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Search Results (1,272)

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18 pages, 1911 KiB  
Article
Effect of Pit and Soil Types on Growth and Development, Nutrient Content and Fruit Quality of Pomegranate in the Central Deccan Plateau Region, India
by Rajagopal Vadivel, Kotha Sammi Reddy, Yogeshwar Singh and Dhananjay D. Nangare
Sustainability 2024, 16(18), 8099; https://doi.org/10.3390/su16188099 (registering DOI) - 16 Sep 2024
Viewed by 227
Abstract
To enhance pomegranate production on marginal gravelly lands, standardized planting techniques were evaluated in an 8-year-old orchard. Trenching, wider pit excavation, pit digging, and auger digs with dimensions of 1 and 2 m were employed. Utilizing native soil from barren land, with or [...] Read more.
To enhance pomegranate production on marginal gravelly lands, standardized planting techniques were evaluated in an 8-year-old orchard. Trenching, wider pit excavation, pit digging, and auger digs with dimensions of 1 and 2 m were employed. Utilizing native soil from barren land, with or without spent wash, and mixing it with black soil up to 1 m deep, growth parameters, leaf nutrients, fruit production, and fruit quality were assessed. The trench and wider pit methods outperformed others, yielding greater above-ground biomass (>70.3 kg tree−1), root biomass (>24.5 kg, tree−1), and cross-sectional area (>3.30 m2 tree−1). These methods also produced longer roots (>4.0 m tree−1) and higher leaf phosphorus (>0.28%) and potassium (>1.81%) levels, fruit juice content (>48.50%), and total soluble solids (>16.05°) compared to other planting methods. This resulted in higher and more sustainable fruit yield production under the trench and wider pit planting methods (>7.21 t ha−1). Similarly, the native and black soil mixture produced healthy fruit trees, improved fruit quality, and sustainably higher fruit yield over the native soil alone. In summary, the trench and wider pit methods (2–3 m3), combined with a soil mixture, are recommended for sustainable, high-quality fruit production in shallow gravelly terrains, thereby improving food security and the livelihoods of farmers in arid regions. Full article
(This article belongs to the Section Sustainable Agriculture)
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<p>Study site location in the Central Deccan Plateau region (Baramati, Pune District in Maharashtra sate).</p>
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<p>Innovative planting techniques for sustainable pomegranate cultivation in the shallow skeletal land.</p>
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<p>The interaction effect of planting pits and soil types on root biomass (kg tree<sup>−1</sup>) in shallow and gravelly land (Capital letters indicate differences among pit types, and the small letters indicate differences among soil types).</p>
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<p>The variations of root length distribution at (<b>A</b>) horizontal and (<b>B</b>) vertical distances under different planting pits followed under the shallow and gravelly land situation. (Capital letters indicate differences among the spread distances, and the small letters indicate differences among the pit types).</p>
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<p>The variations of root length distribution at (<b>A</b>) horizontal and (<b>B</b>) vertical distances under different planting pits followed under the shallow and gravelly land situation. (Capital letters indicate differences among the spread distances, and the small letters indicate differences among the pit types).</p>
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<p>Effect of pit size and soil types (NSBS—Native and Black Soil mixture, NS—Native Soil and NSSW—Native Soil Saturated with Spent Wash) on pomegranate yield between 4th and 8th years of plantings. (Capital letters indicate differences among pit types, and the small letters indicate differences among soil types).</p>
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<p>A linear functional relationship between pit volumes (m<sup>3</sup>) and fruit production (t ha<sup>−1</sup>) from 8-year-old pomegranate under the shallow and gravelly barren land situation.</p>
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16 pages, 2107 KiB  
Article
Exploring Italian Autochthonous Punica granatum L. Accessions: Pomological, Physicochemical, and Aromatic Investigations
by Deborah Beghè, Martina Cirlini, Elisa Beneventi, Chiara Dall’Asta, Ilaria Marchioni and Raffaella Petruccelli
Plants 2024, 13(18), 2558; https://doi.org/10.3390/plants13182558 - 12 Sep 2024
Viewed by 261
Abstract
Autochthonous Italian pomegranate accessions are still underexplored, although they could be an important resource for fresh consumption, processing, and nutraceutical uses. Therefore, it is necessary to characterize the local germplasm to identify genotypes with desirable traits. In this study, six old Italian pomegranate [...] Read more.
Autochthonous Italian pomegranate accessions are still underexplored, although they could be an important resource for fresh consumption, processing, and nutraceutical uses. Therefore, it is necessary to characterize the local germplasm to identify genotypes with desirable traits. In this study, six old Italian pomegranate landraces and a commercial cultivar (Dente di Cavallo) were investigated, evaluating their fruit pomological parameters, physicochemical (TSS, pH, TA, and color) characteristics, sugar content, and aromatic profiles (HeadSpace Solid-Phase MicroExtraction (HS-SPME)) coupled with Gas Chromatographyass Spectrometry (GC–MS) of pomegranate juices. Significant differences were observed in the size and weight of the seed and fruits (127.50–525.1 g), as well as the sugar content (100–133.6 gL−1), the sweetness (12.9–17.6 °Brix), and the aroma profiles. Over 56 volatile compounds, predominantly alcohols (56%), aldehydes (24%), and terpenes (9%), were simultaneously quantified. Large variability among the genotypes was also statistically confirmed. The results indicate a strong potential for commercial exploitation of this germplasm, both as fresh and processed fruit, and highlight its versatility for diverse applications. The genetic diversity of the autochthonous pomegranate accessions represents a precious heritage to be preserved and enhanced. This work represents a preliminary step toward a more comprehensive characterization and qualitative valorization of the Italian pomegranate germplasm. Full article
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<p>The percentage compositions of the volatile chemical groups found in the total juice pomegranate obtained by all the accessions together (<b>A</b>) and in the juice of separate accessions (<b>B</b>). For interpretation of the references to color in this figure legend, the reader is referred to the web version of this article.</p>
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<p>The amounts (μg/mL) of the volatile chemical groups found in the juice of each pomegranate accession. The different letters above each column indicate significant differences among the samples (Tukey’s test <span class="html-italic">p</span> ≤ 0.05). For interpretation of the references to color in this figure legend, the reader is referred to the web version of this article.</p>
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<p>(<b>A</b>–<b>C</b>) The loading plots of the first, second, and third principal components showing the positions of the pomegranate accessions and the different parameters studied.</p>
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25 pages, 7108 KiB  
Article
Coupling Low-Frequency Ultrasound to a Crossflow Microfiltration Pilot: Effect of Ultrasonic Pulse Application on Sono-Microfiltration of Jackfruit Juice
by Herenia Adilene Miramontes-Escobar, Nicolas Hengl, Manuel Dornier, Efigenia Montalvo-González, Martina Alejandra Chacón-López, Nawel Achir, Fabrice Vaillant and Rosa Isela Ortiz-Basurto
Membranes 2024, 14(9), 192; https://doi.org/10.3390/membranes14090192 - 11 Sep 2024
Viewed by 295
Abstract
To reduce membrane fouling during the processing of highly pulpy fruit juices into clarified beverages, a crossflow Sono-Microfiltration (SMF) system was employed, strategically equipped with an ultrasonic probe for the direct application of low-frequency ultrasound (LFUS) to the juice just before the entrance [...] Read more.
To reduce membrane fouling during the processing of highly pulpy fruit juices into clarified beverages, a crossflow Sono-Microfiltration (SMF) system was employed, strategically equipped with an ultrasonic probe for the direct application of low-frequency ultrasound (LFUS) to the juice just before the entrance to the ceramic membrane. Operating conditions were standardized, and the application of LFUS pulses in both corrective and preventive modes was investigated. The effect of SMF on the physicochemical properties and the total soluble phenol (TSP) content of the clarified juice was also evaluated. The distance of ultrasonic energy irradiation guided the selection of the LFUS probe. Amplitude conditions and ultrasonic pulses were more effective in the preventive mode and did not cause membrane damage, reducing the operation time of jackfruit juice by up to 50% and increasing permeability by up to 81%. The SMF did not alter the physicochemical parameters of the clarified juice, and the measured LFUS energy ranges did not affect the TSP concentration during the process. This study is the first to apply LFUS directly to the feed stream in a pilot-scale crossflow microfiltration system to reduce the fouling of ceramic membranes and maintain bioactive compounds in jackfruit juice. Full article
(This article belongs to the Special Issue Membrane Technologies in Food Industry and Bioprocessing)
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<p>Options for using the pumping system that allow different operating modes to be applied in the Sono-Microfiltration pilot. The solid line indicates the use of the SMF pilot with a centrifugal pump; the dashed line indicates the use of the SMF pilot with a positive displacement pump; the solid and dotted lines indicate the use of both pumps. (1) Recirculating bath; (2) Feed tank (30 L); (3) Positive displacement pump; (4) Centrifugal pump; (5) Flowmeter; (6) Ultrasound probe; (7) Filtration membrane housing; (8) Permeate flow outlet; (9) Tubular heat exchanger.</p>
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<p>Thermal imaging of ultrasonic energy irradiation from two probes at different amplitudes of low-frequency ultrasound (LFUS) (without membrane filtration, U = 6 m·s<sup>−1</sup>).</p>
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<p>Thermal imaging of ultrasonic energy irradiation from two probes at different amplitudes of low-frequency ultrasound (LFUS) (without membrane filtration, U = 6 m·s<sup>−1</sup>).</p>
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<p>Effect of LFUS application in corrective mode during the processing of jackfruit juice. Pulp/water ratio of 1:1 at VRR = 1 (ultrasonic diameter probe 2.54 cm, membrane Tami, dpore = 0.2 μm, TMP = 2.7 bar, T<sub>feed</sub> = 30 °C, and U = 6 m·s<sup>−1</sup>). ON: application of LFUS, OFF: without LFUS, A: LFUS amplitude, MF: Microfiltration.</p>
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<p>Multichannel ceramic membrane (0.2 μm) with damage caused by applying a 50% LFUS amplitude, an ultrasonic intensity of 21.2–31.2 W·cm<sup>2</sup>, and 104–153 W power.</p>
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<p>Effect of LFUS application on (<b>A</b>) the volumetric reduction ratio (VRR) during the SMF process of jackfruit juicing on process time and (<b>B</b>) total membrane resistance to the VRR (ultrasonic diameter probe 2.54 cm, membrane Tami, dpore = 0.2 μm, TMP = 2.7 bar, T<sub>feed</sub> = 30 °C, and U = 6 m·s<sup>−1</sup>). ON: LFUS application; OFF: without LFUS application; A: LFUS amplitude.</p>
Full article ">Figure 5 Cont.
<p>Effect of LFUS application on (<b>A</b>) the volumetric reduction ratio (VRR) during the SMF process of jackfruit juicing on process time and (<b>B</b>) total membrane resistance to the VRR (ultrasonic diameter probe 2.54 cm, membrane Tami, dpore = 0.2 μm, TMP = 2.7 bar, T<sub>feed</sub> = 30 °C, and U = 6 m·s<sup>−1</sup>). ON: LFUS application; OFF: without LFUS application; A: LFUS amplitude.</p>
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<p>Effect of low-frequency ultrasound application on the decrease in membrane permeability during Sono-Microfiltration processes of clarified jackfruit juice at VRR = 1.85 (ultrasonic diameter probe 2.54 cm, membrane Tami, dpore = 0.2 μm, TMP = 2.7 bar, T<sub>feed</sub> = 30 °C, and U = 6 m·s<sup>−1</sup>). ON: LFUS application; OFF: no LFUS application; A: LFUS amplitude.</p>
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<p>Contour plots of 2<sup>3−1</sup> fractional factorial design in SMF pilot in jackfruit juice 1:2. (<b>A</b>) Pulse OFF vs. Pulse ON, (<b>B</b>) amplitude vs. pulse ON, (<b>C</b>) amplitude vs. pulse OFF.</p>
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<p>Contour plots of 2<sup>3−1</sup> fractional factorial design in SMF pilot in jackfruit juice 1:2. (<b>A</b>) Pulse OFF vs. Pulse ON, (<b>B</b>) amplitude vs. pulse ON, (<b>C</b>) amplitude vs. pulse OFF.</p>
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<p>Effect of Sono-Microfiltration (SMF) on the turbidity of (<b>A</b>) clarified jackfruit juice (CJJ) and (<b>B</b>) retained jackfruit juice (RJJ). Different letters show statistically significant differences.</p>
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<p>Effect of Sono-Microfiltration (SMF) on (<b>A</b>) total soluble solids (TSS) and (<b>B</b>) viscosity in jackfruit juice. IJJA: fed initial jackfruit juice, CJJ: clarified jackfruit juice, RJJ: retained jackfruit juice. Different letters show statistically significant differences.</p>
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<p>Effect of Sono-Microfiltration (SMF) on (<b>A</b>) total soluble solids (TSS) and (<b>B</b>) viscosity in jackfruit juice. IJJA: fed initial jackfruit juice, CJJ: clarified jackfruit juice, RJJ: retained jackfruit juice. Different letters show statistically significant differences.</p>
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<p>Total soluble phenols (TSP) in clarified jackfruit juice by Sono-Microfiltration (SMF) compared with the raw juice (IJJF). Different letters show statistically significant differences.</p>
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<p>Design of the Sono-Microfiltration pilot. (1) Recirculating bath; (2) Feed tank (30 L); (3) Positive displacement pump; (4) Centrifugal pump; (5) Flowmeter; (6) Ultrasonic probe; (7) Filtration membrane housing; (8) Permeate flow outlet; (9) Tubular heat exchanger.</p>
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<p>Volumetric reduction ratio (VRR) vs. permeate flux (Jp) during the clarification of jackfruit juice by Sono-Microfiltration.</p>
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20 pages, 2187 KiB  
Article
Sustainable Jam with Apple Pomace: Gelling, Rheology, and Composition Analysis
by Ândria Viegas, Maria João Alegria and Anabela Raymundo
Gels 2024, 10(9), 580; https://doi.org/10.3390/gels10090580 - 8 Sep 2024
Viewed by 391
Abstract
Fruit juice processing can generate significant waste, but efficiently repurposing some of its byproducts not only reduces environmental impact but also adds value, thereby enhancing sustainability in the food industry. This work assesses the use of hydrocolloids in jam preparation and the influence [...] Read more.
Fruit juice processing can generate significant waste, but efficiently repurposing some of its byproducts not only reduces environmental impact but also adds value, thereby enhancing sustainability in the food industry. This work assesses the use of hydrocolloids in jam preparation and the influence of time and temperature on gelation in the presence of apple pomace. The effects of different processing conditions were analyzed using response surface methodology. Viscosity, elastic modulus (G′), viscous modulus (G″), and firmness were measured. Results indicated that both time and temperature significantly improved rheological and textural properties. The optimal conditions (35.6 min and 84.2 °C) yielded a viscosity of 3.66 × 10⁴ ± 4.49 × 102 Pa·s and a G′ at 1 Hz of 2596 ± 128 Pa. The final product exhibited the desirable texture, was free of added sugars, had low lipid content, and retained its bioactive compounds. Applying apple pomace in the formulation allows a more efficient hydrocolloid system, promotes a circular economy, and combats food waste. Full article
(This article belongs to the Special Issue Thixotropic Gels: Mechanisms, Functions and Applications)
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<p>Intermolecular (<b>a</b>) hydrogen bonds and (<b>b</b>) hydrophobic interaction involved in high methoxyl pectin gelation. Adapted from Picot-Allain et al. [<a href="#B6-gels-10-00580" class="html-bibr">6</a>].</p>
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<p>Response surface for the: (<b>a</b>) zero-shear rate-limiting viscosity (ƞ<sub>0</sub>); (<b>b</b>) G′ at 1 Hz; and (<b>c</b>) firmness of apple pomace jams prepared under different processing conditions (time and temperature).</p>
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<p>Evolution of the viscosity curves of apple pomace jams prepared with different: (<b>a</b>) stirring times and (<b>b</b>) processing temperatures.</p>
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<p>Evolution of the storage and loss moduli with frequency for apple pomace jam prepared with different: (<b>a</b>) stirring times and (<b>b</b>) temperatures.</p>
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<p>Firmness of apple pomace jam processing with different: (<b>a</b>) stirring times and (<b>b</b>) temperatures. Samples are presented as mean, with error bars indicating the standard deviations from the repetitions. In the same graph, different letters correspond to significant differences (<span class="html-italic">p</span> &lt; 0.05).</p>
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16 pages, 1891 KiB  
Article
Physicochemical and Functional Characterization of Pear Leathers Enriched with Wild Bilberry and Blackcurrant Pomace Powders
by Ana Maria Blejan, Violeta Nour and Georgiana Gabriela Codină
Agronomy 2024, 14(9), 2048; https://doi.org/10.3390/agronomy14092048 - 7 Sep 2024
Viewed by 312
Abstract
Fruit leathers are convenient, delicious and sophisticated alternatives to natural fruits as a source of nutrients, fibers and bioactive compounds. The present study was conducted to develop new fruit leathers by adding 0.5%, 1.0% and 1.5% wild bilberry (BIPP) and blackcurrant (BCPP) pomace [...] Read more.
Fruit leathers are convenient, delicious and sophisticated alternatives to natural fruits as a source of nutrients, fibers and bioactive compounds. The present study was conducted to develop new fruit leathers by adding 0.5%, 1.0% and 1.5% wild bilberry (BIPP) and blackcurrant (BCPP) pomace powders in pear leather manufactured with honey (5%), pectin (1%) and lemon juice (2.5%) as additional ingredients. The CIEL*a*b* color parameters, titratable acidity, total phenolics content, total anthocyanins content and DPPH radical scavenging activity were determined in the fruit leathers. In addition, the puncturing force, flexibility and adhesiveness of the fruit leathers were measured and sensory analysis was conducted. The results showed that the addition of pomace powders significantly decreased the lightness, chroma and hue angle and increased the titratable acidity of the fruit leathers while a* values decreased in the leathers with BIPP addition. Flexibility slightly decreased while adhesiveness significantly increased with increasing BIPP and BCPP addition level, changes that were perceived as negative in the sensory analysis. The total phenolic content increased by 2.03, 3.26 and 4.45 times at 0.5, 1.0 and 1.5% BIPP addition, respectively, while only by 1.22, 1.42 and 1.60 times at the same levels of BCPP addition. The newly developed fruit leathers could be recommended as alternative snack foods with high nutritional value and functionality. Full article
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<p>Drying curves at 57 °C of the control pear leather and fruit leathers made with addition of (<b>a</b>) bilberry pomace powder; (<b>b</b>) blackcurrant pomace powder.</p>
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<p>The appearance of the fruit leathers.</p>
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<p>Sensory profile of control pear leather and pear leathers enriched with (<b>a</b>) bilberry pomace powder; (<b>b</b>) blackcurrant pomace powder.</p>
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<p>Sensory profile of control pear leather and pear leathers enriched with (<b>a</b>) bilberry pomace powder; (<b>b</b>) blackcurrant pomace powder.</p>
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10 pages, 1560 KiB  
Review
Lingonberry (Vaccinium vitis-idaea L.) Fruit Phenolic Bioactivities—A Review of In Vitro and In Vivo Human Studies
by Pirjo Pärnänen, Sari Niikko, Hanna Lähteenmäki, Ismo T. Räisänen, Taina Tervahartiala, Timo Sorsa and Annamari Ranki
Microorganisms 2024, 12(9), 1850; https://doi.org/10.3390/microorganisms12091850 - 6 Sep 2024
Viewed by 433
Abstract
This review is focused on the effects of lingonberry (Vaccinium vitis-idaea L.) fruit phenolic compounds in human in vitro cells and in vivo clinical studies. Studies with lingonberries, lingonberry juice/lingonberry nectar/fermented lingonberry juice, and phenolic fractions with active molecules are reviewed. Lingonberry’s [...] Read more.
This review is focused on the effects of lingonberry (Vaccinium vitis-idaea L.) fruit phenolic compounds in human in vitro cells and in vivo clinical studies. Studies with lingonberries, lingonberry juice/lingonberry nectar/fermented lingonberry juice, and phenolic fractions with active molecules are reviewed. Lingonberry’s bioactive substances have a diverse range of antimicrobial, anti-inflammatory, antiproteolytic, anticancer, and antioxidant properties. Fermentation of lingonberries and modulation of the dysbiotic microbiome to a more symbiotic composition by favoring the growth of lactobacilli and inhibiting the growth of human opportunistic pathogens are discussed. Research results suggest that more studies on humans are needed. Full article
(This article belongs to the Section Microbial Biotechnology)
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<p>(<b>A</b>) <span class="html-italic">Streptococcus mutans</span> cultivation on MSB plate. Initial sample (left) and growth inhibition after 2 weeks of using fermented lingonberry mouthrinse (10 mL burst two times a day), and final sample 2 weeks after the end of use (right). (<b>B</b>) <span class="html-italic">Candida</span> cultures on SDA plates. Initial sample (left), growth inhibition after 2 weeks of using fermented lingonberry mouthrinse (middle, 10 mL ½ min 2 times a day), and final sample 2 weeks after the end of use (right). (<b>C</b>) Plating of lactobacilli. The initial sample (left) and the increase in growth after 2 weeks of using fermented lingonberry mouthrinse (10 mL ½ min burst 2 times a day), and the final sample 2 weeks after the end of use (right). (<b>D</b>) Growth of anaerobic oral bacteria on Brucella blood agar (initial sample on the left) and inhibition of growth after 2 weeks of lingonberry mouthrinse (10 mL mouthrinse ½ min 2 times a day, right image) [<a href="#B37-microorganisms-12-01850" class="html-bibr">37</a>].</p>
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<p>Cariograms of the participants (<span class="html-italic">n</span> = 25) in the study [<a href="#B41-microorganisms-12-01850" class="html-bibr">41</a>] at 0, 6, and 12 months. The average values of the oral variables have been used in the caries risk analysis of the Cariogram program [<a href="#B42-microorganisms-12-01850" class="html-bibr">42</a>] (the picture is a combination of the results given by the program at 0, 6, and 12 months). The green sector reflects the possibility of avoiding new caries. Dental fluoridation was performed at the reception at 0, 6, and 12 months. The participants were classified into a high-caries-risk group due to their high average age, medications, and illnesses. Their diet or oral self-care was not addressed in the studies.</p>
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12 pages, 757 KiB  
Article
Erosive Tooth Wear and Associated Risk Indicators in Schoolchildren from Rural and Urban Areas of the State of Mexico: A Cross-Sectional Study
by José Cuauhtémoc Jiménez-Núñez, Álvaro Edgar González-Aragón Pineda, Teresa Villanueva-Gutiérrez, Rodrigo Leopoldo Longinos-Huerta, Luis Pablo Cruz-Hervert, Adrian Lussi and Socorro Aída Borges-Yáñez
Children 2024, 11(9), 1090; https://doi.org/10.3390/children11091090 - 6 Sep 2024
Viewed by 369
Abstract
Background and Objective: Limited access to health services and low educational levels are factors in the rural population that are associated with the development of oral pathologies. However, the specific risk indicators contributing to erosive tooth wear (ETW) in these populations remain unclear. [...] Read more.
Background and Objective: Limited access to health services and low educational levels are factors in the rural population that are associated with the development of oral pathologies. However, the specific risk indicators contributing to erosive tooth wear (ETW) in these populations remain unclear. The objective of this study was to identify risk indicators associated with the prevalence of erosive tooth wear (ETW) in schoolchildren aged 8–12 years from rural and urban areas in the State of Mexico. Methods: A cross-sectional study was carried out in public schools in rural and urban areas. The prevalence of ETW was evaluated using the Basic Erosive Wear Examination (BEWE). The risk indicators studied were gastroesophageal reflux, vomiting, vitamin C, food, beverages, dental hygiene, bruxism, and hyposalivation. Logistic regression models were used to calculate odds ratios (OR) and 95% confidence intervals (CI). Results: The prevalence of ETW was higher in the rural area (77.3%) compared to the urban area (51.2%) (p = 0.001). The odds of presenting ETW were more than twice in schoolchildren from rural areas compared to those from urban areas (OR: 2.25, 95% CI: 1.11–3.98). Risk indicators varied between rural and urban populations, with different factors such as the consumption of fresh tomato sauce, orange, tangerine, atole (artisanal corn-based drink), and teeth grinding in the rural area, and lemon, soft drink, fruit juice consumption, and the simplified oral hygiene index in the urban area (p < 0.05). Conclusions: To prevent ETW, strategies offering tailored dietary and hygiene advice should be proposed, considering the specific conditions of each geographic area. Full article
(This article belongs to the Section Pediatric Dentistry & Oral Medicine)
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<p>Data collection process.</p>
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<p>Distribution and severity of erosive dental wear based on schoolchildren’s geographic area in the State of Mexico.</p>
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10 pages, 1481 KiB  
Article
Innovative Technology of Continuous-Steam Distillation with Packed Column to Obtain Essential Oil-Differentiated Fractions from Mexican Lime (Citrus aurantifolia)
by Tania Pahua-Angel, Mirna Estarrón-Espinosa, Eduardo Castaño-Tostado, Edmundo Mateo Mercado-Silva, Silvia Lorena Amaya-Llano and José Daniel Padilla-de la Rosa
ChemEngineering 2024, 8(5), 88; https://doi.org/10.3390/chemengineering8050088 - 2 Sep 2024
Viewed by 334
Abstract
Continuous distillation (CD) by steam is a patented emerging technology that allows us to obtain essential-oil fractions from citrus juices. It presents benefits such as reducing steam consumption by 50%, lowering environmental impact, and, by its design, obtaining fractions enriched in terpenic and [...] Read more.
Continuous distillation (CD) by steam is a patented emerging technology that allows us to obtain essential-oil fractions from citrus juices. It presents benefits such as reducing steam consumption by 50%, lowering environmental impact, and, by its design, obtaining fractions enriched in terpenic and oxygenated compounds that can be further processed. The CD of essential oils from Mexican lime juice (Citrus aurantifolia) was studied and the results were compared with conventional steam distillation (batch) in terms of steam consumption, extraction yield, chemical composition, and quality of the essential oils. Different steam flows were used: distillation without a packed column (sc); with packed column (cc); and steam flows of 10, 15, and 20 mL/min with a reflux ratio of 0.5, 1, and 2, respectively. CD was superior in terms of composition, extraction energy savings (0.63 kg steam/kg juice with 1.39 kg steam/kg juice in the conventional), and the extraction yield recovery efficiency was >90%. Gas chromatography-mass spectrometry analysis of the extracted essential oils indicated that the use of CD with a column increases the fractionation of volatile compounds. The result of this study demonstrates that CD can be used as an alternative method to extract the essential oil from lime or any citrus fruit, obtaining differentiated fractions in aroma and composition. Full article
(This article belongs to the Special Issue Green and Sustainable Separation and Purification Technologies)
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<p>Diagram of the continuous distillation process, taken from Padilla et al., 2021 [<a href="#B11-ChemEngineering-08-00088" class="html-bibr">11</a>].</p>
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<p>Steam expenditure in the continuous-steam distillation by steam entrainment compared to conventional distillation (batch30) for an extraction period of 4 h. Column distillation with a steam flow of 10 mL/min (cc10). Column distillation with a steam flow of 15 mL/min (cc15). Distillation with a column with a steam flow of 20 mL/min (cc20). Distillation without column with a steam flow of 10 mL/min (sc10). Distillation without a column with a steam flow of 20 mL/min (sc20). Distillation without a column with a steam flow of 30 mL/min (sc30). An asterisk in superscript expresses a statistically significant difference in the columns of the medians of the treatments by Dunn’s post hoc test, adjusted by Bonferroni’s method (α = 0.05).</p>
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<p>Extraction yield of the lime essential oil in relation to continuous-steam distillation compared to conventional distillation (batch30) for an extraction period of 4 h. Column distillation with a steam flow of 10 mL/min (cc10). Column distillation with a steam flow of 15 mL/min (cc15). Distillation with a column and a steam flow of 20 mL/min (cc20). Distillation without a column and a steam flow of 10 mL/min (sc10). Distillation without a column and a steam flow of 20 mL/min (sc20). Distillation without a column and a steam flow of 30 mL/min (sc30). An asterisk in superscript expresses statistically significant differences in the columns of the medians of the treatments by Dunn’s post hoc test, adjusted by Bonferroni’s method (α = 0.05).</p>
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<p>Density of the essential oil obtained from Mexican lime juice by continuous steam distillation with a column and without a column. Sc, without column; Cc, with column; F1, Fraction 1; F2, Fraction 2; F3 Fraction 3; F4, Fraction 4; and F5, Fraction 5.</p>
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<p>Refractive index of the essential oil obtained from Mexican lime juice by continuous steam distillation with a column and without a column. Sc, without column; Cc, with column; F1, Fraction 1; F2, Fraction 2; F3, Fraction 3; F4, Fraction 4; and F5, Fraction 5.</p>
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<p>Optical rotation of the essential oil obtained from Mexican lime juice by continuous steam distillation with a column and without a column Sc, without column; Cc, with column; F1, Fraction 1; F2, Fraction 2; F3, Fraction 3; F4, Fraction 4; and F5, Fraction 5.</p>
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34 pages, 2351 KiB  
Review
Vaccinium spp. Berries in the Prevention and Treatment of Non-Alcoholic Fatty Liver Disease: A Comprehensive Update of Preclinical and Clinical Research
by Ewelina Książek, Zuzanna Goluch and Marta Bochniak
Nutrients 2024, 16(17), 2940; https://doi.org/10.3390/nu16172940 - 2 Sep 2024
Viewed by 919
Abstract
Non-alcoholic fatty liver disease (NAFLD) is a common chronic liver disorder marked by the buildup of triacylglycerols (TGs) in the liver. It includes a range of conditions, from simple steatosis to more severe forms like non-alcoholic steatohepatitis (NASH), which can advance to fibrosis, [...] Read more.
Non-alcoholic fatty liver disease (NAFLD) is a common chronic liver disorder marked by the buildup of triacylglycerols (TGs) in the liver. It includes a range of conditions, from simple steatosis to more severe forms like non-alcoholic steatohepatitis (NASH), which can advance to fibrosis, cirrhosis, and hepatocellular carcinoma. NAFLD’s prevalence is rising globally, estimated between 10% and 50%. The disease is linked to comorbidities such as obesity, type 2 diabetes, insulin resistance, and cardiovascular diseases and currently lacks effective treatment options. Therefore, researchers are focusing on evaluating the impact of adjunctive herbal therapies in individuals with NAFLD. One herbal therapy showing positive results in animal models and clinical studies is fruits from the Vaccinium spp. genus. This review presents an overview of the association between consuming fruits, juices, and extracts from Vaccinium spp. and NAFLD. The search used the following keywords: ((Vaccinium OR blueberry OR bilberry OR cranberry) AND (“non-alcoholic fatty liver disease” OR “non-alcoholic steatohepatitis”)). Exclusion criteria included reviews, research notes, book chapters, case studies, and grants. The review included 20 studies: 2 clinical trials and 18 studies on animals and cell lines. The findings indicate that juices and extracts from Vaccinium fruits and leaves have significant potential in addressing NAFLD by improving lipid and glucose metabolism and boosting antioxidant and anti-inflammatory responses. In conclusion, blueberries appear to have the potential to alleviate NAFLD, but more clinical trials are needed to confirm these benefits. Full article
(This article belongs to the Special Issue Nutrition in the Liver Damage)
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<p>Flow diagram of the study selection process.</p>
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<p>Systemic anti-inflammatory and antioxidant effects of dietary polyphenols.</p>
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<p>General overview of the impact of <span class="html-italic">Vaccinium</span> spp. on transcription factors. ACC—acetyl-coenzyme A carboxylas; ACOX1—acyl-CoA oxidase1; ADP—adenosine-5′-diphosphate; AMPK—AMP-activated protein kinase; CPTIα—carnitine palmitoyltransferase-I-alpha; PPAR—peroxisome proliferator-activated receptor; SREBP—sterol regulatory element-binding protein; ↑—increase; ↓—decrease;.</p>
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19 pages, 847 KiB  
Article
Hispanic Thrifty Food Plan (H-TFP): Healthy, Affordable, and Culturally Relevant
by Romane Poinsot, Matthieu Maillot and Adam Drewnowski
Nutrients 2024, 16(17), 2915; https://doi.org/10.3390/nu16172915 - 1 Sep 2024
Viewed by 1073
Abstract
The USDA Thrifty Food Plan (TFP) is a federal estimate of a healthy diet at lowest cost for US population groups defined by gender and age. The present goal was to develop a version of the TFP that was more tailored to the [...] Read more.
The USDA Thrifty Food Plan (TFP) is a federal estimate of a healthy diet at lowest cost for US population groups defined by gender and age. The present goal was to develop a version of the TFP that was more tailored to the observed dietary patterns of self-identified Hispanic participants in NHANES 2013–16. Analyses used the same national food prices and nutrient composition data as the TFP 2021. Diet quality was measured using the Healthy Eating Index 2015. The new Hispanic TFP (H-TFP) was cost-neutral with respect to TFP 2021 and fixed at $186/week for a family of four. Two H-TFP models were created using a quadratic programming (QP) algorithm. Fresh pork was modeled separately from other red meats. Hispanic NHANES participants were younger, had lower education and incomes, but had similar or higher HEI 2015 scores than non-Hispanics. Their diet included more pulses, beans, fruit, 100% juice, grain-based dishes, and soups, but less pizza, coffee, candy, and desserts. The H-TFP market basket featured more pork, whole grains, 100% fruit juice, and cheese. The second TFP model showed that pork could replace both poultry and red meat, while satisfying all nutrient needs. A vegetarian H-TFP proved infeasible for most age–gender groups. Healthy, affordable, and culturally relevant food plans can be developed for US population subgroups. Full article
(This article belongs to the Section Nutrition and Public Health)
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<p>A schema of the quadratic programming optimization model, showing model inputs and model constraints. <sup>1</sup> weighed by Hispanic consumptions.</p>
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<p>Food plan costs for all foods groups (<b>a</b>) and for the protein food group (<b>b</b>) in <span>$</span>/week by model and market basket group for a family of four.</p>
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24 pages, 2899 KiB  
Article
Polyphenol-Rich Aronia melanocarpa Fruit Beneficially Impact Cholesterol, Glucose, and Serum and Gut Metabolites: A Randomized Clinical Trial
by Morgan L. Chamberlin, Jesse T. Peach, Stephanie M.G. Wilson, Zachary T. Miller, Brian Bothner, Seth T. Walk, Carl J. Yeoman and Mary P. Miles
Foods 2024, 13(17), 2768; https://doi.org/10.3390/foods13172768 - 30 Aug 2024
Viewed by 651
Abstract
Polyphenol-rich Aronia fruits have great potential as a functional food with anti-inflammatory, hypolipidemic, and hypoglycemic biologic activities. However, clinical intervention trials investigating the impact of Aronia fruit consumption on human health are limited. A randomized, controlled, double-blinded, parallel intervention trial was conducted using [...] Read more.
Polyphenol-rich Aronia fruits have great potential as a functional food with anti-inflammatory, hypolipidemic, and hypoglycemic biologic activities. However, clinical intervention trials investigating the impact of Aronia fruit consumption on human health are limited. A randomized, controlled, double-blinded, parallel intervention trial was conducted using 14 human subjects who ingested either 0 mL or 100 mL of Aronia juice daily for 30 days. Anthropometric measurements, fasting, and postprandial measures of glucose and lipid metabolism and inflammation, 16S rRNA fecal microbial composition data, and mass spectrometry-acquired serum and fecal metabolomic data were collected before and after the intervention period. Data were analyzed using general linear models, ANOVA, and t-tests. Daily consumption of Aronia prevented a rise in cholesterol levels (β = −0.50, p = 0.03) and reduced postprandial glucose (β = −3.03, p < 0.01). No difference in microbial community composition by condition was identified at any taxonomic level, but a decrease (β = −18.2, p = 0.04) in microbial richness with Aronia was detected. Serum and fecal metabolomic profiles indicated shifts associated with central carbon and lipid metabolism and decreases in pro-inflammatory metabolites. Our study further informs the development of polyphenol-based dietary strategies to lower metabolic disease risk. Full article
(This article belongs to the Special Issue Polyphenols and Health Benefits—Volume II)
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<p>Summary plots of delta (d) values calculated as (post-intervention−pre-intervention) in (<b>A</b>) fasting glucose (dGLU), (<b>B</b>) fasting triglyceride (dTG), (<b>C</b>) fasting total cholesterol (dCHOL), (<b>D</b>) fasting HDL cholesterol (dHDL), and (<b>E</b>) fasting LDL cholesterol (dLDL). Differences between intervention groups determined by ANOVA.</p>
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<p>Summary plot of individual changes (post-intervention−pre-intervention) in glucose area under the curve (dGLU<sub>AUC</sub>). dGLU<sub>AUC</sub> values represent the change in the sum of values from fasting and hourly time points for 6 h post-high-fat meal ingestion. Each bar is representative of the value for one participant (<span class="html-italic">n</span> = 13). Difference in dGLU<sub>AUC</sub> between meal groups determined with ANOVA and displayed in inset.</p>
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<p>Alpha and beta diversity of the gut microbiome. (<b>A</b>) Microbial richness, (<b>B</b>) microbial evenness, and (<b>C</b>) microbial community composition. Richness and evenness beta coefficients were derived from non-parametric rank-based estimation methods. Bars represent 95% confidence interval. Beta diversity at the genus level was visualized using non-metric dimensional scaling (NMDS). Each point represents a single sample, with numbers indicating the specific subject.</p>
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<p>Suspect screening statistical analysis results in serum. Violin plots depict relative concentration changes (post−pre intervention) of fasting asparagine and tyrosine levels. Black points represent participant values and yellow rhombus indicates group median. Both amino acids were upregulated in the Aronia group after 4 weeks. <span class="html-italic">p</span>-values are indicated in each panel for the relationship using a <span class="html-italic">t</span>-test.</p>
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<p>Untargeted analysis of the fasting serum metabolome. (<b>A</b>) <span class="html-italic">t</span>-test results comparing relative concentration change (post−pre intervention) of serum metabolome features between experimental groups. Features with <span class="html-italic">p</span> &lt; 0.05 after FDR correction are indicated with red dots and features above this cut-off are indicated with gray dots. (<b>B</b>) Violin plots of the three significant features, with specific <span class="html-italic">t</span>-test <span class="html-italic">p</span>-values shown. Black points represent participant values and yellow rhombus indicates group median.</p>
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<p>Violin plot of the relative concentration change (post–pre intervention) of fecal chenodeoxycholic acid (CDCA). Black points represent participant values and yellow rhombus indicates group median. CDCA levels were upregulated in the Aronia group after 4 weeks. A <span class="html-italic">p</span>-value of 0.07 was calculated using a one-way ANOVA test.</p>
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<p>Untargeted analysis of fecal metabolome. Violin plots (<b>A</b>–<b>D</b>) depict the relative concentrations of significantly different features before and after the intervention in both experimental groups. Black points represent participant values and yellow rhombus indicates group median. All annotated features were found to be lipids: phosphatidylserine (PS), phosphatidic acid (PA), diglyceride (DG), and phosphatidylglycerol (PG).</p>
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15 pages, 3724 KiB  
Article
Blues from Tikuna/Magüta Masks and a Still Unknown Blue Colorant in Technical Art History and Conservation Science
by Thiago Sevilhano Puglieri and Laura Maccarelli
Heritage 2024, 7(9), 4697-4711; https://doi.org/10.3390/heritage7090222 - 29 Aug 2024
Viewed by 576
Abstract
Blue is one of the most challenging colors for humans to produce and one of the most important colors in art history. Literature from the Tikuna/Magüta culture, from the Amazon Forest, suggests the use of chemical reactions between the juice of the naīcü [...] Read more.
Blue is one of the most challenging colors for humans to produce and one of the most important colors in art history. Literature from the Tikuna/Magüta culture, from the Amazon Forest, suggests the use of chemical reactions between the juice of the naīcü fruit and iron to produce a blue colorant still unknown among technical art historians and conservation scientists. Additionally, the coloring materials from the Tikuna/Magüta people were never chemically investigated. Therefore, this manuscript presents the investigation of blue colorants from twenty-two Tikuna/Magüta masks and one stamp used to decorate similar items. Collections from four museums, from the USA and Brazil, were examined, and Raman spectra indicated the presence of Prussian blue, phthalocyanine blue, indigo, ultramarine, crystal violet, amorphous carbon, anatase, and barium sulfate (or lithopone). Although the unknown blue colorant was not detected in this campaign, the authors hypothesize the chemical composition and reactions involved in its production by considering the chemistry of naīcü and anthocyanins. The continuation of this work with community-based participatory research (CBPR) approaches is also discussed, justifying why reproduction was not considered in this work and supporting a more socially responsible and inclusive practice in technical art history and conservation science. Full article
(This article belongs to the Special Issue Dyes in History and Archaeology 42)
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<p>Tikuna/Magüta items from the MAE. Reference numbers: RG 8649, RG 10034, RG 8716, RG 9984, RG 8753 (2), RG 8753, RG 8889, RG 8892, RG 8894, RG 8898, RG 8902, RG 8710, RG 8764, RG 9454, and RG 10098 (by Ader Gotardo); credits: Museu de Arqueologia e Etnologia da Universidade de São Paulo.</p>
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<p>Tikuna/Magüta item 996-24-30/11694 from the Peabody Museum; credits: Gift of Richard E. Schultes, 1996. Courtesy of the Peabody Museum of Archaeology and Ethnology, Harvard University, 996-24-30/11694. No photo is available from item 47-8-30/5627.</p>
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<p>Tikuna/Magüta item X64.965 (by Thiago Sevilhano Puglieri and Christian De Brer) from the Fowler Museum; credits: ©Photo courtesy of the Fowler Museum at UCLA; Tikuna/Magüta.</p>
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<p>Tikuna/Magüta items from the Magüta Museum. Reference numbers: MM374, MM383, MM384, MM385, and MM387 (by Thiago Sevilhano Puglieri); credits: Thiago Sevilhano Puglieri.</p>
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<p>Representative Raman spectra (785 nm) of each colorant identified in this research. From the top to the bottom: Prussian blue, phthalocyanine blue, crystal violet, indigo, amorphous carbon, and ultramarine.</p>
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<p>Chemical structures of cyanidin-3-O-glucoside (R<sub>1</sub> = OH, R<sub>2</sub> = H) and delphinidin-3-O-glucoside (R<sub>1</sub> = OH, R<sub>2</sub> = OH); glc = glycoside.</p>
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<p>Representation of the potential chelates in the blue pigment prepared by the Tikuna/Magüta people by mixing fruits from naīcü with iron. (<b>a</b>) is from cyanidin-3-O-glucoside and (<b>b</b>) from delphinidin-3-O-glucoside; glc = glycoside. Not all the Fe<sup>3+</sup>–ligand chemical bonds are represented in this figure.</p>
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24 pages, 1171 KiB  
Article
Black and Red Currant Pomaces as Raw Materials to Create Smoothies with In Vitro Health-Promoting Potential
by Martyna Szydłowska, Aneta Wojdyło and Paulina Nowicka
Foods 2024, 13(17), 2715; https://doi.org/10.3390/foods13172715 - 27 Aug 2024
Viewed by 442
Abstract
Pomace is a by-product resulting from the pressing of fruits and vegetables into juices, and it is typically treated as waste. Interestingly, pomace contains minimal amounts of protein and fat but is characterized by its high polyphenol and dietary fiber contents, which may [...] Read more.
Pomace is a by-product resulting from the pressing of fruits and vegetables into juices, and it is typically treated as waste. Interestingly, pomace contains minimal amounts of protein and fat but is characterized by its high polyphenol and dietary fiber contents, which may have health benefits for human physiology. Therefore, they are a potentially attractive raw material for the food industry, but to our knowledge, no smoothies with their addition have been prepared and described so far. Consequently, products derived from apple juice, incorporating different doses of fresh (6% and 12%) and dried (3% and 6%) black or red currant pomace, were formulated, and their physical properties, chemical composition, bioactive compound content, and health-promoting potential (in vitro antioxidant and antidiabetic activity) were evaluated. Additionally, the products underwent sensory assessment by consumers. The fortified beverages exhibited different physical characteristics and chemical compositions than apple juice. All smoothies were characterized by higher concentrations of anthocyanins, flavonols, and procyanidin polymers compared to the base product. Moreover, 75% of them exhibited a significantly elevated phenolic acid content as well as a higher concentration of flavan-3-ols. The majority of fresh smoothies exhibited significantly higher in vitro antioxidant capacities and increased in vitro α-amylase and α-glucosidase inhibitory effects compared to the base product. The highest ABTS activity was recorded in the variant with 6% dried black currant pomace. In turn, the smoothie with 3% dried red currant pomace had the most effective FRAP effect and, together with the product containing 12% fresh black currant pomace, ORAC antioxidant activity and α-glucosidase inhibition also. The introduction of 6% dried red currant pomace led to the creation of a beverage that most effectively inhibited α-glucosidase. The study showed that the application of various types of pomace, mainly that of black currant, into apple juice enables the development of new functional products with sensory attributes that are favorably evaluated by consumers. Full article
(This article belongs to the Section Nutraceuticals, Functional Foods, and Novel Foods)
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<p>Sensory evaluation of base juice (BJ) and products with the addition of red and black currant pomaces.</p>
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<p>Average amount of fruit flavors determined in the products.</p>
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<p>The product with the most favorable overall ratings (4.5): apple juice.</p>
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<p>The product with the most favorable overall ratings (4.5): smoothie with 6% dried black currant pomace.</p>
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20 pages, 2178 KiB  
Article
Yield Performance and Quality Assessment of Brazilian Hybrid Grapes Influenced by Rootstocks and Training Systems
by Francisco José Domingues Neto, Marco Antonio Tecchio, Cristine Vanz Borges, João Domingos Rodrigues, Elizabeth Orika Ono, Giuseppina Pace Pereira Lima, Mara Fernandes Moura, José Luiz Hernandes, Marcelo de Souza Silva and Magali Leonel
Horticulturae 2024, 10(9), 909; https://doi.org/10.3390/horticulturae10090909 - 27 Aug 2024
Viewed by 384
Abstract
The choice of training system impacts the architecture and physiological characteristics of grapevines, affecting grape production and quality. Continuous studies are necessary to optimize viticulture production in Brazil. This study aimed to evaluate the effects of rootstocks and different training systems on the [...] Read more.
The choice of training system impacts the architecture and physiological characteristics of grapevines, affecting grape production and quality. Continuous studies are necessary to optimize viticulture production in Brazil. This study aimed to evaluate the effects of rootstocks and different training systems on the production and quality of ‘IAC 138-22 Máximo’ and ‘BRS Violeta’ grapevines for juice and wine. The experiment was conducted over two productive cycles (2019/2020 and 2020/2021) in an experimental vineyard at the Advanced Center for Fruit Research as part of the Agronomic Institute (IAC), in Jundiaí, São Paulo, Brazil (23°06′ S, 46°55′ W, and 745 m altitude). For each cultivar, a randomized block design in a 2 × 2 factorial scheme was used, with two rootstocks (‘IAC 766 Campinas’ and 106-8 ‘Mgt’) and two training systems (low and high trellises), with five blocks of three plants per experimental plot. In both cycles, the gas exchange and grapevine production, the chemical characteristics of the grape juice (must), and the chemical compounds in the berry skins were evaluated. The rootstocks and training systems influenced the variables evaluated in both cultivars, with the high trellis system providing the best results. This approach increased the photosynthetic rate, improved water-use efficiency, elevated grapevine production, and enhanced fruit quality. Therefore, its use is recommended for training grapevines. Regarding rootstocks, the best scion–rootstock affinity was found between hybrid grapevines and ‘IAC 766 Campinas’. Full article
(This article belongs to the Special Issue Orchard Management under Climate Change)
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<p>Pruning and harvest times for Brazilian hybrid grapes in two productive cycles, in Jundiaí, São Paulo, Brazil.</p>
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<p>Principal component analysis of hybrid vines on different rootstocks and training systems. (<b>A</b>) ‘IAC 138-22 Máximo’ and (<b>B</b>) ‘BRS Violeta’. Notes: internal carbon concentration (Ci), total chlorophyll (Chlor), anthocyanins (Ant), soluble solids (SS), fresh cluster weight (FCW), phenolic compounds (PC), productivity (Prod), water-use efficiency (WUE), reducing sugars (RS), number of clusters per plant (NCP), electron transport rate (ETR), assimilation rate (A), titratable acidity (TA), stomatal conductance (gs), transpiration rate (E).</p>
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<p>Graphical abstract of the two grapevine hybrids, ‘IAC 138-22 Maximo’ and ‘BRS Violeta’ and their interaction with the two trellis systems (low 1.6 m and high 2.0 m) and two rootstocks, ‘IAC 766’ (766) and ‘106-8 Mgt’ (Mgt). Notes: water-use efficiency (WUE), electron transport rate (ETR), transpiration rate (E), total chlorophyll (Chlor), number of clusters per plant (NCP), fresh cluster weight (FCW), soluble solids (SS), titratable acidity (TA), reducing sugars (RS), phenolic compounds (PC), total monomeric anthocyanins (Ant), and antioxidant activity (AA).</p>
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9 pages, 892 KiB  
Communication
Influence of Solvent Concentration on the Amount of Individual Phenolic Compounds in Apple and Sour Cherry Pomace
by Maria Bianca Mandache, Ana-Maria Stoenescu and Sina Cosmulescu
Horticulturae 2024, 10(9), 900; https://doi.org/10.3390/horticulturae10090900 - 26 Aug 2024
Viewed by 350
Abstract
Apple and sour cherry pomace, by-products resulting from fruit processing for juice production, were analysed using high-performance liquid chromatography (HPLC) to identify and quantify individual phenolic compounds. In order to determine the most efficient method of extracting these phenolic compounds from pomace, different [...] Read more.
Apple and sour cherry pomace, by-products resulting from fruit processing for juice production, were analysed using high-performance liquid chromatography (HPLC) to identify and quantify individual phenolic compounds. In order to determine the most efficient method of extracting these phenolic compounds from pomace, different concentrations of ethanol were used as the organic solvent. The following phenolic compounds were analysed: gallic acid, neochlorogenic acid, (+)-catechin, (−)-epicatechin, chlorogenic acid, vanillic acid, caffeic acid, ferulic acid, sinapic acid, salicylic acid, ellagic acid, rutin, and myricetin. The amounts of these compounds varied depending on the concentration of ethanol used in the extraction process. Neochlorogenic acid, a potent antioxidant, was quantified in apple and sour cherry pomace extracts, showing significant variation with solvent concentration. In apple pomace, the highest amount was found in ethanol 100% (46.44 mg 100 g−1 DW), followed by ethanol 75% (32.09 mg 100 g−1 DW) and ethanol 50% (7.66 mg 100 g−1 DW). In sour cherry pomace, the highest amount was also extracted into ethanol 100% (45.20 mg 100 g−1 DW) and the lowest in ethanol 50% (29.12 mg 100 g−1 DW). Catechin was detected exclusively in cherry pomace, with a maximum yield observed in 75% ethanol (137.86 mg 100 g−1 DW), which was significantly higher compared to the other phenolic compounds analysed. The obtained results demonstrate the importance of apple and sour cherry pomace as valuable by-products, with the potential to be used in the production of functional foods. Full article
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<p>Chromatogram of 75% Ethanol apple pomace (1, gallic acid; 2, neochlorogenic acid; 4, chlorogenic acid; 5, vanillic acid; 7, (−)-epicatechin; 8, ferulic acid; 11, ellagic acid; 12, rutin; and 13, myricetin).</p>
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<p>Chromatogram of 50% Ethanol sour cherry pomace (1, gallic acid; 2, neochlorogenic acid; 3, (+)-catechin; 4, chlorogenic acid; 5, vanillic acid; 7, (−)-epicatechin; 9, sinapic acid; 10, salicylic acid; 11, ellagic acid; 12, rutin; and 13, myricetin).</p>
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