CN114081038A - Pesticide composition and production process thereof - Google Patents
Pesticide composition and production process thereof Download PDFInfo
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- CN114081038A CN114081038A CN202111214954.9A CN202111214954A CN114081038A CN 114081038 A CN114081038 A CN 114081038A CN 202111214954 A CN202111214954 A CN 202111214954A CN 114081038 A CN114081038 A CN 114081038A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
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- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
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- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
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Abstract
The invention discloses a pesticide composition and a production process thereof, wherein the pesticide composition comprises the following raw materials in parts by weight: 3-7 parts of benzyl dimethyl phenol polyoxyethylene ether, 5-17 parts of abamectin, 2-17 parts of cyfluthrin, 5-7 parts of calcium dodecyl benzene sulfonate, 15-27 parts of tebufenozide, 30-55 parts of soybean oil, 5-15 parts of a penetrating agent, 5-15 parts of an organic solvent, 15-20 parts of an alkaloid, 5-15 parts of a thickening agent and 5-17 parts of an alcohol anti-freezing agent. The production process of the pesticide composition has the advantages that the penetrant and the thickener are added into the pesticide to stabilize the pesticide formulation, so that the storage time of the pesticide composition is prolonged, layering and precipitation and crystallization do not occur, the degradation rate of active ingredients is very low, the practicability of the pesticide composition is improved, the pesticide composition is not easy to freeze in winter by adding the alcohol antifreeze agent into the pesticide solution, the pesticide composition has good adhesion and permeability, the pesticide solution is slightly acidic by setting the regulator, the pest control effect of the pesticide composition is remarkable, the using amount is reduced, and the soil property is not influenced during use.
Description
Technical Field
The invention relates to the technical field of pesticides, in particular to a production process of a pesticide composition.
Background
In recent years, due to the use of a large amount of various pesticides, the pesticide resistance of agricultural pests is higher and higher, such as rice planthoppers, chilo suppressalis, tryporyza incertulas and rice leaf rollers, which are main pests of rice in China, and the occurrence of the pests in rice regions in Yangtze river valley is particularly serious. It can cause a great deal of withered hearts in the tillering stage, and can cause a great deal of insect-damaged plants in addition to white ears in the later growth stage of rice, so that the plants are laid down in pieces. In recent years, although the use of high-toxicity pesticides on vegetables and flower seedlings is prohibited by national commands, poisoning events are often caused by eating the vegetables containing residual high-toxicity pesticides and using and watching the flower seedlings, so that the development of high-efficiency low-toxicity and low-residual pesticides is a necessary development trend, and a production process of the pesticide composition is provided.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a production process of an insecticide composition, which has the following advantages and solves the problems.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme: the pesticide composition comprises the following raw materials in parts by weight: 3-7 parts of benzyl dimethyl phenol polyoxyethylene ether, 5-17 parts of abamectin, 2-17 parts of cyfluthrin, 5-7 parts of calcium dodecyl benzene sulfonate, 15-27 parts of tebufenozide, 30-55 parts of soybean oil, 5-15 parts of a penetrating agent, 5-15 parts of an organic solvent, 15-20 parts of an alkaloid, 5-15 parts of a thickening agent, 5-17 parts of an alcohol anti-freezing agent, 5-15 parts of a regulator, 5-10 parts of a wetting dispersant, 5-15 parts of an organic silicon defoamer, 15-25 parts of bentonite and 60-90 parts of water.
Preferably, the osmotic agent includes at least one of dioctyl sodium sulfosuccinate and sodium di-sec-sulfosuccinate.
Preferably, the organic solvent is one or more of benzene, toluene, kerosene and acetone; the alkaloid is one of derris and folium Artemisiae Argyi.
Preferably, the thickener is one of xanthan gum and magnesium aluminum silicate; the alcohol antifreeze agent is propylene glycol, and the regulator is one of plant ash or citric acid powder.
Preferably, the wetting and dispersing agent is one or more of polyoxyethylene triphenylethylene phenyl phosphate, alkyl naphthalene sulfonate, alkylphenol polyoxyethylene and nonylphenol polyoxyethylene.
A process for producing an insecticide composition comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 1-2h after grinding and stirring for 0.5-1h, then heating, grinding and stirring again for 1-2h, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.02-0.1 mu m, and controlling the shearing time to be 25-30min to obtain a liquid medicament;
5) and (4) cooling the liquid medicine obtained in the step (4) to room temperature, adding a regulator into the liquid medicine, stirring for 10-15min, and finally sieving to obtain the reaction composition.
Preferably, the primary stirring temperature in the step 2 is 60-75 ℃, and the secondary stirring temperature is 80-88 ℃.
Preferably, in the step 5, the regulating agent is added until the liquid medicine is slightly acidic.
(III) advantageous effects
Compared with the prior art, the invention provides a production process of an insecticide composition, which has the following beneficial effects:
1. the production process of the pesticide composition has the advantages that the penetrant and the thickening agent are added into the pesticide to stabilize the pesticide formulation, so that the storage time of the pesticide composition is prolonged, layering and precipitation and crystallization do not occur, the degradation rate of effective components is very low, and the practicability of the pesticide composition is improved.
2. The production process of the pesticide composition has the advantages that the alcohol antifreeze agent is added into the pesticide liquid, so that the pesticide liquid is not easy to freeze in winter and has good adhesion and permeability, the pesticide liquid is slightly acidic through the regulator, the pest control effect of the pesticide liquid is remarkable, the use amount is reduced, and the soil property is not influenced during use.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the pesticide composition comprises the following raw materials in parts by weight: 4 parts of benzyl dimethyl phenol polyoxyethylene ether, 5 parts of abamectin, 2 parts of cyfluthrin, 5 parts of calcium dodecyl benzene sulfonate, 18 parts of tebufenozide, 31 parts of soybean oil and 11 parts of a penetrant, wherein the penetrant comprises dioctyl sodium sulfosuccinate and sodium di-sec-sulfosuccinate, 11 parts of an organic solvent, and the organic solvent is benzene and acetone; the alkaloid is mugwort, 17 parts of alkaloid, 11 parts of thickening agent, 11 parts of alcohol antifreeze agent and 8 parts of regulator, and the thickening agent is xanthan gum; the alcohol antifreezing agent is propylene glycol, the regulator is citric acid powder, the wetting dispersant is 8 parts, the wetting dispersant is alkyl naphthalene sulfonate and alkylphenol polyoxyethylene, the organic silicon defoamer is 5 parts, bentonite is 15 parts, and water is 61 parts;
a process for producing an insecticide composition comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 1h after grinding and stirring for 1h, then heating, grinding and stirring for 1h again, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2, wherein the primary stirring temperature in the step 2 is 61 ℃, and the secondary stirring temperature is 81 ℃;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.04 mu m, and controlling the shearing time to be 28min to obtain a liquid medicament;
5) cooling the liquid medicine obtained in the step 4 to room temperature, adding a regulator into the liquid medicine, stirring for 12min, and finally sieving to obtain a reaction composition, wherein in the step 5, the regulator is added until the liquid medicine is slightly acidic, and the production process of the pesticide composition has the advantages that the agent form is stable by adding a penetrating agent and a thickening agent into the liquid medicine, so that the storage time of the pesticide composition is prolonged, layering and precipitation and crystallization are avoided, the degradation rate of effective components is very low, the practicability of the pesticide composition is improved, the pesticide composition is not easy to freeze in winter by adding an alcohol antifreeze agent into the liquid medicine, and has good adhesion and permeability, the liquid medicine is slightly acidic by setting the regulator, so that the pest control effect of the pesticide composition is remarkable, the using amount is reduced, and the soil property is not influenced during use.
Example two:
the pesticide composition comprises the following raw materials in parts by weight: 3 parts of benzyl dimethylphenol polyoxyethylene ether, 5 parts of abamectin, 2 parts of cyfluthrin, 5 parts of calcium dodecyl benzene sulfonate, 18 parts of tebufenozide, 38 parts of soybean oil and 8 parts of a penetrant, wherein the penetrant comprises dioctyl sodium sulfosuccinate and di-sec-sulfosuccinate sodium sulfonate, and 8 parts of an organic solvent is kerosene and acetone; the alkaloid is mugwort, 18 parts of alkaloid, 8 parts of thickening agent, 8 parts of alcohol antifreeze agent and 8 parts of regulator, and the thickening agent is xanthan gum; the alcohol antifreezing agent is propylene glycol, the regulator is plant ash, the wetting dispersant is 8 parts, the wetting dispersant is polyoxyethylene triphenylethylene phenyl phosphate, the organic silicon defoamer is 5 parts, the bentonite is 18 parts, and the water is 68 parts;
a process for producing an insecticide composition comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 1.5h after grinding and stirring for 0.8h, then heating, grinding and stirring for 1.5h again, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2, wherein the primary stirring temperature in the step 2 is 68 ℃, and the secondary stirring temperature is 86 ℃;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.08 mu m, and controlling the shearing time to be 28min to obtain a liquid medicament;
5) cooling the liquid medicine obtained in the step 4 to room temperature, adding a regulator into the liquid medicine, stirring for 14min, and finally sieving to obtain a reaction composition, wherein in the step 5, the regulator is added until the liquid medicine is slightly acidic, and the production process of the pesticide composition has the advantages that the agent form is stable by adding a penetrating agent and a thickening agent into the liquid medicine, so that the storage time of the pesticide composition is prolonged, layering and precipitation and crystallization are avoided, the degradation rate of effective components is very low, the practicability of the pesticide composition is improved, the pesticide composition is not easy to freeze in winter by adding an alcohol antifreeze agent into the liquid medicine, and has good adhesion and permeability, the liquid medicine is slightly acidic by setting the regulator, so that the pest control effect of the pesticide composition is remarkable, the using amount is reduced, and the soil property is not influenced during use.
Example three:
the pesticide composition comprises the following raw materials in parts by weight: 7 parts of benzyl dimethylphenol polyoxyethylene ether, 17 parts of abamectin, 17 parts of cyfluthrin, 5 parts of calcium dodecyl benzene sulfonate, 17 parts of tebufenozide, 35 parts of soybean oil and 5 parts of a penetrating agent, wherein the penetrating agent comprises dioctyl sodium sulfosuccinate and sodium di-sec-sulfosuccinate, and the organic solvent comprises 5 parts of kerosene and acetone; the alkaloid is derris elliptica, 20 parts of alkaloid, 5 parts of thickening agent, 17 parts of alcohol antifreeze agent and 5 parts of regulator, and the thickening agent is magnesium aluminum silicate; the alcohol antifreezing agent is propylene glycol, the regulator is citric acid powder, the wetting dispersant is 10 parts, the wetting dispersant is polyoxyethylene triphenylethylene phenyl phosphate and nonylphenol polyoxyethylene ether, the organic silicon defoamer is 5 parts, the bentonite is 20 parts, and the water is 69 parts;
a process for producing an insecticide composition comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 1h after grinding and stirring for 1h, then heating, grinding and stirring for 1h again, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2, wherein the primary stirring temperature in the step 2 is 65 ℃, and the secondary stirring temperature is 84 ℃;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.02 mu m, and controlling the shearing time to be 25min to obtain a liquid medicament;
5) cooling the liquid medicine obtained in the step 4 to room temperature, adding a regulator into the liquid medicine, stirring for 11min, and finally sieving to obtain a reaction composition, wherein in the step 5, the regulator is added until the liquid medicine is slightly acidic, and the production process of the pesticide composition has the advantages that the agent form is stable by adding a penetrating agent and a thickening agent into the liquid medicine, so that the storage time of the pesticide composition is prolonged, layering and precipitation and crystallization are avoided, the degradation rate of effective components is very low, the practicability of the pesticide composition is improved, the pesticide composition is not easy to freeze in winter by adding an alcohol antifreeze agent into the liquid medicine, and has good adhesion and permeability, the liquid medicine is slightly acidic by setting the regulator, so that the pest control effect of the pesticide composition is remarkable, the using amount is reduced, and the soil property is not influenced during use.
Example four:
the pesticide composition comprises the following raw materials in parts by weight: 7 parts of benzyl dimethylphenol polyoxyethylene ether, 17 parts of abamectin, 17 parts of cyfluthrin, 7 parts of calcium dodecylbenzene sulfonate, 27 parts of tebufenozide, 55 parts of soybean oil and 15 parts of a penetrant, wherein the penetrant comprises sodium di-sec-sulfosuccinate and 15 parts of an organic solvent, and the organic solvent is benzene, toluene and kerosene; the alkaloid is mugwort, 20 parts of alkaloid, 15 parts of thickening agent, 17 parts of alcohol antifreeze agent and 15 parts of regulator, and the thickening agent is xanthan gum; the alcohol antifreezing agent is propylene glycol, the regulator is plant ash, the wetting dispersant is 10 parts, the wetting dispersant is alkylphenol polyoxyethylene and nonylphenol polyoxyethylene, the organic silicon defoamer is 15 parts, bentonite is 25 parts, and water is 60 parts;
a process for producing an insecticide composition comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 1h after grinding and stirring for 0.5h, then heating, grinding and stirring again for 2h, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2, wherein the primary stirring temperature in the step 2 is 65 ℃, and the secondary stirring temperature is 88 ℃;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.04 mu m, and controlling the shearing time to be 28min to obtain a liquid medicament;
5) cooling the liquid medicine obtained in the step 4 to room temperature, adding a regulator into the liquid medicine, stirring for 15min, and finally sieving to obtain a reaction composition, wherein in the step 5, the regulator is added until the liquid medicine is slightly acidic, and the production process of the pesticide composition has the advantages that the agent form is stable by adding a penetrating agent and a thickening agent into the liquid medicine, so that the storage time of the pesticide composition is prolonged, layering and precipitation and crystallization are avoided, the degradation rate of effective components is very low, the practicability of the pesticide composition is improved, the pesticide composition is not easy to freeze in winter by adding an alcohol antifreeze agent into the liquid medicine, and has good adhesion and permeability, the liquid medicine is slightly acidic by setting the regulator, so that the pest control effect of the pesticide composition is remarkable, the using amount is reduced, and the soil property is not influenced during use.
Example five:
the pesticide composition comprises the following raw materials in parts by weight: 3 parts of benzyl dimethylphenol polyoxyethylene ether, 5 parts of abamectin, 2 parts of cyfluthrin, 5 parts of calcium dodecylbenzene sulfonate, 17 parts of tebufenozide, 35 parts of soybean oil and 5 parts of a penetrating agent, wherein the penetrating agent comprises dioctyl sodium sulfosuccinate and 5 parts of an organic solvent, and the organic solvent is benzene and toluene; the alkaloid is derris elliptica, 20 parts of alkaloid, 15 parts of thickening agent, 5 parts of alcohol antifreeze agent and 15 parts of regulator, and the thickening agent is xanthan gum; the alcohol antifreezing agent is propylene glycol, the regulator is plant ash, the wetting dispersant is 10 parts, the wetting dispersant is polyoxyethylene triphenylethylene phenyl phosphate, alkyl naphthalene sulfonate, the organic silicon defoamer is 15 parts, bentonite is 25 parts, and water is 90 parts;
a process for producing an insecticide composition comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 2 hours after grinding and stirring for 1 hour, then heating, grinding and stirring again for 2 hours, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2, wherein the primary stirring temperature in the step 2 is 75 ℃, and the secondary stirring temperature is 88 ℃;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.1 mu m, and controlling the shearing time to be 30min to obtain a liquid medicament;
5) cooling the liquid medicine obtained in the step 4 to room temperature, adding a regulator into the liquid medicine, stirring for 10-15min, and finally sieving to obtain a reaction composition, wherein in the step 5, the regulator is added until the liquid medicine is slightly acidic.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The pesticide composition is characterized by comprising the following raw materials in parts by weight: 3-7 parts of benzyl dimethyl phenol polyoxyethylene ether, 5-17 parts of abamectin, 2-17 parts of cyfluthrin, 5-7 parts of calcium dodecyl benzene sulfonate, 15-27 parts of tebufenozide, 30-55 parts of soybean oil, 5-15 parts of a penetrating agent, 5-15 parts of an organic solvent, 15-20 parts of an alkaloid, 5-15 parts of a thickening agent, 5-17 parts of an alcohol anti-freezing agent, 5-15 parts of a regulator, 5-10 parts of a wetting dispersant, 5-15 parts of an organic silicon defoamer, 15-25 parts of bentonite and 60-90 parts of water.
2. An insecticidal composition in accordance with claim 1 wherein said penetrant comprises at least one of dioctyl sodium sulfosuccinate and sodium di-sec-sulfosuccinate.
3. A pesticidal composition according to claim 1, wherein the organic solvent is one or more of benzene, toluene, kerosene and acetone; the alkaloid is one of derris and folium Artemisiae Argyi.
4. An insecticidal composition in accordance with claim 1 wherein said thickening agent is one of xanthan gum and magnesium aluminum silicate; the alcohol antifreeze agent is propylene glycol, and the regulator is one of plant ash or citric acid powder.
5. The insecticidal composition according to claim 1, wherein said wetting and dispersing agent is one or more selected from the group consisting of polyoxyethylene triphenylethylene phenyl phosphate, alkyl naphthalene sulfonate, alkylphenol polyoxyethylene and nonylphenol polyoxyethylene.
6. A process for the production of a pesticidal composition according to claim 1, comprising the steps of:
1) quantitatively weighing benzyl dimethylphenol polyoxyethylene ether, abamectin, cyfluthrin, calcium dodecylbenzene sulfonate, tebufenozide, alkaloid and bentonite, fully and uniformly mixing to obtain a mixture, simultaneously injecting a small amount of soybean oil and water into a sand mill, and then putting the mixture into the sand mill for grinding;
2) step 1, gradually adding a wetting dispersant, an organic solvent, a penetrating agent, a thickening agent, water and soybean oil into a sand mill, then continuously grinding and stirring, standing and preserving heat for 1-2h after grinding and stirring for 0.5-1h, then heating, grinding and stirring again for 1-2h, and finally standing and preserving heat;
3) gradually adding an organic silicon defoaming agent during primary grinding and stirring in the step 2, and gradually adding an alcohol antifreezing agent during secondary grinding and stirring in the step 2;
4) adding the medicament obtained in the step 2 into a shearing tank, injecting water into the shearing tank, opening the shearing tank, controlling the shearing particle size to be 0.02-0.1 mu m, and controlling the shearing time to be 25-30min to obtain a liquid medicament;
5) and (4) cooling the liquid medicine obtained in the step (4) to room temperature, adding a regulator into the liquid medicine, stirring for 10-15min, and finally sieving to obtain the reaction composition.
7. The process for producing an insecticidal composition according to claim 6, wherein the temperature of the primary stirring in step 2 is 60 to 75 ℃ and the temperature of the secondary stirring is 80 to 88 ℃.
8. The process for producing an insecticidal composition according to claim 6, wherein in step 5, the liquid medicine is slightly acidic by adding a regulator.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114766501A (en) * | 2022-04-27 | 2022-07-22 | 四川眉山凯尔化工有限公司 | Process for preparing multifunctional biological insecticide |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1075396A (en) * | 1992-12-31 | 1993-08-25 | 张友亮 | A kind of agricultural insecticide and production technology thereof |
| CN101642099A (en) * | 2009-08-31 | 2010-02-10 | 桂林集琦生化有限公司 | Pesticide suspension concentrate with organosilicon surfactant and preparation method thereof |
| CN102885057A (en) * | 2012-09-28 | 2013-01-23 | 王龙华 | Acitretin and pyridaben emulsion-in-water pesticide and production method thereof |
| CN103704247A (en) * | 2013-12-10 | 2014-04-09 | 济南凯因生物科技有限公司 | Cyhalothrin-containing water dispersible granule and application thereof |
| CN107593817A (en) * | 2017-09-30 | 2018-01-19 | 宿松县洲大现代农业发展有限公司 | A kind of Pesticidal combination containing cyfloxylate and AVM |
| CN107743968A (en) * | 2017-10-30 | 2018-03-02 | 广西壮族自治区农业科学院植物保护研究所 | A kind of high-efficiency low-toxicity kills ant bait formulation and preparation method thereof |
-
2021
- 2021-10-19 CN CN202111214954.9A patent/CN114081038A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1075396A (en) * | 1992-12-31 | 1993-08-25 | 张友亮 | A kind of agricultural insecticide and production technology thereof |
| CN101642099A (en) * | 2009-08-31 | 2010-02-10 | 桂林集琦生化有限公司 | Pesticide suspension concentrate with organosilicon surfactant and preparation method thereof |
| CN102885057A (en) * | 2012-09-28 | 2013-01-23 | 王龙华 | Acitretin and pyridaben emulsion-in-water pesticide and production method thereof |
| CN103704247A (en) * | 2013-12-10 | 2014-04-09 | 济南凯因生物科技有限公司 | Cyhalothrin-containing water dispersible granule and application thereof |
| CN107593817A (en) * | 2017-09-30 | 2018-01-19 | 宿松县洲大现代农业发展有限公司 | A kind of Pesticidal combination containing cyfloxylate and AVM |
| CN107743968A (en) * | 2017-10-30 | 2018-03-02 | 广西壮族自治区农业科学院植物保护研究所 | A kind of high-efficiency low-toxicity kills ant bait formulation and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114766501A (en) * | 2022-04-27 | 2022-07-22 | 四川眉山凯尔化工有限公司 | Process for preparing multifunctional biological insecticide |
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