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CN107782696B - Sensing system and method for measuring the refractive index of distributed liquid using a taper fiber - Google Patents

Sensing system and method for measuring the refractive index of distributed liquid using a taper fiber Download PDF

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CN107782696B
CN107782696B CN201710860221.XA CN201710860221A CN107782696B CN 107782696 B CN107782696 B CN 107782696B CN 201710860221 A CN201710860221 A CN 201710860221A CN 107782696 B CN107782696 B CN 107782696B
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refractive index
fiber
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optical fiber
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CN107782696A (en
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丁振扬
刘铁根
刘琨
江俊峰
杨迪
孙可亮
于哲
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Tianjin University
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Abstract

A sensing system and a method for measuring a distributed liquid refractive index by using a tapered optical fiber relate to the technical field of optical fiber sensing, refractive index sensing is carried out based on back Rayleigh scattering intermode interference generated in a tapered area of the tapered optical fiber, and the effective mode refractive index of back Rayleigh scattering propagation in the tapered optical fiber is changed by sensing the change of an external refractive index through stronger evanescent waves generated in the tapered area; and placing the tapered optical fiber in liquid, detecting the wavelength shift of Rayleigh scattering spectrum of the tapered optical fiber through a distributed optical fiber sensing device, analyzing the wavelength shift, and obtaining the continuously distributed refractive index distribution condition of the liquid. The refractive index measurement of the distributed liquid with high spatial resolution reaching millimeter level is realized.

Description

利用拉锥光纤测量分布式液体折射率的传感系统及方法Sensing system and method for measuring the refractive index of distributed liquid using a taper fiber

技术领域technical field

本发明涉及光纤传感技术领域,尤其涉及一种利用拉锥光纤测量分布式液体折射率的传感系统及方法,应用于光频域反射。The invention relates to the technical field of optical fiber sensing, in particular to a sensing system and method for measuring the refractive index of distributed liquid by using a tapered optical fiber, which is applied to optical frequency domain reflection.

背景技术Background technique

物质折射率是反映物质内部信息的一个重要物理量。物质折射率的测量在基础研究、化学分析、环境污染评估、医疗诊断和食品工业等领域有着广泛的应用。The refractive index of a substance is an important physical quantity that reflects the internal information of a substance. The measurement of the refractive index of substances has a wide range of applications in basic research, chemical analysis, environmental pollution assessment, medical diagnosis, and the food industry.

光纤折射率传感器具有传感器本质绝缘、抗电磁干扰、高灵敏度、高精度、集成度高、高带宽、可复用等特征成为折射率传感器研究热点。传统光纤折射率传感器有布拉格光纤光栅、长周期光栅、微弯光纤、光子晶体光纤、光纤表面等离子共振、F-P传感器、在线MZ传感器、微球、微环振荡器、以及单模多模光纤串接等结构。Optical fiber refractive index sensors have the characteristics of intrinsic insulation, anti-electromagnetic interference, high sensitivity, high precision, high integration, high bandwidth, and reusability, which have become the research hotspot of refractive index sensors. Traditional fiber optic refractive index sensors include fiber Bragg gratings, long period gratings, microbend fibers, photonic crystal fibers, fiber surface plasmon resonance, F-P sensors, online MZ sensors, microspheres, microring oscillators, and single-mode multi-mode fiber tandem etc. structure.

上述的传统光纤折射率传感器一般采用宽带光源和光谱仪解调或可调谐激光器扫描探测,利用透射光方式,只能进行单点传感,为分立式传感,无法准确测量在一定长度上的折射率分布。The above-mentioned traditional optical fiber refractive index sensors generally use broadband light source and spectrometer demodulation or tunable laser scanning detection. Using transmitted light method, only single-point sensing can be performed, which is a discrete sensing, and cannot accurately measure a certain length. Refractive index distribution.

目前迫切需要一种光纤折射率传感器可实现沿光纤上分布式折射率传感,在光纤一定长度上任何一点都是敏感点,实现多点连续传感。At present, there is an urgent need for an optical fiber refractive index sensor that can realize distributed refractive index sensing along the optical fiber. Any point on a certain length of the optical fiber is a sensitive point to realize multi-point continuous sensing.

发明内容SUMMARY OF THE INVENTION

本发明提供了一种利用拉锥光纤测量分布式液体折射率的传感系统及方法,本发明实现了高空间分辨率达到mm(毫米)级的分布式液体折射率测量,可成功应用于密集的液体折射率分布式测量、监测液体扩散,以及液层精确定位等场合,详见下文描述:The invention provides a sensing system and method for measuring the refractive index of distributed liquid by using a tapered optical fiber. The invention realizes the measurement of the refractive index of distributed liquid with high spatial resolution reaching mm (millimeter) level, and can be successfully applied to dense For distributed measurement of liquid refractive index, monitoring liquid diffusion, and precise positioning of liquid layers, please refer to the following descriptions:

一种利用拉锥光纤测量分布式液体折射率的传感系统,所述传感系统包括:光频域反射的分布式光纤传感装置,所述传感系统用于实现高空间分辨率达到毫米级的分布式液体折射率测量;A sensing system for measuring the refractive index of distributed liquid by using a tapered optical fiber, the sensing system comprises: a distributed optical fiber sensing device of optical frequency domain reflection, and the sensing system is used to achieve high spatial resolution up to millimeters Distributed Refractive Index Measurement of Levels of Liquids;

所述传感系统包括:拉锥光纤,The sensing system includes: a tapered optical fiber,

基于所述拉锥光纤的锥形区域部分发生的背向瑞利散射模间干涉,进行折射率传感,通过锥形区域产生的较强倏逝波感知外界折射率的变化,改变所述拉锥光纤内背向瑞利散射传播的有效模式折射率;Based on the interference between the back Rayleigh scattering modes in the tapered region of the tapered fiber, the refractive index sensing is performed, and the change of the external refractive index is sensed by the strong evanescent wave generated in the tapered region, and the change of the tapered fiber is changed. The effective mode index of back-Rayleigh scattering propagation in the tapered fiber;

将所述拉锥光纤置于液体中,通过所述分布式光纤传感装置,检测所述拉锥光纤的瑞利散射光谱的波长移动,分析所述波长移动,获取液体连续分布式的折射率分布状况。The tapered fiber is placed in the liquid, and the distributed optical fiber sensing device detects the wavelength shift of the Rayleigh scattering spectrum of the tapered fiber, analyzes the wavelength shift, and obtains the continuously distributed refractive index of the liquid distribution.

所述拉锥光纤为细径光纤在拉锥机上拉制而成。The tapered optical fiber is drawn by a thin-diameter optical fiber on a tapered machine.

拉锥过程中的拉伸速度为200μm/s,氢氧焰往复距离为2000μm,往复速度为360μm/s,光纤伸长量为100000μm,锥区直径为4μm。During the taper drawing, the drawing speed was 200 μm/s, the reciprocating distance of the hydrogen-oxygen flame was 2000 μm, the reciprocating speed was 360 μm/s, the fiber elongation was 100000 μm, and the diameter of the cone region was 4 μm.

一种利用拉锥光纤测量分布式液体折射率的传感方法,所述传感方法包括以下步骤:A sensing method for measuring the refractive index of a distributed liquid by using a tapered optical fiber, the sensing method comprises the following steps:

在主干涉仪中由拉锥光纤背向瑞利散射形成拍频干涉信号,并对拍频干涉信号分别进行快速傅里叶变换,将光频域信息转换到对应拉锥光纤中各个位置的距离域信息,对距离域信息通过一定宽度的移动窗依次选取拉锥光纤的各个位置形成本地距离域信息;In the main interferometer, the back-rayleigh scattering of the taper fiber is used to form a beat-frequency interference signal, and the beat-frequency interference signal is respectively subjected to fast Fourier transform to convert the optical frequency domain information to the distance corresponding to each position in the taper fiber. Domain information, for the distance domain information, each position of the taper fiber is sequentially selected through a moving window of a certain width to form the local distance domain information;

参考信号和测量信号都利用移动窗选取拉锥光纤的本地距离域信息,将本地距离域信息补零,补零数量可以是补零前本地距离域数据长度数倍,然后将补零后本地距离域信息利用复数傅里叶反变换、再转换到光频域得到参考信号和测量信号的本地光频域信息;Both the reference signal and the measurement signal use the moving window to select the local distance field information of the tapered fiber, and fill the local distance field information with zeros. The domain information uses the complex inverse Fourier transform, and then converts it to the optical frequency domain to obtain the local optical frequency domain information of the reference signal and the measurement signal;

利用互相关运算对参考信号和测量信号的本地光频域信息进行光谱波长移动估计,互相关峰移动量反映瑞利散射光谱波长移动,瑞利散射光谱波长移动与液体折射率变化量成正比,通过互相关峰移动量即反映液体折射率变化量。The cross-correlation operation is used to estimate the spectral wavelength shift of the local optical frequency domain information of the reference signal and the measurement signal. The shift of the cross-correlation peak reflects the wavelength shift of the Rayleigh scattering spectrum. The wavelength shift of the Rayleigh scattering spectrum is proportional to the change of the refractive index of the liquid. The amount of change in the refractive index of the liquid is reflected by the amount of cross-correlation peak shift.

本发明提供的技术方案的有益效果是:The beneficial effects of the technical scheme provided by the present invention are:

1、本发明可成功应用于密集的液体折射率分布式测量、监测液体扩散,以及液层精确定位等场合;1. The present invention can be successfully applied to dense distributed measurement of liquid refractive index, monitoring of liquid diffusion, and precise positioning of liquid layers;

2、实现了高空间分辨率达到5mm的分布式液体折射率测量,灵敏度达到68.52nm/RIU;2. Realize distributed liquid refractive index measurement with high spatial resolution of 5mm and sensitivity of 68.52nm/RIU;

3、经试验验证,温度变化的测量误差最大为0.0002RI,验证了本发明的有效性。3. It is verified by experiments that the maximum measurement error of temperature change is 0.0002RI, which verifies the effectiveness of the present invention.

附图说明Description of drawings

图1为一种利用拉锥光纤测量分布式液体折射率的传感系统的结构示意图;1 is a schematic structural diagram of a sensing system for measuring the refractive index of a distributed liquid by utilizing a taper fiber;

图2为一种利用拉锥光纤测量分布式液体折射率的传感系统的另一结构示意图;FIG. 2 is another schematic structural diagram of a sensing system for measuring the refractive index of a distributed liquid by utilizing a tapered optical fiber;

图3为一种利用拉锥光纤测量分布式液体折射率的传感方法的流程图;3 is a flow chart of a sensing method for measuring the refractive index of a distributed liquid by utilizing a taper optical fiber;

图4为标定曲线的示意图;Fig. 4 is the schematic diagram of calibration curve;

图5为检测结果举例的示意图。FIG. 5 is a schematic diagram of an example of detection results.

附图中,各标号所代表的部件列表如下:In the accompanying drawings, the list of components represented by each number is as follows:

A:光频域反射的分布式光纤传感装置;A: Distributed optical fiber sensing device of optical frequency domain reflection;

1:可调谐激光器; 2:探测器;1: Tunable laser; 2: Detector;

3:50:50分束器; 4:1:99光分束器;3: 50:50 beam splitter; 4: 1:99 beam splitter;

5:50:50耦合器; 6:时钟整形电路模块;5: 50:50 coupler; 6: clock shaping circuit module;

7:延迟光纤; 8:第一法拉第转镜;7: Delay fiber; 8: First Faraday mirror;

9:第二法拉第转镜; 10:隔离器;9: Second Faraday mirror; 10: Isolator;

11:计算机; 12:偏振控制器;11: Computer; 12: Polarization Controller;

13:环形器; 14 50:50耦合器;13: Circulator; 14 50:50 Coupler;

15:拉锥光纤; 16:偏振分束器;15: Tapered fiber; 16: Polarizing beam splitter;

17:偏振分束器; 18:平衡探测器;17: Polarizing beam splitter; 18: Balance detector;

19:平衡探测器; 20:采集装置;19: balance detector; 20: acquisition device;

21:GPIB控制模块; 22:参考臂;21: GPIB control module; 22: Reference arm;

23:测试臂; 24:基于辅助干涉仪的时钟触发装置;23: Test arm; 24: Clock trigger device based on auxiliary interferometer;

25:主干涉仪; 26:拉锥光纤15的包层;25: main interferometer; 26: cladding of tapered fiber 15;

27:拉锥光纤15的纤芯。27: The core of the tapered optical fiber 15.

具体实施方式Detailed ways

为使本发明的目的、技术方案和优点更加清楚,下面对本发明实施方式作进一步地详细描述。In order to make the objectives, technical solutions and advantages of the present invention clearer, the embodiments of the present invention are further described in detail below.

传统基于拉锥光纤的折射率传感都是单点传感,而拉锥光纤的锥区可以保持一定长度即几厘米到几米,如采用专业拉丝设备可更长达到几十米甚至几公里,这为分布式光纤折射率传感提供可能。此外,将光频域反射技术与拉锥光纤结合,光频域反射技术解调拉锥光纤锥区的背向瑞利散射,有望实现分布式折射率传感。The traditional refractive index sensing based on tapered fiber is single-point sensing, and the tapered region of the tapered fiber can maintain a certain length, that is, a few centimeters to several meters. This provides the possibility for distributed optical fiber refractive index sensing. In addition, combining the optical frequency domain reflectometry technology with the tapered fiber, the optical frequency domain reflectometry demodulates the back Rayleigh scattering in the tapered region of the tapered fiber, and is expected to realize distributed refractive index sensing.

实施例1Example 1

为了解决现有技术无法实现密集的液体折射率分布式测量、监测液体扩散,液层精确定位等技术问题,本发明实施例提供了一种利用拉锥光纤测量分布式液体折射率的传感系统,参见图1,详见下文描述:In order to solve the technical problems such as the inability to achieve dense distributed measurement of liquid refractive index, monitor liquid diffusion, and precise positioning of liquid layers in the prior art, the embodiment of the present invention provides a sensing system for measuring distributed liquid refractive index by using a taper optical fiber , see Figure 1, and details are described below:

本发明实施例的设计原理如下:基于在拉锥光纤15的锥形区域部分,发生的背向瑞利散射模间干涉进行折射率传感,是通过锥形区域产生的较强倏逝波(具体的强弱确定根据实际经验值确定,本发明实施例对此不做限制)感知外界折射率的变化,从而改变拉锥光纤15内背向瑞利散射传播的有效模式折射率。The design principle of the embodiment of the present invention is as follows: the refractive index sensing is performed based on the interference between the back Rayleigh scattering modes in the tapered region of the tapered fiber 15, which is a strong evanescent wave ( The specific strength is determined according to the actual experience value, which is not limited in this embodiment of the present invention) to sense the change of the external refractive index, thereby changing the effective mode refractive index of back Rayleigh scattering propagation in the taper fiber 15 .

背向瑞利散射有效模式折射率的变化引起干涉相位差的改变,表现在瑞利散射光谱上的波长移动。通过光频域反射的分布式光纤传感装置A检测拉锥光纤15区域上瑞利散射光谱上的波长移动。当将拉锥光纤15置于液体中时,由于上述过程中的作用,通过分析分布式瑞利散射光谱波长移动,得到液体连续分布式的折射率分布状况。Changes in the index of refraction in the effective mode of back-Rayleigh scattering cause changes in the interference retardation, manifested as wavelength shifts on the Rayleigh scattering spectrum. The wavelength shift on the Rayleigh scattering spectrum on the region of the tapered fiber 15 is detected by the distributed optical fiber sensing device A of optical frequency domain reflection. When the tapered optical fiber 15 is placed in the liquid, the continuous distributed refractive index distribution of the liquid is obtained by analyzing the wavelength shift of the distributed Rayleigh scattering spectrum due to the effect of the above process.

综上所述,本发明实施例实现了高空间分辨率达到mm(毫米)级的分布式液体折射率测量,可成功应用于密集的液体折射率分布式测量、监测液体扩散,以及液层精确定位等场合。To sum up, the embodiment of the present invention realizes distributed liquid refractive index measurement with high spatial resolution reaching mm (millimeter) level, and can be successfully applied to dense distributed measurement of liquid refractive index, monitoring of liquid diffusion, and accurate liquid layer measurement. positioning, etc.

实施例2Example 2

下面结合图1对实施例1中的传感系统进行进一步地介绍,详见下文描述:该传感系统包括:拉锥光纤15、以及光频域反射的分布式光纤传感装置,其中,拉锥光纤15由细径在拉锥机上拉制而成。,包括:包层26和纤芯27(均拉至锥状)。The sensing system in Embodiment 1 will be further introduced below with reference to FIG. 1, and the details will be described below: the sensing system includes: a tapered optical fiber 15, and a distributed optical fiber sensing device for optical frequency domain reflection, wherein the pulling The tapered optical fiber 15 is drawn by a tapered machine with a small diameter. , including: cladding 26 and core 27 (both drawn to a tapered shape).

本发明实施例在拉锥过程中的拉伸速度为200μm/s,氢氧焰往复距离为2000μm,往复速度为360μm/s,光纤伸长量为100000μm,锥区直径为4μm。In the embodiment of the present invention, the drawing speed during the taper drawing process is 200 μm/s, the oxyhydrogen flame reciprocating distance is 2000 μm, the reciprocating speed is 360 μm/s, the fiber elongation is 100000 μm, and the diameter of the cone region is 4 μm.

光频域反射的分布式光纤传感装置包括:可调谐激光器1、1:99光分束器4、计算机11、GPIB(通用接口总线)控制模块21、基于辅助干涉仪的时钟触发装置24、主干涉仪25。The distributed optical fiber sensing device of optical frequency domain reflection includes: a tunable laser 1, a 1:99 optical beam splitter 4, a computer 11, a GPIB (General Purpose Interface Bus) control module 21, a clock trigger device 24 based on an auxiliary interferometer, Main interferometer 25.

其中,基于辅助干涉仪的时钟触发装置24包括:探测器2、第一50:50耦合器5、时钟倍频电路模块6、延迟光纤7、第一法拉第转镜8、第二法拉第转镜9和隔离器10。基于辅助干涉仪的时钟触发装置24用于实现等光频间距采样,其目的是抑制光源的非线性扫描。The clock triggering device 24 based on the auxiliary interferometer includes: a detector 2 , a first 50:50 coupler 5 , a clock frequency doubling circuit module 6 , a delay fiber 7 , a first Faraday turning mirror 8 , and a second Faraday turning mirror 9 and isolator 10. The clock triggering device 24 based on the auxiliary interferometer is used to realize sampling with equal optical frequency interval, and its purpose is to suppress the nonlinear scanning of the light source.

其中,主干涉仪25包括:50:50分束器3、偏振控制器12、环形器13、第二50:50耦合器14、第一偏振分束器16、第二偏振分束器17、第一平衡探测器18、第二平衡探测器19、采集装置20、参考臂22和测试臂23。主干涉仪25是光频域反射的分布式光纤传感装置A的核心,其为改进型马赫泽德干涉仪。The main interferometer 25 includes: a 50:50 beam splitter 3, a polarization controller 12, a circulator 13, a second 50:50 coupler 14, a first polarization beam splitter 16, a second polarization beam splitter 17, The first balance probe 18 , the second balance probe 19 , the acquisition device 20 , the reference arm 22 and the test arm 23 . The main interferometer 25 is the core of the optical frequency domain reflection distributed optical fiber sensing device A, which is an improved Mach-Zehnder interferometer.

GPIB控制模块21输入端与计算机11相连;GPIB控制模块21输出端与可调谐激光器1相连;可调谐激光器1与1:99光分束器4的a端口相连;1:99光分束器4的b端口与隔离器10的一端相连;1:99光分束器4的c端口与50:50分束器3的a端口相连;隔离器10的另一端与相连第一50:50耦合器5的b端口相连;第一50:50耦合器5的a端口与探测器2的一端相连;第一50:50耦合器5的c端口与第一法拉第转镜8相连;第一50:50耦合器5的d端口通过延迟光纤7与第二法拉第转镜9相连;探测器2的另一端与时钟倍频电路模块6的输入端相连;时钟整形电路模块6的输出端与采集装置20的输入端相连;50:50分束器3的b端口通过参考臂22与偏振控制器12的输入端相连;50:50分束器3的c端口通过测试臂23与环形器13的a端口相连;偏振控制器12的输出端与第二50:50耦合器14的a端口相连;环形器13的b端口与第二50:50耦合器14的b端口相连;环形器13的c端口与拉锥光纤15相连;第二50:50耦合器14的c端口与第一偏振分束器16的输入端相连;第二50:50耦合器14的d端口与第二偏振分束器17的输入端相连;第一偏振分束器16的输出端分别与第一平衡探测器18的输入端、第二平衡探测器19的输入端相连;第二偏振分束器17的输出端分别与第一平衡探测器18的输入端、第二平衡探测器19的输入端相连;第一平衡探测器18的输出端与采集装置20的输入端相连;第二平衡探测器19的输出端与采集装置20的输入端相连;采集装置20的输出端与计算机11相连。The input end of the GPIB control module 21 is connected to the computer 11; the output end of the GPIB control module 21 is connected to the tunable laser 1; the tunable laser 1 is connected to the a port of the 1:99 optical beam splitter 4; the 1:99 optical beam splitter 4 The b port of the isolator 10 is connected to one end; the c port of the 1:99 optical beam splitter 4 is connected to the a port of the 50:50 beam splitter 3; the other end of the isolator 10 is connected to the first 50:50 coupler The b port of the first 50:50 coupler 5 is connected to one end of the detector 2; the c port of the first 50:50 coupler 5 is connected to the first Faraday turning mirror 8; the first 50:50 The d port of the coupler 5 is connected with the second Faraday turning mirror 9 through the delay fiber 7; the other end of the detector 2 is connected with the input end of the clock frequency multiplying circuit module 6; the output end of the clock shaping circuit module 6 is connected with the output end of the acquisition device 20. The input end is connected; the b port of the 50:50 beam splitter 3 is connected to the input end of the polarization controller 12 through the reference arm 22; the c port of the 50:50 beam splitter 3 is connected to the a port of the circulator 13 through the test arm 23 The output end of the polarization controller 12 is connected with the a port of the second 50:50 coupler 14; the b port of the circulator 13 is connected with the b port of the second 50:50 coupler 14; the c port of the circulator 13 is connected with the pull The tapered fiber 15 is connected; the c port of the second 50:50 coupler 14 is connected to the input end of the first polarization beam splitter 16; the d port of the second 50:50 coupler 14 is connected to the input of the second polarization beam splitter 17 The output ends of the first polarization beam splitter 16 are respectively connected with the input end of the first balanced detector 18 and the input end of the second balanced detector 19; the output ends of the second polarization beam splitter 17 are respectively connected with the first balanced detector 18 and the second balanced detector 19. The input end of the balance detector 18 is connected with the input end of the second balance detector 19; the output end of the first balance detector 18 is connected with the input end of the acquisition device 20; the output end of the second balance detector 19 is connected with the acquisition device 20 The input end of the collecting device 20 is connected to the computer 11 .

装置工作时,计算机11通过GPIB控制模块21控制可调谐激光器1控制调谐速度、中心波长、调谐启动等;可调谐激光器1的出射光由1:99光分束器4的a端口进入,并以1:99的比例从1:99光分束器4的b端口经过隔离器10进入第一50:50耦合器5的b端口,光从第一50:50耦合器5的b端口进入,从第一50:50耦合器5的c和d端口出射,分别被两臂的第一法拉第转镜8和第二法拉第转镜9反射,返回到第一50:50耦合器5的c、d端口,两束光在第一50:50耦合器5中发生干涉,从第一50:50耦合器5的a端口输出;第一50:50耦合5器从a端口的出射光进入探测器2,探测器2将探测到的光信号转换为干涉拍频信号传输至时钟整形模块6,时钟整形模块6干涉拍频信号整形为方波,整形后的信号传输至采集装置20,作为采集装置20的外部时钟信号。When the device is working, the computer 11 controls the tunable laser 1 to control the tuning speed, center wavelength, tuning start, etc. through the GPIB control module 21; The ratio of 1:99 goes from the b port of the 1:99 optical beam splitter 4 through the isolator 10 into the b port of the first 50:50 coupler 5, and the light enters the b port of the first 50:50 coupler 5 from the b port of the first 50:50 coupler 5. The c and d ports of the first 50:50 coupler 5 exit, are respectively reflected by the first Faraday turning mirror 8 and the second Faraday turning mirror 9 of the two arms, and return to the c and d ports of the first 50:50 coupler 5 , the two beams of light interfere in the first 50:50 coupler 5 and output from the a port of the first 50:50 coupler 5; the outgoing light from the a port of the first 50:50 coupler 5 enters the detector 2, The detector 2 converts the detected optical signal into an interference beat frequency signal and transmits it to the clock shaping module 6 . The clock shaping module 6 shapes the interference beat frequency signal into a square wave, and the shaped signal is transmitted to the acquisition device 20 as a external clock signal.

可调谐激光器1的出射光由1:99光分束器4的a端口进入,从1:99光分束器4的c端口进入50:50分束器3的a端口;经过50:50分束器3从b端口进入参考臂22中的偏振控制器12,从c端口进入测试臂23上的环行器13的a端口;光从环行器13的a端口进入,从环行器13的c端口进入拉锥光纤15,而拉锥光纤15的背向散射光从环行器13端口c端口进入,从环行器13端口b端口输出;参考臂22中的偏振控制器12输出的参考光通过第二50:50耦合器14的a端口与环行器13上的背向散射光通过第二50:50耦合器14的b端口进形合束,形成拍频干涉并从第二50:50耦合器14的c端口和d端口输出至第一偏振分束器16和第一偏振分束器17,第一偏振分束器16和第一偏振分束器17通过第一平衡探测器18和第二平衡探测器19对应采集两个偏振分束器输出的正交方向的信号光,第一平衡探测器18和第二平衡探测器19将输出的模拟电信号传输至采集装置20,采集装置20在时钟整形模块6形成的外部时钟信号作用下将采集到的模拟电信号传输至计算机11。The output light of tunable laser 1 enters from port a of 1:99 optical beam splitter 4, and enters port a of 50:50 beam splitter 3 from port c of 1:99 optical beam splitter 4; after 50:50 minutes The beamer 3 enters the polarization controller 12 in the reference arm 22 from the b port, and enters the a port of the circulator 13 on the test arm 23 from the c port; Enter the tapered fiber 15, and the backscattered light of the tapered fiber 15 enters from the port c of the circulator 13 and outputs from the port b of the circulator 13; the reference light output by the polarization controller 12 in the reference arm 22 passes through the second The a-port of the 50:50 coupler 14 and the backscattered light on the circulator 13 are combined by the b-port of the second 50:50 coupler 14 to form beat interference and transmit from the second 50:50 coupler 14 The c port and the d port are output to the first polarization beam splitter 16 and the first polarization beam splitter 17, and the first polarization beam splitter 16 and the first polarization beam splitter 17 pass through the first balance detector 18 and the second balance The detector 19 correspondingly collects the signal light in the orthogonal direction output by the two polarization beam splitters, the first balanced detector 18 and the second balanced detector 19 transmit the output analog electrical signal to the acquisition device 20, and the acquisition device 20 is clocked. The collected analog electrical signal is transmitted to the computer 11 under the action of the external clock signal formed by the shaping module 6 .

GPIB控制模块21用于计算机11通过其控制可调谐激光器1。The GPIB control module 21 is used by the computer 11 to control the tunable laser 1 therethrough.

可调谐激光器1用于为光频域反射系统提供光源,其光频能够进行线性扫描。The tunable laser 1 is used to provide a light source for the optical frequency domain reflectometry system, and its optical frequency can be scanned linearly.

隔离器10防止辅助干涉仪中第一50:50耦合器5的b端口的反射光进入激光器。The isolator 10 prevents the reflected light from the b port of the first 50:50 coupler 5 in the auxiliary interferometer from entering the laser.

第一50:50耦合器5用于光干涉。The first 50:50 coupler 5 is used for optical interference.

延迟光纤7用于实现非等臂的拍频干涉,能够根据拍频和延迟光纤长度得到光频。The delay fiber 7 is used to realize the beat frequency interference of the anisotropic arms, and the optical frequency can be obtained according to the beat frequency and the length of the delay fiber.

第一法拉第转镜8和第二法拉第转镜9用于为干涉仪提供反射,且能够消除干涉仪的偏振衰落现象。The first Faraday turning mirror 8 and the second Faraday turning mirror 9 are used to provide reflection for the interferometer, and can eliminate the polarization fading phenomenon of the interferometer.

偏振控制器12作用是调节参考光偏振态,使其在偏振分束时两个正交方向上光强基本一致。The function of the polarization controller 12 is to adjust the polarization state of the reference light so that the light intensities in the two orthogonal directions are basically the same during polarization splitting.

第二50:50耦合器14完成对信号进行偏振分束,消除偏振衰落噪声的影响。The second 50:50 coupler 14 completes the polarization beam splitting of the signal to eliminate the influence of polarization fading noise.

计算机11:对采集装置20采集的干涉信号进行数据处理,实现基于光频域反射中利用拉锥光纤测量分布式液体折射率的光纤传感。Computer 11 : performs data processing on the interference signal collected by the collecting device 20 , and realizes optical fiber sensing based on optical frequency domain reflection using a taper fiber to measure the refractive index of a distributed liquid.

综上所述,本发明实施例实现了高空间分辨率达到mm(毫米)级的分布式液体折射率测量,可成功应用于密集的液体折射率分布式测量、监测液体扩散,以及液层精确定位等场合。To sum up, the embodiment of the present invention realizes distributed liquid refractive index measurement with high spatial resolution reaching mm (millimeter) level, and can be successfully applied to dense distributed measurement of liquid refractive index, monitoring of liquid diffusion, and accurate liquid layer measurement. positioning, etc.

实施例3Example 3

本发明实施例提供了一种利用拉锥光纤测量分布式液体折射率的传感方法,该传感方法是与实施例1和2中的传感系统相对应,如图2所示,该传感方法的步骤是:An embodiment of the present invention provides a sensing method for measuring the refractive index of a distributed liquid by using a tapered optical fiber. The sensing method corresponds to the sensing systems in Embodiments 1 and 2. As shown in FIG. The steps of the sensing method are:

101:在主干涉仪25中由拉锥光纤15背向瑞利散射形成拍频干涉信号,并对这拍频干涉信号分别进行快速傅里叶变换,将光频域信息转换到对应拉锥光纤15中各个位置的距离域信息,对距离域信息通过一定宽度的移动窗依次选取拉锥光纤15的各个位置形成本地距离域信息;101: In the main interferometer 25, a beat-frequency interference signal is formed by back Rayleigh scattering from the taper fiber 15, and fast Fourier transform is performed on the beat-frequency interference signal respectively, and the optical frequency domain information is converted to the corresponding taper fiber. The distance domain information of each position in 15, the distance domain information is successively selected through a moving window of a certain width to form the local distance domain information of each position of the tapered optical fiber 15;

102:参考信号和测量信号都利用移动窗选取拉锥光纤的本地距离域信息,将本地距离域信息补零,补零数量可以是补零前本地距离域数据长度数倍,然后将补零后本地距离域信息利用复数傅里叶反变换、再转换到光频域得到参考信号和测量信号的本地光频域信息;102: Both the reference signal and the measurement signal use the moving window to select the local distance field information of the tapered fiber, and zero-fill the local distance field information. The number of zero-filling can be several times the length of the local distance field data before zero-filling. The local distance domain information uses the complex inverse Fourier transform, and then converts it to the optical frequency domain to obtain the local optical frequency domain information of the reference signal and the measurement signal;

103:利用互相关运算对参考信号和测量信号的本地光频域信息进行光谱波长移动估计,互相关峰移动量反映瑞利散射光谱波长移动,瑞利散射光谱波长移动与液体折射率变化量成正比,通过互相关峰移动量即反映液体折射率变化量。103: Use the cross-correlation operation to estimate the spectral wavelength shift of the local optical frequency domain information of the reference signal and the measurement signal. The shift of the cross-correlation peak reflects the wavelength shift of the Rayleigh scattering spectrum, and the wavelength shift of the Rayleigh scattering spectrum is proportional to the change of the refractive index of the liquid. It is proportional to the amount of change in the refractive index of the liquid through the amount of cross-correlation peak shift.

综上所述,本发明实施例实现了高空间分辨率达到mm(毫米)级的分布式液体折射率测量,可成功应用于密集的液体折射率分布式测量、监测液体扩散,以及液层精确定位等场合。To sum up, the embodiment of the present invention realizes distributed liquid refractive index measurement with high spatial resolution reaching mm (millimeter) level, and can be successfully applied to dense distributed measurement of liquid refractive index, monitoring of liquid diffusion, and accurate liquid layer measurement. positioning, etc.

实施例4Example 4

下面结合具体的试验对实施例1-3中的传感系统和传感方法进行可行性验证,参见图3和图4,详见下文描述:The feasibility verification of the sensing system and sensing method in Embodiments 1-3 is carried out below in conjunction with specific tests, referring to FIG. 3 and FIG. 4 , and details are described below:

本发明实施例验证实验为采用细径光纤拉锥,利用该细径光纤的椎体测量折射率分布式变化,根据前期测量的拉锥光纤15的折射率传感系数,如图3所示,为K=68.52nm/RIU。The verification experiment of the embodiment of the present invention adopts the taper of a thin-diameter optical fiber, and uses the cone of the thin-diameter optical fiber to measure the distributed change of the refractive index. is K=68.52 nm/RIU.

将拉锥光纤15置入测量用的水槽,测量甘油水溶液折射率,逐步改变甘油水溶液浓度,进而改变其折射率进行测量。Put the tapered optical fiber 15 into the water tank for measurement, measure the refractive index of the glycerin aqueous solution, gradually change the concentration of the glycerin aqueous solution, and then change the refractive index for measurement.

真实折射率变化可以通过计算及查表得出。利用本发明实施例1-3中的传感系统和传感方法解调出折射率变化与真实折射率变化值进行比对,来验证本申请的有效性见表1。The real refractive index change can be obtained by calculation and look-up table. Using the sensing system and sensing method in Embodiments 1-3 of the present invention, the demodulated refractive index change is compared with the real refractive index change value to verify the validity of the present application as shown in Table 1.

表1测量折射率变化与真实折射率变化对比Table 1 Comparison of measured refractive index change and real refractive index change

真实折射率变化/RITrue Refractive Index Change/RI 测量折射率变化/RIMeasuring Refractive Index Change/RI 误差(测量值-真实值)/RIError (measured value - true value)/RI 1.35741.3574 1.35761.3576 0.00020.0002 1.35851.3585 1.35851.3585 00 1.35951.3595 1.35951.3595 00 1.36041.3604 1.36041.3604 00 1.36141.3614 1.36131.3613 -0.0001-0.0001 1.36241.3624 1.36231.3623 -0.0001-0.0001 1.36331.3633 1.36321.3632 -0.0001-0.0001 1.36421.3642 1.36411.3641 -0.0001-0.0001 1.36511.3651 1.36511.3651 00 1.36601.3660 1.36601.3660 00 1.36691.3669 1.36691.3669 00 1.36781.3678 1.36791.3679 0.00010.0001 1.36861.3686 1.36881.3688 0.00020.0002

从表1可以看到,温度变化的测量误差最大为0.0002RI,验证了本发明实施例设计的传感系统和方法的有效性。It can be seen from Table 1 that the maximum measurement error of the temperature change is 0.0002RI, which verifies the effectiveness of the sensing system and method designed in the embodiment of the present invention.

如图4所示,为检测结果的举例说明,在拉锥光纤15位于整条光纤的3.51m至3.54m范围内,检测到液体存在折射率变化,每点空间分辨率达到5mm。横坐标为距离,纵坐标为背向瑞利散射波长移动量,不同折射率变化对应着不同曲线,可见不同折射率对应的波长移动量不同。As shown in FIG. 4 , to illustrate the detection results, when the tapered optical fiber 15 is located in the range of 3.51m to 3.54m of the entire fiber, it is detected that there is a refractive index change in the liquid, and the spatial resolution of each point reaches 5mm. The abscissa is the distance, and the ordinate is the wavelength shift of the back Rayleigh scattering. Different refractive index changes correspond to different curves. It can be seen that the wavelength shift corresponding to different refractive indices is different.

综上所述,本发明实施例实现了高空间分辨率达到mm(毫米)级的分布式液体折射率测量,可成功应用于密集的液体折射率分布式测量、监测液体扩散,以及液层精确定位等场合。To sum up, the embodiment of the present invention realizes distributed liquid refractive index measurement with high spatial resolution reaching mm (millimeter) level, and can be successfully applied to dense distributed measurement of liquid refractive index, monitoring of liquid diffusion, and accurate liquid layer measurement. positioning, etc.

本发明实施例对各器件的型号除做特殊说明的以外,其他器件的型号不做限制,只要能完成上述功能的器件均可。In the embodiment of the present invention, the models of each device are not limited unless otherwise specified, as long as the device can perform the above functions.

本领域技术人员可以理解附图只是一个优选实施例的示意图,上述本发明实施例序号仅仅为了描述,不代表实施例的优劣。Those skilled in the art can understand that the accompanying drawing is only a schematic diagram of a preferred embodiment, and the above-mentioned serial numbers of the embodiments of the present invention are only for description, and do not represent the advantages or disadvantages of the embodiments.

以上所述仅为本发明的较佳实施例,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included in the protection of the present invention. within the range.

Claims (5)

1.一种利用拉锥光纤测量分布式液体折射率的传感系统,所述传感系统包括:光频域反射的分布式光纤传感装置,其特征在于,1. a sensing system utilizing a tapered optical fiber to measure the refractive index of a distributed liquid, the sensing system comprising: a distributed optical fiber sensing device of optical frequency domain reflection, characterized in that, 所述传感系统用于实现高空间分辨率达到毫米级的分布式液体折射率测量;The sensing system is used to realize distributed liquid refractive index measurement with high spatial resolution reaching millimeter level; 所述传感系统包括:拉锥光纤,The sensing system includes: a tapered optical fiber, 基于所述拉锥光纤的锥形区域部分发生的背向瑞利散射模间干涉,进行折射率传感,通过锥形区域产生的较强倏逝波感知外界折射率的变化,改变所述拉锥光纤内背向瑞利散射传播的有效模式折射率;Based on the interference between the back Rayleigh scattering modes in the tapered region of the tapered fiber, the refractive index sensing is performed, and the change of the external refractive index is sensed by the strong evanescent wave generated in the tapered region, and the change of the tapered fiber is changed. The effective mode index of back-Rayleigh scattering propagation in the tapered fiber; 将所述拉锥光纤置于液体中,通过所述分布式光纤传感装置,检测所述拉锥光纤的瑞利散射光谱的波长移动,分析所述波长移动,获取液体连续分布式的折射率分布状况;The tapered fiber is placed in the liquid, and the distributed optical fiber sensing device detects the wavelength shift of the Rayleigh scattering spectrum of the tapered fiber, analyzes the wavelength shift, and obtains the continuously distributed refractive index of the liquid distribution; 其中,光频域反射的分布式光纤传感装置包括:可调谐激光器、1:99光分束器、计算机、GPIB控制模块、基于辅助干涉仪的时钟触发装置、主干涉仪,The distributed optical fiber sensing device for optical frequency domain reflection includes: a tunable laser, a 1:99 optical beam splitter, a computer, a GPIB control module, a clock trigger device based on an auxiliary interferometer, and a main interferometer, 时钟触发装置包括:探测器、第一50:50耦合器、时钟倍频电路模块、延迟光纤、第一法拉第转镜、第二法拉第转镜和隔离器;所述时钟触发装置用于实现等光频间距采样,其目的是抑制光源的非线性扫描;The clock triggering device includes: a detector, a first 50:50 coupler, a clock frequency doubling circuit module, a delay fiber, a first Faraday turning mirror, a second Faraday turning mirror and an isolator; the clock triggering device is used to realize isooptical Frequency spacing sampling, the purpose of which is to suppress nonlinear scanning of the light source; 主干涉仪包括:50:50分束器、偏振控制器、环形器、第二50:50耦合器、第一偏振分束器、第二偏振分束器、第一平衡探测器、第二平衡探测器、采集装置、参考臂和测试臂;The main interferometer includes: 50:50 beam splitter, polarization controller, circulator, second 50:50 coupler, first polarization beam splitter, second polarization beam splitter, first balance detector, second balance detectors, acquisition devices, reference arms and test arms; GPIB控制模块输入端与计算机相连;GPIB控制模块输出端与可调谐激光器相连;可调谐激光器与1:99光分束器的a端口相连;1:99光分束器的b端口与隔离器的一端相连;1:99光分束器的c端口与50:50分束器的a端口相连;隔离器的另一端与相连第一50:50耦合器的b端口相连;第一50:50耦合器的a端口与探测器2的一端相连;第一50:50耦合器的c端口与第一法拉第转镜相连;第一50:50耦合器的d端口通过延迟光纤与第二法拉第转镜相连;探测器的另一端与时钟倍频电路模块的输入端相连;时钟整形电路模块的输出端与采集装置的输入端相连;50:50分束器的b端口通过参考臂与偏振控制器的输入端相连;50:50分束器的c端口通过测试臂与环形器的a端口相连;偏振控制器的输出端与第二50:50耦合器的a端口相连;环形器的b端口与第二50:50耦合器的b端口相连;环形器的c端口与拉锥光纤相连;第二50:50耦合器的c端口与第一偏振分束器的输入端相连;第二50:50耦合器的d端口与第二偏振分束器的输入端相连;第一偏振分束器的输出端分别与第一平衡探测器的输入端、第二平衡探测器的输入端相连;第二偏振分束器的输出端分别与第一平衡探测器的输入端、第二平衡探测器的输入端相连;第一平衡探测器的输出端与采集装置的输入端相连;第二平衡探测器的输出端与采集装置的输入端相连;采集装置的输出端与计算机相连;The input end of the GPIB control module is connected to the computer; the output end of the GPIB control module is connected to the tunable laser; the tunable laser is connected to the a port of the 1:99 optical beam splitter; the b port of the 1:99 optical beam splitter is connected to the isolator One end is connected; the c port of the 1:99 beam splitter is connected to the a port of the 50:50 beam splitter; the other end of the isolator is connected to the b port of the first 50:50 coupler; the first 50:50 coupling The a port of the first 50:50 coupler is connected to one end of the detector 2; the c port of the first 50:50 coupler is connected to the first Faraday turning mirror; the d port of the first 50:50 coupler is connected to the second Faraday turning mirror through a delay fiber ; The other end of the detector is connected to the input end of the clock frequency doubling circuit module; the output end of the clock shaping circuit module is connected to the input end of the acquisition device; the b port of the 50:50 beam splitter is connected to the input end of the polarization controller through the reference arm The c port of the 50:50 beam splitter is connected to the a port of the circulator through the test arm; the output of the polarization controller is connected to the a port of the second 50:50 coupler; the b port of the circulator is connected to the second The b port of the 50:50 coupler is connected to the b port; the c port of the circulator is connected to the taper fiber; the c port of the second 50:50 coupler is connected to the input of the first polarization beam splitter; the second 50:50 coupler The d port is connected with the input end of the second polarization beam splitter; the output end of the first polarization beam splitter is respectively connected with the input end of the first balanced detector and the input end of the second balanced detector; the second polarization beam splitter The output end of the detector is respectively connected with the input end of the first balanced detector and the input end of the second balanced detector; the output end of the first balanced detector is connected with the input end of the acquisition device; the output end of the second balanced detector is connected with The input end of the collection device is connected; the output end of the collection device is connected with the computer; 可调谐激光器用于为光频域反射系统提供光源,其光频进行线性扫描;隔离器防止辅助干涉仪中第一50:50耦合器的b端口的反射光进入激光器;延迟光纤用于实现非等臂的拍频干涉,根据拍频和延迟光纤长度得到光频;第一法拉第转镜和第二法拉第转镜用于为干涉仪提供反射,且消除干涉仪的偏振衰落现象;第二50:50耦合器完成对信号进行偏振分束,消除偏振衰落噪声的影响;计算机对采集装置采集的干涉信号进行数据处理,实现基于光频域反射中利用拉锥光纤测量分布式液体折射率的光纤传感。The tunable laser is used to provide the light source for the optical frequency domain reflectometry system, and its optical frequency is linearly scanned; the isolator prevents the reflected light from the b port of the first 50:50 coupler in the auxiliary interferometer from entering the laser; the delay fiber is used to realize non- The beat frequency interference of the equal arms, the optical frequency is obtained according to the beat frequency and the length of the delay fiber; the first Faraday turning mirror and the second Faraday turning mirror are used to provide reflection for the interferometer and eliminate the polarization fading phenomenon of the interferometer; the second 50: The 50 coupler completes the polarization beam splitting of the signal and eliminates the influence of polarization fading noise; the computer processes the data of the interference signal collected by the acquisition device, and realizes the optical fiber transmission based on the optical frequency domain reflection using the taper fiber to measure the refractive index of the distributed liquid. sense. 2.根据权利要求1所述的一种利用拉锥光纤测量分布式液体折射率的传感系统,其特征在于,所述拉锥光纤为细径光纤经过拉锥机拉制而成。2 . The sensing system for measuring the refractive index of distributed liquid by using a tapered optical fiber according to claim 1 , wherein the tapered optical fiber is a thin-diameter optical fiber drawn by a taper machine. 3 . 3.根据权利要求2所述的一种利用拉锥光纤测量分布式液体折射率的传感系统,其特征在于,所述拉锥机拉制具体为;拉伸速度为200μm/s,氢氧焰往复距离为2000μm,往复速度为360μm/s,光纤伸长量为100000μm,锥区直径为4μm。3 . The sensing system for measuring the refractive index of distributed liquid by using a taper fiber according to claim 2 , wherein the drawing of the taper machine is as follows: the drawing speed is 200 μm/s, the hydrogen-oxygen The flame reciprocating distance was 2000 μm, the reciprocating speed was 360 μm/s, the fiber elongation was 100000 μm, and the diameter of the cone region was 4 μm. 4.根据权利要求1-3中任一权利要求所述的一种利用拉锥光纤测量分布式液体折射率的传感系统,其特征在于,所述高空间分辨率达到5mm的分布式液体折射率测量,灵敏度达到68.52nm/RIU。4. A sensing system for measuring distributed liquid refractive index using tapered optical fiber according to any one of claims 1-3, characterized in that the high spatial resolution reaches a distributed liquid refractive index of 5 mm Rate measurement, the sensitivity reaches 68.52nm/RIU. 5.一种用于权利要求1所述的一种利用拉锥光纤测量分布式液体折射率的传感系统的传感方法,其特征在于,所述传感方法包括以下步骤:5. A sensing method for a sensing system using a tapered optical fiber to measure the refractive index of a distributed liquid according to claim 1, wherein the sensing method comprises the following steps: 在主干涉仪中由拉锥光纤背向瑞利散射形成拍频干涉信号,并对拍频干涉信号分别进行快速傅里叶变换,将光频域信息转换到对应拉锥光纤中各个位置的距离域信息,对距离域信息通过一定宽度的移动窗依次选取拉锥光纤的各个位置形成本地距离域信息;In the main interferometer, the back-rayleigh scattering of the taper fiber is used to form a beat-frequency interference signal, and the beat-frequency interference signal is respectively subjected to fast Fourier transform to convert the optical frequency domain information to the distance corresponding to each position in the taper fiber. Domain information, for the distance domain information, each position of the taper fiber is sequentially selected through a moving window of a certain width to form the local distance domain information; 参考信号和测量信号都利用移动窗选取拉锥光纤的本地距离域信息,将本地距离域信息补零,补零数量是补零前本地距离域数据长度数倍,然后将补零后本地距离域信息利用复数傅里叶反变换、再转换到光频域得到参考信号和测量信号的本地光频域信息;Both the reference signal and the measurement signal use the moving window to select the local distance field information of the tapered fiber, and fill the local distance field information with zeros. The information is transformed into the optical frequency domain by inverse complex Fourier transform to obtain the local optical frequency domain information of the reference signal and the measurement signal; 利用互相关运算对参考信号和测量信号的本地光频域信息进行光谱波长移动估计,互相关峰移动量反映瑞利散射光谱波长移动,瑞利散射光谱波长移动与液体折射率变化量成正比,通过互相关峰移动量即反映液体折射率变化量。The cross-correlation operation is used to estimate the spectral wavelength shift of the local optical frequency domain information of the reference signal and the measurement signal. The shift of the cross-correlation peak reflects the wavelength shift of the Rayleigh scattering spectrum. The wavelength shift of the Rayleigh scattering spectrum is proportional to the change of the refractive index of the liquid. The amount of change in the refractive index of the liquid is reflected by the amount of cross-correlation peak shift.
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