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CN110907475A - A Remaining Life Evaluation Method of Martensitic Heat Resistant Steel - Google Patents

A Remaining Life Evaluation Method of Martensitic Heat Resistant Steel Download PDF

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CN110907475A
CN110907475A CN201910986910.4A CN201910986910A CN110907475A CN 110907475 A CN110907475 A CN 110907475A CN 201910986910 A CN201910986910 A CN 201910986910A CN 110907475 A CN110907475 A CN 110907475A
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resistant steel
martensitic
life
martensitic heat
loss rate
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张作贵
田根起
王峥
侍克献
赵双群
王延峰
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Shanghai Power Equipment Research Institute Co Ltd
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Abstract

本发明公开了一种马氏体耐热钢的剩余寿命评估方法。目前对在役锅炉材料的寿命预测常用到的检测手段，在检测可靠性和准确性方面存在不足。本发明首先设计一组马氏体耐热钢在实验室模拟服役过程中的温度和应力条件，获得不同试验条件下马氏体耐热钢试样的组织损伤特征参量与材料寿命损耗率之间的对应关系。对实际服役过程中马氏体耐热钢高温部件的组织损伤进行定量化分析，获得相应的特征参量值，代入该马氏体耐热钢的组织损伤参量与寿命损耗率的关系式，得出该服役马氏体耐热钢高温部件的寿命损耗率，并进一步计算出其剩余寿命。

Figure 201910986910

The invention discloses a residual life evaluation method of martensitic heat-resistant steel. At present, the commonly used detection methods for life prediction of in-service boiler materials are insufficient in detection reliability and accuracy. The invention first designs a group of temperature and stress conditions of martensitic heat-resistant steel in the laboratory simulation service process, and obtains the relationship between the characteristic parameters of microstructure damage and the material life loss rate of martensitic heat-resistant steel samples under different test conditions. Correspondence. Quantitatively analyze the microstructure damage of high-temperature components of martensitic heat-resistant steel in the actual service process, obtain the corresponding characteristic parameter values, and substitute the relationship between the microstructure damage parameter and the life loss rate of the martensitic heat-resistant steel to obtain The service life loss rate of martensitic heat-resistant steel high-temperature components, and further calculate its remaining life.

Figure 201910986910

Description

Method for evaluating residual life of martensite heat-resistant steel
Technical Field
The invention relates to a residual life evaluation method of martensite heat-resistant steel, in particular to a residual life evaluation method of a martensite heat-resistant steel high-temperature component based on tissue damage characteristic parameter analysis, and belongs to the field of thermal power generation equipment materials.
Background
The martensite heat-resistant steel has higher strength and hardness, and good high-temperature oxidation resistance and smoke corrosion resistance, and is widely applied to high-temperature component materials of thermal power generation equipment. In recent years, more than 1000 300MW subcritical boilers, more than 600-660 MW supercritical (super) boilers and more than 100 MW super supercritical (super) boilers have been put into operation in China in succession. However, in the long-term service process of the thermal power generating unit, the martensite heat-resistant steel and other high-temperature components are damaged by one or more factors such as creep, fatigue, corrosion and the like, and various changes can be generated on the structure. The failure of high-temperature components of the unit in the long-term operation process is one of the main factors influencing the safe and economic operation of the power plant, and whether the high-temperature components are safely and stably operated or not directly relates to the safety of the whole power plant. Therefore, the service life of the thermal power generating unit is managed in advance according to the tissue damage state of the material by analyzing the tissue damage degree of the martensite heat-resistant steel boiler pipeline and other power station high-temperature component materials in the long-term service process, and the method has very important significance for ensuring the safe operation of the thermal power generating unit.
At present, detection means commonly used for predicting the service life of the in-service power generation equipment material are generally based on means such as hardness, room temperature and high temperature tensile property detection, oxide scale detection and the like, and have certain defects in the aspects of detection reliability and accuracy.
Disclosure of Invention
The invention aims to provide a more accurate and effective method for evaluating the residual life of a martensite heat-resistant steel high-temperature component based on tissue damage characteristic parameter analysis.
In order to solve the technical problems, the technical scheme of the invention provides a method for evaluating the residual life of martensite heat-resistant steel, which is mainly characterized in that according to the corresponding trend relation between the width of a martensite lath of a martensite heat-resistant steel sample and the material life loss rate obtained by analysis under a Transmission Electron Microscope (TEM), the residual life of the service high-temperature component is calculated by micro-damage sampling of the martensite heat-resistant steel high-temperature component in the service process and the tissue damage characteristic parameter analysis of the sample.
The method comprises the following specific steps:
carrying out endurance tests on the martensite heat-resistant steel sample under different working conditions, and sampling at different time under different working conditions;
calculating the service life loss rate of the martensite heat-resistant steel according to the test data;
measuring the sampling, and measuring the average width of the martensite lath as a tissue damage characteristic parameter;
establishing a corresponding trend relation between the tissue damage characteristic parameters and the life loss rate;
locally sampling the martensite heat-resistant steel in service, measuring the width of the locally sampled martensite lath, and calculating the residual life according to the corresponding relation between the tissue damage characteristic parameter and the life loss rate.
The endurance test is a 5-grade stress endurance test of a martensite heat-resistant steel sample at a service temperature under a laboratory condition, and the longest test time is 3.3 ten thousand hours; at each stress, the test was stopped for test times of 3000 hours, 5000 hours, 10000 hours and 20000 hours, respectively, and intermediate sampling was performed.
Establishing a life loss rate model: the corresponding permanent fracture time of the sample under the same temperature and stress conditions (i.e. the actual life of the sample under the temperature and stress) is defined as taIf the actual endurance test time is t, the actual life loss rate corresponding to the test time t is m ═ t/ta. According to the above definition, for the original state sample, t is 0, and the life loss rate is 0; for a permanent fracture specimen, t ═ taThe life loss rate at the time of breakage of the specimen was 1.
Obtaining tissue damage characteristic parameters: according to the original state test sample and the martensite heat-resistant steel test samples under different stresses and test time, the martensite structure morphology in the test sample is observed under a Transmission Electron Microscope (TEM), and a TEM morphology photograph of 10 martensite lath structures is taken under a magnification of 10 k. And directly measuring the width of each martensite lath in each picture under related image processing software, and averaging the width measurement values of all the martensite laths to obtain the width of the martensite lath under the corresponding test condition of the sample.
Establishing a corresponding relation between the tissue damage characteristic parameters and the material life loss rate: and according to the obtained width values of the martensite laths in the samples under different test conditions, the service life loss rate of the samples is taken as an abscissa and the width value of the martensite laths is taken as an ordinate, and the corresponding trend relation of the width of the martensite laths along with the service life loss rate is obtained, so that a service life loss model of the martensite heat-resistant steel samples in the endurance test process is established.
Calculating the residual life: obtaining long-term service t by adopting a structure analysis means according to a service life loss model of a martensite heat-resistant steel sample in a endurance test processsThe width of the martensite lath of the martensite heat-resistant steel after the time is partially sampled, the corresponding service life loss rate m is determined according to the width of the martensite lath, and the actual service time is tsThen, the remaining life tr＝ts/m-ts。
According to the method for evaluating the residual life of the martensite heat-resistant steel, the structure damage comprises the change of the internal structure of the material under the comprehensive action of temperature, stress and time.
The method for evaluating the residual life of the martensite heat-resistant steel is suitable for thermal power generating units which run for a long time and heat-resistant steel high-temperature parts with martensite structures, such as various boiler pipelines and the like.
The method can be used for accurately calculating the residual service life of the martensite heat-resistant steel high-temperature component of the thermal generator set after long-term operation, and provides more accurate basis for the safe operation and service life management of the thermal generator set.
The invention has the following beneficial effects:
the method tracks the change of the service life of the material through the change of the tissue damage characteristic parameters, and has the advantage of easy quantification.
The method calculates the residual service life of the high-temperature component of the service unit by establishing the corresponding trend relation between the material tissue damage characteristic parameter and the service life loss rate, and has the advantage of intuition.
The invention is suitable for martensite heat-resistant steel high-temperature components of thermal generator sets with various parameters.
Drawings
FIG. 1 is a graph showing the relationship between the width of martensite laths in the martensitic heat-resistant steel T91 boiler tube and the life loss rate of the material;
wherein the abscissa is the life loss rate and the ordinate is the width of the martensite lath.
Detailed Description
In order to make the invention more comprehensible, preferred embodiments are described in detail below with reference to the accompanying drawings.
Examples
The method takes a Transmission Electron Microscope (TEM) as a detection means, and carries out quantitative analysis on the tissue damage characteristic parameters of samples from different tissue damage states to a material life termination (fracture) state, so as to establish the corresponding relation between the width of a martensite lath of the martensite heat-resistant steel material and the life loss rate of the sample. And obtaining the width of the martensite lath of the martensite heat-resistant steel T91 boiler pipeline in the service state by sampling the micro-loss of the martensite heat-resistant steel T91 boiler pipeline in the long-term service process, obtaining the service life loss rate of the martensite heat-resistant steel T91 boiler pipeline according to the corresponding trend relationship, and calculating the residual service life of the martensite heat-resistant steel T91 boiler pipeline of the service unit.
The method comprises the following specific steps:
1) carrying out high-temperature endurance tests at service temperature and under different stress conditions under laboratory conditions;
2) carrying out quantitative analysis on tissue damage characteristic parameters on samples in different tissue damage states until the material service life is stopped (broken) by adopting a Transmission Electron Microscope (TEM);
3) establishing a corresponding relation between the width of a martensite lath and the service life loss rate of a martensite heat-resistant steel T91 boiler tube sample;
4) sampling the micro-loss of the boiler pipeline T91 in the service process to obtain the width of the martensite lath of the martensite heat-resistant steel in the state;
5) and calculating the residual service life of the martensite heat-resistant steel T91 boiler pipeline of the service unit according to the corresponding trend relation between the tissue damage parameter and the service life loss rate obtained under the laboratory condition.
According to the steps, the martensite refractory steel T91 boiler pipe local micro-loss sampling during the field service process is adopted in the embodiment, and the martensite lath width value inside the T91 boiler pipe sample is analyzed. And obtaining the service life loss rate of the T91 boiler pipeline made of the service heat-resistant steel according to the corresponding relation between the structure damage characteristic parameters of the corresponding martensite heat-resistant steel T91 material and the service life loss rate of the material, and further calculating the residual service life of the T91 boiler pipeline.
A T91 reheater pipeline of a certain thermal generator set which is in service for 12 ten thousand hours for a long time is sampled, the tissue damage state of the martensite heat-resistant steel T91 pipe sample after 12 ten thousand hours of long-term service is observed and measured through a Transmission Electron Microscope (TEM), and the width of a martensite lath, namely the tissue damage characteristic parameter is 520 nm. According to the relation between the width of martensite laths in the martensite heat-resistant steel T91 boiler tube and the service life loss rate of a sample, the service life loss rate m of the T91 boiler tube after 12 ten thousand hours of long-term service is obtained to be 0.48, and the residual service life T of the T91 reheater tube in service can be calculatedrIs 13 ten thousand hours.

Claims (6)

1.一种马氏体耐热钢的剩余寿命评估方法，其步骤为：1. A method for evaluating residual life of martensitic heat-resistant steel, the steps of which are: 对马氏体耐热钢试样进行不同工况下的持久性能试验，在不同工况下不同时间进行取样；The endurance performance test under different working conditions is carried out on the martensitic heat-resistant steel samples, and the samples are taken at different times under different working conditions; 根据试验数据计算马氏体耐热钢的寿命损耗率；Calculate the life loss rate of martensitic heat-resistant steel according to the test data; 对取样进行组织分析，测量马氏体板条的平均宽度作为组织损伤特征参量；Microstructure analysis was performed on the samples, and the average width of the martensitic lath was measured as the characteristic parameter of tissue damage; 建立组织损伤特征参量与寿命损耗率的对应关系；Establish the corresponding relationship between tissue damage characteristic parameters and life loss rate; 对服役的马氏体耐热钢局部取样，测量局部取样的马氏体板条宽度，根据组织损伤特征参量与寿命损耗率的对应关系计算剩余寿命。The martensitic heat-resistant steel in service is sampled locally, the width of the locally sampled martensitic lath is measured, and the remaining life is calculated according to the corresponding relationship between the characteristic parameters of tissue damage and the life loss rate. 2.如权利要求1所述的一种马氏体耐热钢的剩余寿命评估方法，其特征在于，所述的持久性能试验为马氏体耐热钢试样在服役温度下5档应力的持久性能试验，最长试验时间为3.3万小时；每一应力下，分别在试验时间达到3000小时、5000小时、10000小时和20000小时进行中间取样。2. the residual life evaluation method of a kind of martensitic heat-resistant steel as claimed in claim 1, is characterized in that, described lasting performance test is martensitic heat-resistant steel sample under the service temperature of 5 files of stress. For the endurance performance test, the longest test time is 33,000 hours; under each stress, intermediate sampling is performed when the test time reaches 3,000 hours, 5,000 hours, 10,000 hours and 20,000 hours. 3.如权利要求1所述的一种马氏体耐热钢的剩余寿命评估方法，其特征在于，所述的寿命损耗率为m，在某一试验条件下试样持久断裂时间为ta，实际持久试验时间为t，m＝t/ta。3. the residual life evaluation method of a kind of martensitic heat-resistant steel as claimed in claim 1, is characterized in that, described life loss rate is m, and under certain test condition, the permanent fracture time of sample is t a , the actual durable test time is t, m=t/t a . 4.如权利要求3所述的一种马氏体耐热钢的剩余寿命评估方法，其特征在于，所述的剩余寿命为tr，根据服役锅炉管道的局部取样的马氏体板条宽度确定对应的寿命损耗率m，服役锅炉管道的实际服役时间为ts，则剩余寿命tr＝ts/m-ts。4. The residual life evaluation method of a martensitic heat-resistant steel as claimed in claim 3, wherein the residual life is tr , according to the martensitic lath width of the local sampling of the service boiler pipeline Determine the corresponding life loss rate m, and the actual service time of the boiler pipes in service is ts , then the remaining life t r = ts /mts . 5.如权利要求1所述的一种马氏体耐热钢的剩余寿命评估方法，其特征在于，所述的测量马氏体板条的平均宽度为通过透射电子显微镜观察取样内部的马氏体组织形貌，在10k倍率下拍摄至少10张马氏体板条的形貌照片，通过图像处理测量每张图片中每条马氏体板条的宽度，并将所有测量值取平均值。5. The method for evaluating the remaining life of a martensitic heat-resistant steel according to claim 1, wherein the measured average width of the martensitic lath is to observe the martensite inside the sampling through a transmission electron microscope To determine the morphology of the body structure, take at least 10 pictures of the morphology of the martensitic lath at a magnification of 10k, measure the width of each martensitic lath in each picture through image processing, and take the average of all the measured values. 6.如权利要求1所述的一种马氏体耐热钢的剩余寿命评估方法，其特征在于，所述的组织损伤特征参量用于评估组织损伤，组织损伤包括温度、应力、时间综合作用下的材料内部组织变化。6. The method for evaluating the remaining life of a martensitic heat-resistant steel according to claim 1, wherein the tissue damage characteristic parameter is used to evaluate tissue damage, and the tissue damage includes the comprehensive effect of temperature, stress and time. Changes in the internal organization of the material.
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CN112525907A (en) * 2020-11-23 2021-03-19 华能国际电力股份有限公司 Method for evaluating residual creep life of high-temperature static component material of gas turbine in service
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CN113203760A (en) * 2021-04-19 2021-08-03 上海发电设备成套设计研究院有限责任公司 Austenitic steel service life evaluation method based on electron back scattering diffraction
TWI820563B (en) * 2022-01-05 2023-11-01 台灣電力股份有限公司 Method of predicting material life

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