0E-02
1.0E-07 1.0E-06 1.0E-05 1.0E-04 1.0E-03 1.0E-02 1.0E-01 1.0E+00 1.0E+01 1.0E+02
Critical capillary number Cacrit Sample of a glucose dispersion with 5% additive (viscosity ratio =5x
10-4)
The graph shows the influence of the viscosity ratio on • Incorporation and emulsification of insoluble
the critical capillary number Ca for droplet break-up in additives prior to pelletising (mineral oil,
simple shear flow (a = 0) as well as in planar elongation- lubricants, etc.)
al flow (a = 1).
• Dispersion of gas or liquids upstream of
a spray dryer
The flow parameter a, which describes the elongational
component of the total deformation rate, can be repre- • Washing unwanted aromas or additives out of viscous
sented as follows. liquids
• Dispersion and cooling for reactive
Equation 9
mass transfer processes
It is clear from the measured values that CSE-X static • Incorporation and emulsification of blowing and nu-
mixers have a high elongational component. A corre- cleating agents for foams (e.g. pentane, air, nitrogen,
spondingly lower energy consumption is thus neces- etc.)
sary to achieve the droplet size dT. Static mixers have an
• Establishment of uniform cell structures in foams (re-
a value from 0.2 to 0.7 depending on the mixer geometry.
dispersion and homogenisation)
Droplet break-up time tz • Manufacture of mousses
With static mixers, the droplet break-up time in disper-
• Manufacture of creams
sion processes depends mainly on the nature of the
break up.The break-up time tz is influenced by the viscos- • Dispersion during extraction processes
ity ratio and the dosing technology. A large initial drop-
let size can have negative impacts on the droplet spec-
trum, especially in conjunction with a high viscosity ratio
, leading to a longer droplet break-up time and / or a
longer mixer. Special dosing modules with a flow meas-
urement function, a pump and a special injection nozzle
have been developed for CSE-X mixers for this reason.
Typical applications
Within the practical limits, static mixers for dispersion
and emulsification are suited for the following applica-
tions
• Mixing of partially soluble liquids (miscibility gap)
• Contacting and heating of polymer prior to
flash evaporation (water, nitrogen, etc.)
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Laminar mixing applications www.fluitec.ch
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www.fluitec.ch Static mixers for turbulent flow
High-tech, energy efficient and affordable The VORTIX and VORTIX-T in-line mixers can be made
from either metal materials or plastic (PP, PE, PVDF or
The Fluitec «Aquamix» and «VORTIX» mixers are now- PVC).
adays standard solutions for use in the turbulent flow
regime.
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Static mixers for turbulent flow www.fluitec.ch
σ
10
X
5 Reynolds-Number > 15‘000
Concentration X 0.01 - 0.05
Sample size 0.033 D
Ratio of viscosity < 10
1
0.5
VORTIX
VORTIX-T
Aquamix
0.1
0.05
0.01
0 1 2 3 4 5 6 7 8 9 10 11 12
L
Relative Length
D
500
Aquamix
VORTIX-T
VORTIX
100
dp (mbar)
50
10
0.5 1 1.5 2 3 4
w (m s-1)
Pressure drop
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www.fluitec.ch Static mixers for turbulent flow
Liquid gasification with unknown here and like kL is itself a function of the mate-
static mixers rial and process-specific parameters. Both parameters
are difficult to quantify in practice, which is why, as the
Mass transfer product, they usually represent the target variable dur-
In liquid gasification processes, the mass transfer is in- ing the mass transfer.
fluenced on the one hand by the system’s coalescence
behaviour and on the other by Henry’s law. Today, it is above all the CSE-X and CSE-V geometries
With static mixers, high gas transfer rates are achieved which are used for dispersion processes and thus for liq-
not only by the concentration gradient, which is normal- uid gasification.
ly fixed, and by intensive contacting of the two phases
but also by the formation of small gas bubbles with a
large specific interfacial area.
Equation 10
Equation 10
gas / liquid
interface
gas liquid
pi c*
Hi p*i
Hi
δG δL c(t)
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Food and pharmaceutical industries www.fluitec.ch
Fluitec mixers made of stainless steel or Hastelloy have The following tube fittings can be used together with Flu-
been used throughout the process industry for many itec mixers:
years. Fluitec specialises in high quality mixing ele-
• Dairy fittings acc. to DIN 11851
ments, which is why we are able to meet even the very
high – and highly individual – quality requirements for • Clamp fittings (Tri-clamp)
static mixers in sterile processes or food industry appli-
• BioConnect couplings (Neumo)
cations without any problems.
• BBS couplings
• Aseptic tube connections (Südmo)
High on hygiene, low on maintenance
• Small flange connections acc. to DIN 11850
Fluitec CSE-W, CSE-X and Aquamix mixers destined for
• Other fittings on request
the food and pharmaceutical industries can be manu-
factured with electropolished surfaces and the required
tube fittings, so that they are suitable for use in sterile en- Increased quality requirements
vironments. However, the requirements relating to the
quality of the mixer tend to vary from one application to After selecting the type of connection, the next step is to
another and are influenced by factors like process safe- define the welding method and the surface treatment. A
ty, quality assurance, GMP, CIP / SIP, economic efficien- great many requirements have to be satisfied here. How-
cy, etc. ever, the overarching regulation is the Pressure Equip-
ment Directive (PED) 2014/68/EU.
Since both CSE-W and CSE-X mixers provide excellent
self-cleanability, absolute sterility with no dead spots is The housings can be either orbitally or manually weld-
guaranteed provided the apparatus can be emptied and ed.Thanks to our in-house laser welding line, we are in a
the welds are expertly made. position to weld mixing elements with a diameter of just
4.6 mm.
CSE-X/4 for sterile applications CSE-W mixer (DN10) with electropolished surfaces, a Tri-clamp fitting and
a ferrite content of < 0.5% in the welds
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www.fluitec.ch Dosing technology
Injection nozzle
Polymer melt
Transient calculation of an injection nozzle Injection nozzle for polymer mixers with mechanical protection against
polymer plugging
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Fluitec mixing + reaction solutions AG, 8413 Neftenbach Formular 11-90001; Rev. 1
Process Data:
Unit: Main stream Side stream 1 Side stream 2 Side stream 3
Name fluid: [-]
Flow minimal: [m3 h-1]
Flow normal: [m3 h-1]
Flow maximal: [m3 h-1]
Density: [kg m-3]
Viscosity: [mPas]
Temperature: [°C]
Are the fluids mixable? Yes No è Surface tension: mN m-1 Maximal droplet size: mm
Connections: Flange EN1092 Flange ANSI Thread connection Free tube end
Heating jacket: No Yes è Max. allowed pressure: bar Max. allowed temperature: °C
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www.fluitec.ch Other Fluitec products
Systems www.fluitec.ch
DeNOx systems, mixing and dosing systems Further information on our website
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Switzerland
Fluitec
mixing + reaction solutions AG
Seuzachstrasse 40
CH – 8413 Neftenbach
Switzerland
T + 41 52 305 00 40
F + 41 52 305 00 44
Germany
Fluitec
mixing + reaction solutions AG
Engineering Office Germany
Neue Roßstrasse 17
DE – 10179 Berlin
T + 49-3092-109 670
F + 49-3092-103 505
info@fluitec.ch
www.fluitec.ch
2018