WO2008084844A1 - ハニカム構造体の製造方法 - Google Patents
ハニカム構造体の製造方法 Download PDFInfo
- Publication number
- WO2008084844A1 WO2008084844A1 PCT/JP2008/050248 JP2008050248W WO2008084844A1 WO 2008084844 A1 WO2008084844 A1 WO 2008084844A1 JP 2008050248 W JP2008050248 W JP 2008050248W WO 2008084844 A1 WO2008084844 A1 WO 2008084844A1
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- WIPO (PCT)
- Prior art keywords
- molding
- honeycomb
- honeycomb structure
- slope
- straight line
- Prior art date
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
- B01J35/56—Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional monoliths
- B01J35/57—Honeycombs
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
- C04B35/185—Mullite 3Al2O3-2SiO2
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- C—CHEMISTRY; METALLURGY
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
- C04B35/19—Alkali metal aluminosilicates, e.g. spodumene
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
- C04B35/195—Alkaline earth aluminosilicates, e.g. cordierite or anorthite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
- C04B35/478—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on aluminium titanates
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
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- C—CHEMISTRY; METALLURGY
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
- C04B35/573—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide obtained by reaction sintering or recrystallisation
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/581—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on aluminium nitride
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/584—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on silicon nitride
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/0006—Honeycomb structures
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00793—Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
- F01N3/00—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust
- F01N3/02—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for cooling, or for removing solid constituents of, exhaust
- F01N3/021—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for cooling, or for removing solid constituents of, exhaust by means of filters
- F01N3/022—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for cooling, or for removing solid constituents of, exhaust by means of filters characterised by specially adapted filtering structure, e.g. honeycomb, mesh or fibrous
- F01N3/0222—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for cooling, or for removing solid constituents of, exhaust by means of filters characterised by specially adapted filtering structure, e.g. honeycomb, mesh or fibrous the structure being monolithic, e.g. honeycombs
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Filtering Materials (AREA)
- Press-Shaping Or Shaping Using Conveyers (AREA)
- Porous Artificial Stone Or Porous Ceramic Products (AREA)
Abstract
セラミックスからなる主成分材料に、成形助剤、添加材及び気孔形成材を含有する成形原料を混練し・調製された坏土を成形、乾燥してハニカム形状の成形体(ハニカム成形体)を作製し、作製されたハニカム成形体を仮焼成して仮焼体とした後に仮焼体を本焼成してハニカム焼成体を得るハニカム構造体の製造方法である。坏土もしくは成形体の引張り荷重測定を行った際、得られた引張り荷重と変位量との関係を示すグラフの変極点bと降伏点cを結ぶ直線の傾きθが、弾性変形を示す始点aと変極点bを結ぶ直線の傾きδの100%未満である。本発明のハニカム構造体の製造方法によれば、ハニカム成形時の欠陥生成を抑制し、歩留まりを向上させ、且つハニカム構造体の実使用時においても新たな欠陥が生成しにくく、耐久性に優れたハニカム構造体を製造することができる。
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2008553118A JPWO2008084844A1 (ja) | 2007-01-12 | 2008-01-11 | ハニカム構造体の製造方法 |
EP08703112A EP2119687A4 (en) | 2007-01-12 | 2008-01-11 | METHOD FOR PRODUCING A WAVE STRUCTURE |
US12/498,883 US20090267273A1 (en) | 2007-01-12 | 2009-07-07 | Process for producing honeycomb structure |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2007004864 | 2007-01-12 | ||
JP2007-004864 | 2007-01-12 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US12/498,883 Continuation US20090267273A1 (en) | 2007-01-12 | 2009-07-07 | Process for producing honeycomb structure |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2008084844A1 true WO2008084844A1 (ja) | 2008-07-17 |
Family
ID=39608731
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/JP2008/050248 WO2008084844A1 (ja) | 2007-01-12 | 2008-01-11 | ハニカム構造体の製造方法 |
Country Status (4)
Country | Link |
---|---|
US (1) | US20090267273A1 (ja) |
EP (1) | EP2119687A4 (ja) |
JP (1) | JPWO2008084844A1 (ja) |
WO (1) | WO2008084844A1 (ja) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2010022785A (ja) * | 2008-07-22 | 2010-02-04 | Shinwa Corp | 脱臭フィルタ |
JP2010052407A (ja) * | 2008-08-29 | 2010-03-11 | Hitachi Metals Ltd | セラミックスの製造方法 |
JP2010228219A (ja) * | 2009-03-26 | 2010-10-14 | Ngk Insulators Ltd | ハニカム成形体の乾燥方法 |
WO2012023375A1 (ja) * | 2010-08-19 | 2012-02-23 | 東亞合成株式会社 | セラミック成形用乾燥収縮低減剤及びセラミック成形体の乾燥収縮低減方法 |
WO2012023376A1 (ja) * | 2010-08-19 | 2012-02-23 | 東亞合成株式会社 | セラミック成形用乾燥収縮低減剤及びセラミック成形体の乾燥収縮低減方法 |
WO2012033078A1 (ja) * | 2010-09-10 | 2012-03-15 | 東亞合成株式会社 | セラミック成形用添加剤 |
CN108358641A (zh) * | 2018-03-23 | 2018-08-03 | 陕西科技大学 | 一种Al4SiC4陶瓷材料的制备方法 |
CN112939583A (zh) * | 2021-02-22 | 2021-06-11 | 山东奥福环保科技股份有限公司 | 一种铝矾土尾矿制备的rto蜂窝陶瓷蓄热体及其制备方法 |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2597075B1 (de) * | 2011-11-23 | 2016-01-27 | Stiholt, Leif | Poröser alpha-sic-haltiger formkörper mit durchgehend offener porenstruktur |
CN111402540B (zh) * | 2020-02-25 | 2021-08-24 | 王勇强 | 吸气式感烟火灾探测装置、方法及设备 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999007652A1 (en) | 1997-08-08 | 1999-02-18 | Corning Incorporated | Improved method of forming and shaping plasticized mixtures and the green bodies made therefrom |
WO1999010294A1 (en) | 1997-08-27 | 1999-03-04 | Corning Incorporated | Improved method of forming and shaping plasticized mixtures by low to moderate shear extrusion |
US6344078B1 (en) | 1999-05-27 | 2002-02-05 | Corning Incorporated | Binder system for honeycomb ceramic bodies and a method for producing said honeycomb bodies |
WO2005063360A1 (ja) * | 2003-12-26 | 2005-07-14 | Ngk Insulators, Ltd. | ハニカム構造体の製造方法 |
US20060290036A1 (en) | 2005-06-27 | 2006-12-28 | Ngk Insulators, Ltd. | Method of manufacturing honeycomb structure |
-
2008
- 2008-01-11 JP JP2008553118A patent/JPWO2008084844A1/ja active Pending
- 2008-01-11 WO PCT/JP2008/050248 patent/WO2008084844A1/ja active Application Filing
- 2008-01-11 EP EP08703112A patent/EP2119687A4/en not_active Withdrawn
-
2009
- 2009-07-07 US US12/498,883 patent/US20090267273A1/en not_active Abandoned
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999007652A1 (en) | 1997-08-08 | 1999-02-18 | Corning Incorporated | Improved method of forming and shaping plasticized mixtures and the green bodies made therefrom |
WO1999010294A1 (en) | 1997-08-27 | 1999-03-04 | Corning Incorporated | Improved method of forming and shaping plasticized mixtures by low to moderate shear extrusion |
US6344078B1 (en) | 1999-05-27 | 2002-02-05 | Corning Incorporated | Binder system for honeycomb ceramic bodies and a method for producing said honeycomb bodies |
WO2005063360A1 (ja) * | 2003-12-26 | 2005-07-14 | Ngk Insulators, Ltd. | ハニカム構造体の製造方法 |
EP1698388A1 (en) | 2003-12-26 | 2006-09-06 | Ngk Insulators, Ltd. | Method of producing honeycomb structure body |
US20060290036A1 (en) | 2005-06-27 | 2006-12-28 | Ngk Insulators, Ltd. | Method of manufacturing honeycomb structure |
JP2007001836A (ja) * | 2005-06-27 | 2007-01-11 | Ngk Insulators Ltd | ハニカム構造体の製造方法 |
Non-Patent Citations (1)
Title |
---|
See also references of EP2119687A4 |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2010022785A (ja) * | 2008-07-22 | 2010-02-04 | Shinwa Corp | 脱臭フィルタ |
JP2010052407A (ja) * | 2008-08-29 | 2010-03-11 | Hitachi Metals Ltd | セラミックスの製造方法 |
JP2010228219A (ja) * | 2009-03-26 | 2010-10-14 | Ngk Insulators Ltd | ハニカム成形体の乾燥方法 |
WO2012023375A1 (ja) * | 2010-08-19 | 2012-02-23 | 東亞合成株式会社 | セラミック成形用乾燥収縮低減剤及びセラミック成形体の乾燥収縮低減方法 |
WO2012023376A1 (ja) * | 2010-08-19 | 2012-02-23 | 東亞合成株式会社 | セラミック成形用乾燥収縮低減剤及びセラミック成形体の乾燥収縮低減方法 |
JP5660135B2 (ja) * | 2010-08-19 | 2015-01-28 | 東亞合成株式会社 | セラミック成形用乾燥収縮低減剤及びセラミック成形体の乾燥収縮低減方法 |
JP5660136B2 (ja) * | 2010-08-19 | 2015-01-28 | 東亞合成株式会社 | セラミック成形用乾燥収縮低減剤及びセラミック成形体の乾燥収縮低減方法 |
WO2012033078A1 (ja) * | 2010-09-10 | 2012-03-15 | 東亞合成株式会社 | セラミック成形用添加剤 |
JP5273311B2 (ja) * | 2010-09-10 | 2013-08-28 | 東亞合成株式会社 | セラミック成形用添加剤 |
US9056800B2 (en) | 2010-09-10 | 2015-06-16 | Toagosei., Ltd. | Additive for molding of ceramic material |
CN108358641A (zh) * | 2018-03-23 | 2018-08-03 | 陕西科技大学 | 一种Al4SiC4陶瓷材料的制备方法 |
CN112939583A (zh) * | 2021-02-22 | 2021-06-11 | 山东奥福环保科技股份有限公司 | 一种铝矾土尾矿制备的rto蜂窝陶瓷蓄热体及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
EP2119687A1 (en) | 2009-11-18 |
JPWO2008084844A1 (ja) | 2010-05-06 |
US20090267273A1 (en) | 2009-10-29 |
EP2119687A4 (en) | 2011-08-17 |
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