CN108424814A - A kind of preparation method of matrimony vine essence and the application in cigarette - Google Patents
A kind of preparation method of matrimony vine essence and the application in cigarette Download PDFInfo
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- CN108424814A CN108424814A CN201810229949.7A CN201810229949A CN108424814A CN 108424814 A CN108424814 A CN 108424814A CN 201810229949 A CN201810229949 A CN 201810229949A CN 108424814 A CN108424814 A CN 108424814A
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- matrimony vine
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- 235000015459 Lycium barbarum Nutrition 0.000 title claims abstract description 81
- 244000241838 Lycium barbarum Species 0.000 title claims abstract description 80
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 241000208125 Nicotiana Species 0.000 claims abstract description 47
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 47
- 238000006243 chemical reaction Methods 0.000 claims abstract description 42
- 108090000790 Enzymes Proteins 0.000 claims abstract description 26
- 102000004190 Enzymes Human genes 0.000 claims abstract description 26
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000012141 concentrate Substances 0.000 claims abstract description 16
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 claims abstract description 8
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000796 flavoring agent Substances 0.000 claims abstract description 7
- 235000019634 flavors Nutrition 0.000 claims abstract description 5
- 229940088598 enzyme Drugs 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 18
- 238000010992 reflux Methods 0.000 claims description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 11
- 238000000926 separation method Methods 0.000 claims description 11
- 239000000243 solution Substances 0.000 claims description 10
- 238000010790 dilution Methods 0.000 claims description 7
- 239000012895 dilution Substances 0.000 claims description 7
- 108010059892 Cellulase Proteins 0.000 claims description 6
- 229940106157 cellulase Drugs 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 6
- 230000002779 inactivation Effects 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 230000015556 catabolic process Effects 0.000 claims description 4
- 238000006731 degradation reaction Methods 0.000 claims description 4
- 235000002710 Ilex cornuta Nutrition 0.000 claims description 3
- 241001310146 Ilex cornuta Species 0.000 claims description 3
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 claims description 3
- 102000004169 proteins and genes Human genes 0.000 claims description 3
- 108090000623 proteins and genes Proteins 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 230000007935 neutral effect Effects 0.000 claims description 2
- 239000006228 supernatant Substances 0.000 claims description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 6
- 239000003546 flue gas Substances 0.000 abstract description 6
- 239000003205 fragrance Substances 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 210000001124 body fluid Anatomy 0.000 abstract description 3
- 239000010839 body fluid Substances 0.000 abstract description 3
- 235000013355 food flavoring agent Nutrition 0.000 abstract description 2
- 230000001737 promoting effect Effects 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 238000005119 centrifugation Methods 0.000 abstract 1
- 230000002787 reinforcement Effects 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 description 11
- 230000000694 effects Effects 0.000 description 6
- 101000693530 Staphylococcus aureus Staphylokinase Proteins 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- 150000004676 glycans Chemical class 0.000 description 4
- 239000007791 liquid phase Substances 0.000 description 4
- 229920001282 polysaccharide Polymers 0.000 description 4
- 239000005017 polysaccharide Substances 0.000 description 4
- 244000241872 Lycium chinense Species 0.000 description 3
- 235000015468 Lycium chinense Nutrition 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 235000013334 alcoholic beverage Nutrition 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 240000000950 Hippophae rhamnoides Species 0.000 description 1
- 235000003145 Hippophae rhamnoides Nutrition 0.000 description 1
- 241000208292 Solanaceae Species 0.000 description 1
- 239000007853 buffer solution Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to tobacco chemistry and essence and flavoring agent technical fields, and in particular to a kind of preparation method of matrimony vine essence and the application in cigarette；Tobacco leaf is not suitable for using the matrimony vine clout after the use of matrimony vine brewery with tobacco enterprise to mix in proportion as raw material, a certain amount of complex enzyme is added to degrade, suitable phenylalanine is added later carries out Maillard reaction, with 90% alcohol steep, centrifugation after the reaction was complete, it is concentrated to give matrimony vine essence concentrate with revolving instrument again, is finally configured to corresponding cigarette matrimony vine essence in proportion；Gained cigarette can be obviously improved flue gas concentration with matrimony vine flavor application in cigarette, when smokeing panel test flue gas texture it is mellow and full, it is fine and smooth it is graceful, increase sense of promoting the production of body fluid, fragrance main line is clear, style reinforcement.
Description
Technical field
The invention belongs to tobacco chemistry and essence and flavoring agent technical fields, and in particular to a kind of preparation method of matrimony vine essence and
Application in cigarette.
Background technology
Matrimony vine, the also known as fruit of Chinese wolfberry are the ripening fruits of Solanaceae undershrub matrimony vine.Matrimony vine is the rare Chinese medicine having won fame both at home and abroad
Material is widely used in food, drug, health products, China is since ancient times rich in active ingredients such as a variety of sugar, amino acid
The custom that useful matrimony vine is steep in wine.Currently, the industry manufacture of annual Lycium chinense wine will consume a large amount of matrimony vines, and matrimony vine generates after brewing alcoholic beverages
A large amount of clouts in still contain the active ingredients such as a large amount of polysaccharides, protein, cellulose and can utilize.
China Patent No. CN201610368578.1 discloses a kind of sea-buckthorn, fig, wolfberry fruit extract etc. and is uniformly mixed system
The tobacco aromaticss of standby sweet flue gas are applied to the method for cigarette.Patent No. CN200910189842.5 discloses one kind and containing Chinese holly
The technical issues of cigarette and preparation method thereof of Qi polysaccharide, solution, is the increase in cigarette flavor, enhancing flue gas promotes the production of body fluid sense.Existing skill
There are open polysaccharides and its method for extraction and purification in art, there is good physics and sense organ humectation effect to cigarette, as one
The tobacco humectant of kind function admirable is applied in cigarette.And it there are no prepare flavouring essence for tobacco using matrimony vine clout in the prior art
The technology of fragrance.
Invention content
The present invention is that will produce a large amount of clouts and the not applicable tobacco leaf of tobacco enterprise after solution matrimony vine brews alcoholic beverages not utilizing,
The problem of leading to the wasting of resources, provides a kind of preparation side of the matrimony vine essence using matrimony vine clout and not applicable tobacco leaf for raw material
Method.
In order to solve the above technical problems, the technical solution adopted in the present invention is：A kind of preparation method of matrimony vine essence,
It is characterized in that, includes the following steps：
1）The discarded matrimony vine clout of matrimony vine brewery is not suitable for after tobacco leaf mixes with tobacco enterprise and carries out complex enzyme degradation：By discarded Chinese holly
Qi clout is not suitable for after tobacco leaf mixes with tobacco enterprise and distilled water, solid-to-liquid ratio 1 is added:5~1:10, it is heated to reflux 20 ~ 40 points
Clock；Then cooling control temperature presses 1 to 35 ~ 45 DEG C:2:Cellulase, glucuroide, neutral protein is added portionwise in 1 ratio
Enzyme carries out enzymolysis 24 hours, wherein the total amount of adding of three kinds of enzymes accounts for the 5- that matrimony vine clout mixes total weight with not applicable tobacco leaf
10‰；
2）Mixture carries out Maillard reaction after enzymolysis：Mixture after complex enzyme zymohydrolysis is heated to reflux inactivation, adds into system
2% phenylalanine for entering total weight of the mixture, it is 5.8-6.2 to adjust reaction system PH with citric acid solution, is heated to reflux
Carry out Maillard reaction 24 hours；
3）The extraction and concentration of effective flavor component：By system after the completion of Maillard reaction through alcohol steep, separation is concentrated to give
Matrimony vine essence concentrate；
4）By step 3）The matrimony vine essence concentrate of gained obtains matrimony vine essence with 0.01% ~ 0.1% dilution proportion.
Phenylalanine best results are added in step 2, other amino acid aroma-increasings are not obvious, and pH value of reaction system control exists
5.8-6.2, reaction rate and best results, flavouring effect are more excellent.
Preferably, step 1）In to discard matrimony vine clout and tobacco enterprise to be not suitable for the mixed proportion of tobacco leaf be 1:4~1:6.
Matrimony vine clout and not applicable tobacco leaf are with 1 in step 1:4~1:6 mixed effects are more excellent, and hydrolysis temperature should control 35 ~
Best enzymatic activity can be reached between 45 DEG C, enzymolysis time is advisable for 24 hours, and the time, short degradation was not complete enough, and extended the time again
It is not notable to final products influential effect.
Preferably, step 3）In extracting and developing condition be：System is added in equal volume after the completion of to Maillard reaction
90% ethanol solution is cooled to room temperature extraction 48 hours；Centrifuge 2000rmp is centrifuged 15 minutes, and supernatant is in Rotary Evaporators
It is concentrated under reduced pressure to give matrimony vine essence concentrate.
90% ethyl alcohol can reach higher extraction rate in step 3, improve concentration of alcohol, and fragrance can increased and moisture feeling
Declined.Centrifuge speed, which reaches 2000rpm, can reach preferable solid-liquid separation effect.
The proportioning and diluted concentration of matrimony vine essence concentrate can be suitably allocated according to different demands.
It is another object of the present invention to by the matrimony vine flavor application prepared by above-mentioned preparation method in cigarette.
Compared with prior art the invention has the advantages that：
The present invention takes full advantage of the active ingredients such as remaining polysaccharide, amino acid, cellulose and not applicable cigarette in matrimony vine clout
Through complex enzyme degradation after leaf mixing, adds amino acid and carry out Maillard reaction, obtained concentration essence is by 0.01%-0.1%'s
Dilution proportion obtains matrimony vine flavouring essence for tobacco, mellow and full, fine and smooth refined applied to that can be obviously improved flue gas concentration, flue gas texture in cigarette
It causes, increase sense of promoting the production of body fluid, fragrance main line is clear, style is reinforced.The matrimony vine clout that brewery discards is not suitable for tobacco enterprise simultaneously
Tobacco leaf has carried out development and reuse, and obtained cigarette has very with matrimony vine essence in terms of improving cigarette concentration, fragrance and satisfaction
Good effect has positive contribution for enterprise's cost efficiency.
Specific implementation mode
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
A kind of preparation method of matrimony vine essence, step are：
1）Matrimony vine clout is mixed with not applicable tobacco leaf, is digested using complex enzyme.Reaction condition is：Matrimony vine clout with it is not applicable
Tobacco leaf presses 1:4 ratios mix, and are added in distilled water, solid-to-liquid ratio 1:6, it is heated to reflux 30 minutes；Cooling control temperature to 40 DEG C,
1 is pressed in batches:2:Cellulase is added in 1 ratio, and the complex enzyme of glucuroide, neutral proteinase carries out enzymolysis 24 hours, wherein
The total amount of adding of three kinds of enzymes accounts for matrimony vine clout and mixes the 5 ‰ of total weight with not applicable tobacco leaf；
2）Mixture after complex enzyme zymohydrolysis is heated to reflux inactivation, and carries out Maillard reaction.Reaction condition is：It is added in system
2% phenylalanine of total weight of the mixture adjusts reaction system PH to 5.8 with citric acid solution, it is beautiful to be heated to reflux progress
Maillard reaction 24 hours；
3）System is concentrated to give corresponding extract through alcohol steep, separation after the completion of Maillard reaction.Extract separation condition：
Isometric 90% ethyl alcohol is added in reaction system, is cooled to room temperature extraction 48 hours；Centrifuge 2000 leaves the heart 15 minutes, collection liquid
Phase is concentrated to give matrimony vine essence concentrate for 45 DEG C on a rotary evaporator；
4) configuration of cigarette matrimony vine essence：Matrimony vine essence concentrate obtains matrimony vine flavouring essence for tobacco feed liquid with 0.1% dilution proportion.
Example 2
A kind of preparation method of matrimony vine essence, step are：
1）Matrimony vine clout is mixed with not applicable tobacco leaf, is digested using complex enzyme.Reaction condition is：Matrimony vine clout with it is not applicable
Tobacco leaf presses 1:5 ratios mix, and are added in distilled water, solid-to-liquid ratio 1:7, it is heated to reflux 20 minutes；Cooling control temperature to 35 DEG C,
1 is pressed in batches:2:Cellulase is added in 1 ratio, and the complex enzyme of glucuroide, neutral proteinase carries out enzymolysis 24 hours, wherein
The total amount of adding of three kinds of enzymes accounts for matrimony vine clout and mixes the 10 ‰ of total weight with not applicable tobacco leaf；
2）Mixture after complex enzyme zymohydrolysis is heated to reflux inactivation, and carries out Maillard reaction.Reaction condition is：It is added in system
2% phenylalanine of total weight of the mixture adjusts reaction system PH to 6.2 with citric acid solution, it is beautiful to be heated to reflux progress
Maillard reaction 24 hours；
3）System is concentrated to give corresponding medicinal extract through alcohol steep, separation after the completion of Maillard reaction.Extract separation condition：Instead
It answers system that isometric absolute ethyl alcohol is added, is cooled to room temperature extraction 48 hours；Centrifuge 2000 leaves the heart 15 minutes, collects liquid phase
It is concentrated to give matrimony vine essence concentrate for 45 DEG C on a rotary evaporator；
4）The configuration of matrimony vine flavouring essence for tobacco：Matrimony vine essence concentrate obtains matrimony vine flavouring essence for tobacco feed liquid with 0.01% dilution proportion.
Example 3
A kind of preparation method of matrimony vine essence, step are：
1）Matrimony vine clout is mixed with not applicable tobacco leaf, is digested using complex enzyme.Reaction condition is：Matrimony vine clout with it is not applicable
Tobacco leaf presses 1:5 ratios mix, and are added in distilled water, solid-to-liquid ratio 1:6, it is heated to reflux 40 minutes；Cooling control temperature to 45 DEG C,
1 is pressed in batches:2:Cellulase is added in 1 ratio, and the complex enzyme of glucuroide, neutral proteinase carries out enzymolysis 24 hours, wherein
The total amount of adding of three kinds of enzymes accounts for matrimony vine clout and mixes the 7 ‰ of total weight with not applicable tobacco leaf；
2）Mixture after complex enzyme zymohydrolysis is heated to reflux inactivation, and carries out Maillard reaction.Reaction condition is：It is added in system
2% phenylalanine of total weight of the mixture adjusts reaction system PH to 6 with buffer solution, is heated to reflux carry out Maillard reaction
24 hours；
3）System is concentrated to give corresponding extract through alcohol steep, separation after the completion of Maillard reaction.Extract separation condition：
Isometric 90% ethyl alcohol is added in reaction system, is cooled to room temperature extraction 48 hours；Centrifuge 2000 leaves the heart 15 minutes, collection liquid
Phase is concentrated to give matrimony vine essence concentrate for 45 DEG C on a rotary evaporator；
4）The configuration of matrimony vine flavouring essence for tobacco：Matrimony vine essence concentrate obtains matrimony vine flavouring essence for tobacco feed liquid with 0.08% dilution proportion.
Example 4
A kind of preparation method of matrimony vine essence, step are：
1）Matrimony vine clout is mixed with not applicable tobacco leaf, is digested using complex enzyme.Reaction condition is：Matrimony vine clout with it is not applicable
Tobacco leaf presses 1:6 ratios mix, and are added in distilled water, solid-to-liquid ratio 1:5, it is heated to reflux 30 minutes；Cooling control temperature to 37 DEG C,
1 is pressed in batches:2:Cellulase is added in 1 ratio, and the complex enzyme of glucuroide, neutral proteinase carries out enzymolysis 24 hours, wherein
The total amount of adding of three kinds of enzymes accounts for matrimony vine clout and mixes the 8 ‰ of total weight with not applicable tobacco leaf；
2）Mixture after complex enzyme zymohydrolysis is heated to reflux inactivation, and carries out Maillard reaction.Reaction condition is：It is added in system
2% phenylalanine of total weight of the mixture, with citric acid solution adjust reaction system PH to 6.0 or so, be heated to reflux into
Row Maillard reaction 24 hours；
3）System is concentrated to give corresponding extract through alcohol steep, separation after the completion of Maillard reaction.Extract separation condition：
Isometric 90% ethyl alcohol is added in reaction system, is cooled to room temperature extraction 48 hours；Centrifuge 2000 leaves the heart 15 minutes, collection liquid
Phase is concentrated to give matrimony vine essence concentrate for 45 DEG C on a rotary evaporator；
4）The configuration of matrimony vine flavouring essence for tobacco：Matrimony vine essence concentrate obtains matrimony vine flavouring essence for tobacco feed liquid with 0.05% dilution proportion.
Claims (4)
1. a kind of preparation method of matrimony vine essence, which is characterized in that include the following steps：
1）The discarded matrimony vine clout of matrimony vine brewery is not suitable for after tobacco leaf mixes with tobacco enterprise and carries out complex enzyme degradation：By discarded Chinese holly
Qi clout is not suitable for after tobacco leaf mixes with tobacco enterprise and distilled water, solid-to-liquid ratio 1 is added:5~1:10, it is heated to reflux 20 ~ 40 points
Clock；Then cooling control temperature presses 1 to 35 ~ 45 DEG C:2:Cellulase, glucuroide, neutral protein is added portionwise in 1 ratio
Enzyme carries out enzymolysis 24 hours, wherein the total amount of adding of three kinds of enzymes accounts for the 5- that matrimony vine clout mixes total weight with not applicable tobacco leaf
10‰；
2）Mixture carries out Maillard reaction after enzymolysis：Mixture after complex enzyme zymohydrolysis is heated to reflux inactivation, adds into system
2% phenylalanine for entering total weight of the mixture, it is 5.8-6.2 to adjust reaction system PH with citric acid solution, is heated to reflux
Carry out Maillard reaction 24 hours；
3）The extraction and concentration of effective flavor component：By system after the completion of Maillard reaction through alcohol steep, separation is concentrated to give
Matrimony vine essence concentrate；
4）By step 3）The matrimony vine essence concentrate of gained obtains matrimony vine essence with 0.01% ~ 0.1% dilution proportion.
2. a kind of preparation method of matrimony vine essence according to claim 1, which is characterized in that step 1）In discard matrimony vine more than
The mixed proportion that material is not suitable for tobacco leaf with tobacco enterprise is 1:4~1:6.
3. a kind of preparation method of matrimony vine essence according to claim 1, which is characterized in that step 3）In extraction, point
It is from condition：90% isometric ethanol solution is added in system after the completion of to Maillard reaction, is cooled to room temperature extraction 48 hours；
Centrifuge 2000rmp is centrifuged 15 minutes, and supernatant is concentrated under reduced pressure to give matrimony vine essence concentrate in Rotary Evaporators.
4. the matrimony vine essence prepared by a kind of preparation method of matrimony vine essence as described in claim 1-3 Arbitrary Terms is in cigarette
Application.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111374345A (en) * | 2018-12-29 | 2020-07-07 | 贵州中烟工业有限责任公司 | Method for preparing Maillard reaction product by using Lycium barbarum extract, Maillard reaction product and application |
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