Drew Marine
COOLING WATER TREATMENT-1 TESTING, CONTROL AND DOSAGE CHART DREWSM
Technical
CWT TITRET TEST METHOD Service
For use with LIQUIDEWTTM cooling water treatment, MAXIGARD® diesel engine water treatment and DEWT® NC diesel engine water treatment
Apparatus: CWT Titrets Test Set Order No. 0367-01-2
PROCEDURE WITHOUT USING THE TITRETTOR2
2
PROCEDURE FOR USING THE TITRETTOR
Valve
1. Slide the open end of the valve assembly over 1. Fill the sample cup to the 25ml mark with your Assembly Snap the
the tapered tip of the Titret so that it fits snugly. sample. tip at the
(Figure 1). 2. Push the valve assembly (in ampoule tray) onto score mark
2. Snap the tip of the Titret by hand (Figure 2). the Titret ampoule tip until it fits snugly (Figure 1).
3. With the tip of the sample pipe immersed in the 3. Gently snap the tip of the ampoule at the score
Score
sample, squeeze the bead valve briefly to pull mark (Figure 2). Mark
in a small amount of sample. CAUTION: Do 4. Lift the control bar and insert the Titret assem- Reference
not squeeze the bead valve unless the sample bly into the body of the Titrettor (Figure 3). Line
pipe is immersed below the surface of the 5. With the tip of the sample pipe immersed in the Ampoule 1 2
liquid or the vacuum will be lost and the test sample, press the control bar firmly, but briefly,
ruined. (Figure 3). to pull in a small amount of sample (Figure 4). Lift control bar
4. Rock the Titret to mix the contents. The first CAUTION: If the control bar is pressed when
addition of sample will pull in the reagent from the sample pipe is not immersed in the liquid,
the sample pipe. The contents of the ampoule then the vacuum in the Titret will be destroyed.
6. Press the control bar again briefly to allow
will turn a GREEN color. another small amount of sample to be drawn 3
5. Continue to add sample water until the liquid into the ampoule.
in the Titret turns from GREEN to a bright 7. After each addition, rock the entire assembly to
ORANGE.* When the orange color appears, mix the contents of the ampoule. Watch for the
the end point has been reached. Stop test, color change from green to orange (end point). Watch for Read
hold the Titret with its tip pointed upward and 8. Repeat steps 6 and 7 until the end point is color change scale units
read the scale opposite the liquid level. Check reached. here. when color
the control and dosage chart for the appropri- 9. Remove the ampoule from the Titrettor. Hold Press changes
control bar permanently.
ate product concentrations. (Figure 5) the Titret ampoule in a vertical position and
carefully read the test result on the scale oppo- Sample pipe
*Note: Immediately before the end point is 4
reached, the contents will turn BLUE. Make site the liquid level (Figure 5). 5
Sample
further additions with care.
TEST RESULTS & DOSAGE REQUIREMENTS (Control Limits in Bold Italics)
CONVERSION CHART CONVERSION CHART CONVERSION CHART
MAXIGARD® diesel engine water treatment LIQUIDEWTTM cooling water treatment DEWT® NC diesel engine water treatment
SCALE MAXIGARD DOSAGE SCALE LIQUIDEWT DOSAGE SCALE DEWT NC DOSAGE
UNITS as ppm prod in liters/ton UNITS as ppm prod in liters/ton UNITS as ppm prod in kgs/ton
Initial Dosage: 16.0 liters/ton Initial Dosage: 8.0 liters/ton Initial Dosage: 3.2 kgs/ton
1.0 12,000* 6.0 1.0 8,000* 1.5 1.0 800 2.7
1.1 13,000 6.0 1.1 9,000 1.5 1.1 900 2.7
1.2 14,000 6.0 1.2 10,000 Satisfactory - no dosage 1.2 1,000 2.3
1.3 16,000 6.0 1.3 11,000 Satisfactory - no dosage 1.3 1,100 2.3
1.4 17,000 4.0 1.4 12,000 Satisfactory - no dosage 1.4 1,200 2.3
1.5 18,000 4.0 1.5 13,000 Satisfactory - no dosage 1.5 1,300 2.3
1.6 19,000 Satisfactory - no dosage 1.6 14,000 Satisfactory - no dosage 1.6 1,400 2.3
1.8 22,000 Satisfactory - no dosage 1.8 15,000 Satisfactory - no dosage 1.8 1,500 1.8
2.0 24,000 Satisfactory - no dosage 2.0 17,000 High 2.0 1,700 1.8
2.5 30,000 Satisfactory - no dosage 2.5 22,000 High 2.5 2,200 1.4
3.0 36,000 Satisfactory - no dosage 3.0 26,000 High Partially drain 3.0 2,600 0.9
3.5 42,000 High 3.5 30,000 High and freshen 3.5 3,000 Satisfactory - no dosage
4.0 48,000 High Partially drain 4.0 34,000 High system 4.0 3,400 Satisfactory - no dosage
5.0 60,000 High and freshen 5.0 43,000 High 5.0 4,300 Satisfactory - no dosage
7.0 84,000 High system 7.0 60,000 High 7.0 6,000 High
10.0 120,000 High 10.0 86,000 High 10.0 8,600 High
High quality distilled makeup water is recommended. High quality distilled makeup water is recommended. High quality distilled makeup water is mandatory.
*If readings are below 12,000 (scale unit 1.0), use 10.0 ltr/ton and retest. *If readings are below 8,000 (scale unit 1.0), use 5.0 ltr/ton and retest.
If system has been partially drained and refilled, use initial dosage. If system has been partially drained and refilled, use initial dosage.
CW-CS-1 (1/03)R9
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The use of high quality, distilled makeup water is recommended as the best means
CHLORIDE SAMPLE PRETREATMENT
of controlling scale formation for LIQUIDEWTTM and MAXIGARD®-treated systems
Use for cooling water treated with MAXIGARD or LIQUIDEWT treatments.
and is mandatory for DEWT NC-treated systems.
Apparatus and Reagents
Drew Chloride LMP Test Kit PCN 0373-01-9
REFERENCE TESTS FOR MAKEUP WATER CONTAMINANTS Sample Pretreatment 50 gm PCN 0374-02-5
(includes 0.5 gm scoop)
Use any one of the following parameters as an indicator of makeup water contamination. Filter Paper, Box of 100 PCN 0225-01-2
Funnel, Plastic PCN 0221-01-0
Parameter Limit Stirring Rod, Plastic, 150mm PCN 0417-01-5
Conductivity 500 µmhos maximum PROCEDURE
Chloride 100 ppm maximum 1. Add one scoop (0.5 gm) of Sample Pretreatment to approximately 70 ml of cooling water and stir well.
Hardness 170 ppm maximum 2. Let stand for two (2) minutes to allow precipitate to settle.
*If any parameter is higher than the maximum, use better quality water. 3. Filter the sample and proceed with the chloride detemrination using the Drew Chloride LMP Test Kit.
ALTERNATE TEST FOR DEWT® NC diesel engine water treatment
Preferred method is to use the CWT Titrets1
Apparatus: DEWT NC Test Kit Order No. 0302-01-8
Test Kit Contains: 1 Cylinder, 50ml Order No. 0236-01-9
1 0.2g spoon Order No. 0224-01-4
1 DEWT NC Reagent No. 1, (100 gms) Order No. 0306-01-0
PROCEDURE 1 DEWT NC Reagent No. 2, (100 gms) Order No. 0307-01-8
1. Draw a cooling water sample from a full flowing part of the system into the graduated mixing cylinder to the
25 ml mark. (Figure 1)
2. Add 5 level measuring spoons of DEWT NC Reagent No. 1 and mix until all of the reagent is dissolved. (Figure 2)
3. Add 1 level measuring spoon of DEWT NC Reagent No. 2, stopper the mixing cylinder, and thoroughly mix. (Figure 3)
4. If the sample turns purple-red and the color lasts for at least 30 seconds, the test indicates that the treatment level
is below 500 ppm. However, if the color disappears within 30 seconds, add additional Reagent No. 2, one level measuring
spoon at a time (counting spoonfuls) with thorough mixing until the purple-red color persists for over 30 seconds.
5. To determine the concentration of DEWT NC, count the total number of measuring spoons of Reagent No. 2 added
and convert to ppm.
Calculation: ppm DEWT NC = (number of spoons-1) x 500
6. Record results as ppm DEWT NC on the Cooling Water Treatment Onboard Graphing Log (CW-LS-3).
7. Determine the dosage of DEWT NC treatment required per tonne of circulating water as indicated on the Dosage Requirement Chart.
DOSAGE REQUIREMENT CHART (Control Limits in Bold Italics)
DEWT NC diesel engine water treatment
Total Number of ppm
Measuring Spoons of of DEWT NC Dosage Requirement per Ton
Reagent No. 2 Used Recorded of Circulating Water
1 None 3.2 kg (7 lbs.)
2 500 2.7 kg (6 lbs.)
3 1000 2.3 kg (5 lbs.)
4 1500 1.8 kg (4 lbs.)
5 2000 1.4 kg (3 lbs.)
6 2500 0.9 kg (2 lbs.)
7 3000 Satisfactory - No dose required.
8 3500 Satisfactory - No dose required.
9 4000 Satisfactory - No dose required.
10 4500 Satisfactory - No dose required. CW-CS-1 (1/03)R9
11 5000 High - No dose required.
©2003 Ashland Inc. ®Registered trademark, TMTrademark of Ashland Inc.
SM
Service Mark of Ashland Inc. 1Registered trademark, 2Trademark of CHEMetrics, Inc. Printed in U.S.A.
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