CN107496287A - The no added synthetic surfactant face cleaning product of whole plant - Google Patents
The no added synthetic surfactant face cleaning product of whole plant Download PDFInfo
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- CN107496287A CN107496287A CN201710754559.7A CN201710754559A CN107496287A CN 107496287 A CN107496287 A CN 107496287A CN 201710754559 A CN201710754559 A CN 201710754559A CN 107496287 A CN107496287 A CN 107496287A
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- face cleaning
- cleaning product
- extract
- synthetic surfactant
- whole plant
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- 238000004140 cleaning Methods 0.000 title claims abstract description 52
- 239000004094 surface-active agent Substances 0.000 title claims abstract description 40
- 239000000284 extract Substances 0.000 claims abstract description 67
- 241000196324 Embryophyta Species 0.000 claims abstract description 66
- 240000003377 Shepherdia canadensis Species 0.000 claims abstract description 56
- 235000018324 Shepherdia canadensis Nutrition 0.000 claims abstract description 56
- 239000000047 product Substances 0.000 claims abstract description 51
- 239000000203 mixture Substances 0.000 claims abstract description 42
- 239000006260 foam Substances 0.000 claims abstract description 29
- 239000004599 antimicrobial Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000003381 stabilizer Substances 0.000 claims abstract description 15
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 14
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims abstract description 14
- -1 glycosyl trehalose Chemical compound 0.000 claims abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 50
- 239000007788 liquid Substances 0.000 claims description 41
- 239000003755 preservative agent Substances 0.000 claims description 21
- 230000002335 preservative effect Effects 0.000 claims description 21
- 235000021028 berry Nutrition 0.000 claims description 15
- 241000193830 Bacillus <bacterium> Species 0.000 claims description 12
- 239000011812 mixed powder Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 9
- 235000015489 Emblica officinalis Nutrition 0.000 claims description 8
- 244000277583 Terminalia catappa Species 0.000 claims description 8
- 235000011517 Terminalia chebula Nutrition 0.000 claims description 8
- 240000003826 Eichhornia crassipes Species 0.000 claims description 7
- 241000628997 Flos Species 0.000 claims description 7
- 240000004153 Hibiscus sabdariffa Species 0.000 claims description 7
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 claims description 7
- 239000009806 pulsatillae Substances 0.000 claims description 7
- 240000008574 Capsicum frutescens Species 0.000 claims description 6
- 235000002568 Capsicum frutescens Nutrition 0.000 claims description 6
- 241000721692 Lythrum Species 0.000 claims description 6
- 241000006302 Usnea Species 0.000 claims description 6
- 238000010521 absorption reaction Methods 0.000 claims description 6
- 238000005119 centrifugation Methods 0.000 claims description 6
- 239000003480 eluent Substances 0.000 claims description 6
- 238000010828 elution Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 230000008014 freezing Effects 0.000 claims description 6
- 238000007710 freezing Methods 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 239000012982 microporous membrane Substances 0.000 claims description 6
- 239000011148 porous material Substances 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 6
- 239000011347 resin Substances 0.000 claims description 6
- 229920005989 resin Polymers 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 6
- 239000006228 supernatant Substances 0.000 claims description 6
- 238000002137 ultrasound extraction Methods 0.000 claims description 6
- 238000001291 vacuum drying Methods 0.000 claims description 6
- 238000005260 corrosion Methods 0.000 claims description 2
- 239000012530 fluid Substances 0.000 claims description 2
- 238000000855 fermentation Methods 0.000 claims 4
- 230000004151 fermentation Effects 0.000 claims 4
- 238000001694 spray drying Methods 0.000 claims 1
- 229920001908 Hydrogenated starch hydrolysate Polymers 0.000 abstract description 12
- 230000002500 effect on skin Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 10
- 230000003020 moisturizing effect Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- 230000001186 cumulative effect Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 239000000706 filtrate Substances 0.000 description 5
- 238000001035 drying Methods 0.000 description 4
- 238000005457 optimization Methods 0.000 description 4
- 230000003255 anti-acne Effects 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 2
- 108010009736 Protein Hydrolysates Proteins 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
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- 238000013329 compounding Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
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- 239000002736 nonionic surfactant Substances 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 2
- 229930182490 saponin Natural products 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 235000008534 Capsicum annuum var annuum Nutrition 0.000 description 1
- 240000008384 Capsicum annuum var. annuum Species 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 238000001604 Rao's score test Methods 0.000 description 1
- 206010040830 Skin discomfort Diseases 0.000 description 1
- 208000028990 Skin injury Diseases 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
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- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000004872 foam stabilizing agent Substances 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
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- 230000002688 persistence Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000006916 protein interaction Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229930183111 sapindoside Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- RXHIKAIVEMAPRU-JRIGQVHBSA-N sequiterpene Natural products C1=C(C)[C@@H](OC(C)=O)[C@H](O)[C@@]2(O)[C@H](C)CC[C@@H](C(C)=C)[C@H]21 RXHIKAIVEMAPRU-JRIGQVHBSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 150000008130 triterpenoid saponins Chemical class 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of no added synthetic surfactant face cleaning product of whole plant, aim to provide one kind and only contain natural surfactant, other synthetic surfactants are not contained, the good face cleaning product of clean skin effect, its technical scheme is based on gross mass 100%, soapberry extract 5 30%, foam stabilizer 10 30%, plant antiseptic agent 0.8 1.2%, surplus is water；Described foam stabilizer is by hydrogenated starch hydrolysate and glycosyl trehalose according to mass ratio 0.5:1.2 1.6 compositions；Belong to technical field of skin care.
Description
Technical field
The invention discloses a kind of face cleaning product, is that a kind of no added synthetic surfactant of whole plant is clean specifically
Face product, belongs to technical field of skin care.
Background technology
Basic engineering of the face cleaning as skin nursing, along with the worsening of environment and the continuous of air quality
Drop, its spatter property have indispensable important function in daily life.
Most of common face cleaning product is all based on surfactant in the market, is had during face cleaning quite
The surfactant of quantity interacts with cuticula, while cleaning, can dissolve the lipid of part cuticula, cause
Dry skin；Part surface activating agent also with cuticula protein interaction, causes protein denaturation, is brought to sensitive skin
Injury.
And although the non-soap fundamental mode face cleaning product based on amino acid type surfactant is fine in skin-friendly, excitant is small,
But dirt-removing power is not strong, and need excellent by can just obtain foaming characteristic, water solubility with other surfaces activating agent reasonable compatibility
Good face cleaning product, therefore complicated component.
Under the trend of " advocating green, back to nature ", safe and reliable natural surfactant substitutes chemistry and closed
Forming surfactants are by as the development trend from now on of face cleaning product.
Soapberry is China's conventional articles for washing among the people from ancient times, contains abundant glycoside material (master in its aril
To be triterpenoid saponin and sequiterpene glucosides), content is about 4%, has good foaming characteristic, dirt-removing power is strong, there is " natural plants
The title of property soap ".But as the continuous progress of science and technology, increasing chemical synthesis cleaning agent are come out one after another, no trouble
Sub just few people shows any interest.Nonionic surface active agent of the soapberry as natural origin, easily biological-degradable, with skin compatibility
It is good, meet the theory of " advocating green, back to nature ", can also meet that consumer is growing to green safe face cleaning product
Psychological needs.
The surface tension that foam has can increase contact of the surfactant with skin, increase dirt-carrying to a certain extent
Power, the foam quality of face cleaning product are closely related with its pouplarity.The foamability and foam stabilization of soapberry extract
Property increases with the increase of the pH value of solution, and soapberry extract exists with non-ionic form in an acidic solution, foaming properties
It is poor.There are some researches show soapberry extract can be remarkably reinforced the foam stability of system with nonionic surfactant compounding
Can, but other nonionic surfactants not only complicated component is added in face cleaning formula, it is not green safe enough, and without trouble
Sub- saponin has expansion capillary of skin and has haemocylolysis, particularly there is strong impulse effect to eye, even if so
Soapberry extract has good clean result, still cannot be directly used to face's cleaning washing.
There is presently no have the faintly acid of good foam stability energy clean separately as surfactant soapberry extract
Face product.
The content of the invention
For above-mentioned deficiency, it is an object of the invention to provide one kind only to contain natural surfactant, does not contain otherization
Learn synthetic surfactant, the good face cleaning product of clean skin effect.
Therefore, technical scheme provided by the invention is such：
A kind of no added synthetic surfactant face cleaning product of whole plant, based on gross mass 100%, soapberry extract 5-
30%, foam stabilizer 10-30%, plant antiseptic agent 0.8-1.2%, surplus are water；Described foam stabilizer is by hydrogenated starch hydrolysate
With glycosyl trehalose according to mass ratio 0.5:1.2-1.6 composition.
As present invention further optimization, the no added synthetic surfactant face cleaning product of above-mentioned whole plant is described
Plant antiseptic agent be preservative compositions A or preservative compositions B or preservative compositions A and preservative compositions B mixture, the anti-corrosion group
A is closed by lythrum salucaria, cyani flos extract, myrobalan's berry extract according to mass ratio 3:2:3 compositions, the preservative compositions
B is by long and thin hot pepper berry extract, Radix Pulsatillae extract, palpus extractive of usnea according to mass ratio 3:2:4 compositions.
As present invention further optimization, the no added synthetic surfactant face cleaning product of above-mentioned whole plant is described
Soapberry extract pass sequentially through following step and be made：20-40 parts by weight soapberry pericarps are weighed, are placed in 150-280 weight
Soaked 20 days in part plant fermented liquid, by the soapberry pericarp of soaking processing in 0 to 4 DEG C of low-temperature vacuum drying, after freezing
Soapberry ultramicro grinding, into soapberry fine powder add 20-80% ethanol, solid-liquid ratio 1:40-60, carried in 25 DEG C of ultrasounds
20min is taken, supersonic frequency 1.5-2.0MHz, filtering with microporous membrane, filtrate, then upper large pore resin absorption column is collected, is washed to
After colourless, then it is colourless to eluent with 20-80% ethanol elutions, ethanol eluate is collected, film concentration removes ethanol, and spraying is dry
It is dry, obtain soapberry extract.
As present invention further optimization, the no added synthetic surfactant face cleaning product of above-mentioned whole plant is described
Plant fermented liquid pass sequentially through following step and be made：Roselle flower 25-40 parts by weight are weighed, water hyacinth 30-50 parts by weight, are dried
It is dry, 20-80 mesh is crushed to, mixes, obtains mixed-powder；The water of mixed-powder 40-50 times of volume of weight is added, is then added mixed
Liquid cumulative volume 10-30% Bacillus acidi lactici liquid is closed, is fermented under conditions of 25-30 DEG C 2-3 months, it is filtered, centrifugation, take supernatant
Liquid, the 1/4 of original volume is concentrated in vacuo to, obtains plant fermented liquid.
As present invention further optimization, the no added synthetic surfactant face cleaning product of above-mentioned whole plant is described
Bacillus acidi lactici liquid concentration be 105-108CFU/ml。
Compared with prior art, technical scheme provided by the invention has the advantages that：
1st, technical scheme provided by the invention is only containing soapberry extract, hydrogenated starch hydrolysate, glycosyl trehalose, thousand
Bend dish extract, cyani flos extract, myrobalan's berry extract (or long and thin hot pepper berry extract, Radix Pulsatillae extract, must sunglo extraction
Thing) several compositions, composition is simple, and each composition derives from natural plants, without other synthetic surfactants, to skin
Fanout free region.
2nd, soapberry extract is sapindoside in technical scheme provided by the invention, and its minimum addition is 5%, i.e.,
The soapberry extract of the present invention has the advantages of " dosage is few, and effect is good, and cost is low ".
3rd, hydrogenated starch hydrolysate and glycosyl trehalose are this area routine NMF in technical scheme provided by the invention,
But the present invention is by both according to 0.5:Used after 1.4 special ratios compounding as foam stabilizer, increasing is cooperateed with soapberry extract
Effect, obtains rich solid, more and dense, the good face cleaning product of persistence.
Wherein, hydrogenated starch hydrolysate be by obtained multi-sugar alcohol mixture after Starch Hydrolysis, hydrogenation, except containing
Outside single, double poly- multi-sugar alcohol, also containing substantial amounts of hydrogenated oligosaccharides and hydrogenated polysaccharides, there is moisturizing, the physico-chemical property of crystallization-preventive；
Glycosyl trehalose (glycosyl trehalose) is the polysaccharide body from corn；Two kinds of compositions and soapberry extract phase interaction
With also acting as the effect of good replenishing water and preserving moisture.
4th, plant antiseptic agent is preservative compositions A or preservative compositions B or preservative compositions A in technical scheme provided by the invention
With preservative compositions B, preservative compositions A is by lythrum salucaria, cyani flos extract, myrobalan's berry extract according to 3:2:3 spy
Certainty ratio forms, and preservative compositions B is by long and thin hot pepper berry extract, and Radix Pulsatillae extract and palpus extractive of usnea are according to 3:2:4 it is specific
Ratio composition, preservative compositions A or preservative compositions B and soapberry extract, hydrogenated starch hydrolysate, glycosyl trehalose three are mutual
Effect, acts not only as the preservative of face cleaning product, suppresses harmful bacteria after can also aiding in soapberry extract face cleaning, adjusts
Nodal section portion microorganism microecological balance.
Sum it up, the no added synthetic surfactant face cleaning product of whole plant provided by the invention, successfully will be without trouble
Seed extract is applied to faintly acid face cleaning product separately as surfactant, has the good careful degree of foam, durable lather
Degree and cleaning force, and it is gently non-stimulated to skin during cleaning.
Embodiment
It is further to claim of the invention to be limited with reference to embodiment, but do not form to this
Any restrictions of invention, anyone limited number of time made in the claims in the present invention protection domain modification, the present invention's
Within claims.
It should be noted that the unspecified technological parameter of the present invention, raw material etc. are according to this area routine techniques hand
Duan Jinhang.
Embodiment 1
The no added synthetic surfactant face cleaning product of a kind of whole plant provided by the invention, based on gross mass 100g, nothing
Suffer from seed extract 30g, foam stabilizer 23.5g, plant antiseptic agent 0.8g, surplus is water.
Wherein：Described foam stabilizer is by hydrogenated starch hydrolysate and glycosyl trehalose according to mass ratio 0.5:1.2 composition；Institute
The plant antiseptic agent stated is by long and thin hot pepper berry extract, and Radix Pulsatillae extract and palpus extractive of usnea are according to 3:2:4 compositions.
Described soapberry extract passes sequentially through following step and is made：40 parts by weight soapberry pericarps are weighed, are placed in 150
Soaked 20 days in parts by weight plant fermented liquid, by the soapberry pericarp of soaking processing in 0 DEG C of low-temperature vacuum drying, after freezing
Soapberry ultramicro grinding, 60mL 20% ethanol is added in every gram of soapberry fine powder, and (i.e. solid-liquid ratio is 1:60), at 25 DEG C
Ultrasonic extraction 20min, supersonic frequency 2.0MHz, filtering with microporous membrane, collect filtrate, then upper large pore resin absorption column, washing
To after colourless, then it is colourless to eluent with 80% ethanol elution, ethanol eluate is collected, film concentration removes ethanol, is spray-dried,
Obtain soapberry extract.
Above-mentioned plant fermented liquid passes sequentially through following step and is made：Weigh the parts by weight of Roselle flower 40, the weight of water hyacinth 50
Part is measured, drying, is crushed to 80 mesh, mixes, obtains mixed-powder；The water of mixed-powder 50 times of volumes of weight is added, is then added
The Bacillus acidi lactici liquid of mixed liquor cumulative volume 30%, described Bacillus acidi lactici liquid concentration are 108CFU/ml, sent out under conditions of 25 DEG C
Ferment 3 months, it is filtered, centrifugation, supernatant is taken, the 1/4 of original volume is concentrated in vacuo to, obtains plant fermented liquid.
Embodiment 2
The no added synthetic surfactant face cleaning product of a kind of whole plant provided by the invention, based on gross mass 100g, nothing
Suffer from seed extract 20g, foam stabilizer 14.5g, plant antiseptic agent 1.2g, surplus is water.
Wherein：Described foam stabilizer is by hydrogenated starch hydrolysate and glycosyl trehalose according to mass ratio 0.5:1.6 composition；Institute
The plant antiseptic agent stated is by long and thin hot pepper berry extract, and Radix Pulsatillae extract and palpus extractive of usnea are according to quality 3:2:4 compositions.
Described soapberry extract passes sequentially through following step and is made：40 parts by weight soapberry pericarps are weighed, are placed in 280
Soaked 20 days in parts by weight plant fermented liquid, by the soapberry pericarp of soaking processing in 4 DEG C of low-temperature vacuum dryings, after freezing
Soapberry ultramicro grinding, 60mL 80% ethanol is added in every gram of soapberry fine powder, and (i.e. solid-liquid ratio is 1:60), at 25 DEG C
Ultrasonic extraction 20min, supersonic frequency 2.0MHz, filtering with microporous membrane, collect filtrate, then upper large pore resin absorption column, washing
To after colourless, then it is colourless to eluent with 80% ethanol elution, ethanol eluate is collected, film concentration removes ethanol, is spray-dried,
Obtain soapberry extract.
Above-mentioned plant fermented liquid passes sequentially through following step and is made：Weigh the parts by weight of Roselle flower 25, the weight of water hyacinth 50
Part is measured, drying, is crushed to 20 mesh, mixes, obtains mixed-powder；The water of mixed-powder 40 times of volumes of weight is added, is then added
The Bacillus acidi lactici liquid of mixed liquor cumulative volume 30%, described Bacillus acidi lactici liquid concentration are 108CFU/ml, sent out under conditions of 25 DEG C
Ferment 2 months, it is filtered, centrifugation, supernatant is taken, the 1/4 of original volume is concentrated in vacuo to, obtains plant fermented liquid.
Embodiment 3
The no added synthetic surfactant face cleaning product of a kind of whole plant provided by the invention, based on gross mass 100g, nothing
Suffer from seed extract 5g, foam stabilizer 15g, plant antiseptic agent 1g, surplus is water.
Wherein：Described foam stabilizer is by hydrogenated starch hydrolysate and glycosyl trehalose according to mass ratio 0.5:1.4 composition；Institute
The plant antiseptic agent stated is by lythrum salucaria, cyani flos extract, myrobalan's berry extract according to mass ratio 3:2:3 compositions.
Described soapberry extract passes sequentially through following step and is made：30 parts by weight soapberry pericarps are weighed, are placed in 200
Soaked 20 days in parts by weight plant fermented liquid, by the soapberry pericarp of soaking processing in 2 DEG C of low-temperature vacuum dryings, after freezing
Soapberry ultramicro grinding, 50mL 50% ethanol is added in every gram of soapberry fine powder, and (i.e. solid-liquid ratio is 1:50), at 25 DEG C
Ultrasonic extraction 20min, supersonic frequency 1.8MHz, filtering with microporous membrane, collect filtrate, then upper large pore resin absorption column, washing
To after colourless, then it is colourless to eluent with 50% ethanol elution, ethanol eluate is collected, film concentration removes ethanol, is spray-dried,
Obtain soapberry extract.
Above-mentioned plant fermented liquid passes sequentially through following step and is made：Weigh the parts by weight of Roselle flower 30, the weight of water hyacinth 40
Part is measured, drying, is crushed to 50 mesh, mixes, obtains mixed-powder；The water of mixed-powder 40 times of volumes of weight is added, is then added
The Bacillus acidi lactici liquid of mixed liquor cumulative volume 20%, described Bacillus acidi lactici liquid concentration are 106CFU/ml, sent out under conditions of 28 DEG C
Ferment 2 months, it is filtered, centrifugation, supernatant is taken, the 1/4 of original volume is concentrated in vacuo to, obtains plant fermented liquid.
Embodiment 4
The no added synthetic surfactant face cleaning product of a kind of whole plant provided by the invention, based on gross mass 100g, nothing
Suffer from seed extract 10g, foam stabilizer 21g, plant antiseptic agent 0.9, surplus is water.
Wherein：Described foam stabilizer is by hydrogenated starch hydrolysate and glycosyl trehalose according to mass ratio 0.5:1.5 composition；Institute
The plant antiseptic agent stated is by preservative A and preservative B according to mass ratio 1:1 mixes；Described plant antiseptic agent A is bent by thousand
Dish extract, cyani flos extract, myrobalan's berry extract are according to mass ratio 3:2:3 compositions；Described plant antiseptic agent B is by the Qin
Green pepper berry extract, Radix Pulsatillae extract and palpus extractive of usnea are according to 3:2:4.
Described soapberry extract passes sequentially through following step and is made：35 parts by weight soapberry pericarps are weighed, are placed in 250
Soaked 20 days in parts by weight plant fermented liquid, by the soapberry pericarp of soaking processing in 3 DEG C of low-temperature vacuum dryings, after freezing
Soapberry ultramicro grinding, 50mL 60% ethanol is added in every gram of soapberry fine powder, and (i.e. solid-liquid ratio is 1:50), at 25 DEG C
Ultrasonic extraction 20min, supersonic frequency 1.6MHz, filtering with microporous membrane, collect filtrate, then upper large pore resin absorption column, washing
To after colourless, then it is colourless to eluent with 40% ethanol elution, ethanol eluate is collected, film concentration removes ethanol, is spray-dried,
Obtain soapberry extract.
Above-mentioned plant fermented liquid passes sequentially through following step and is made：Weigh the parts by weight of Roselle flower 35, the weight of water hyacinth 40
Part is measured, drying, is crushed to 50 mesh, mixes, obtains mixed-powder；The water of mixed-powder 45 times of volumes of weight is added, is then added
The Bacillus acidi lactici liquid of mixed liquor cumulative volume 20%, described Bacillus acidi lactici liquid concentration is 105CFU/ml, is sent out under conditions of 28 DEG C
Ferment 2 months, it is filtered, centrifugation, supernatant is taken, the 1/4 of original volume is concentrated in vacuo to, obtains plant fermented liquid.
The no added synthetic surfactant face cleaning product preparation method of above-mentioned whole plant is by soapberry extract, foam stabilizing
Agent, plant antiseptic agent are added to the water, well mixed to produce.
In order to better illustrate beneficial effects of the present invention, comparative example 1-4 is given below, and by they and embodiment 1-
4 together carry out normal individual trial test：
The face cleaning product that comparative example 1 provides, its soapberry pericarp do not soak plant fermented liquid, and remaining is protected with embodiment 3
Hold consistent；
The face cleaning product that comparative example 2 provides, tea saponin is substituted for by soapberry extract, and remaining keeps one with embodiment 3
Cause；
The face cleaning product that comparative example 3 provides, 1 is changed to by the ratio of hydrogenated starch hydrolysate and glycosyl trehalose:1, remaining
It is consistent with embodiment 3；
Comparative example 4 provide face cleaning product, by lythrum salucaria, cyani flos extract, myrobalan's berry extract ratio
Example is changed to 3:1:4, remaining is consistent with embodiment 3.
Test population：160 subjects are chosen, age 20-40 year, sex is random, is divided into 8 groups, every group of 20 people.
Test sample：Embodiment 1-4 face cleaning product and comparative example 1-4 face cleaning product.
Method of testing：Test sample is issued into subject to use, subject is used, first using clear water drenched sooner or later daily
Skin of face, face is applied in right amount using test product, gently rub about one minute, then rinsed well with clear water, daily weight sooner or later
Multiple above-mentioned steps, after each test sample uses two weeks, score test sample, the results are shown in Table shown in 1.Scoring takes 10
Divide system, 1 point worst, and 10 points best.
Table 1
As a result show, the face cleaning product that 1-4 of the embodiment of the present invention is provided, the careful degree average 8.54 of foam, foam are held
Degree average 8.28, cleannes average 7.63, gentle degree average 7.41, moisturizing degree average 7.56, pre- long
Anti-acne average 6.59, and do not have reaction phenomena such as allergy, skin discomfort occur, illustrate whole plant provided by the invention without
Adding synthetic surfactant face cleaning product not only has good foam careful degree, durable lather degree and cleannes, Er Qieqing
It is gently non-stimulated to skin when clean.
The embodiment of the present invention 3 has higher average compared with comparative example 1, illustrates to soak on soapberry pericarp and plants
Thing zymotic fluid, have an impact to the careful degree of foam of product, durable lather degree, cleannes, gentle degree, moisturizing degree and pre- anti-acne；
The embodiment of the present invention 3 has higher average compared with comparative example 2, illustrates the foam stabilizing of soapberry extract and the present invention
Agent and plant antiseptic agent collaboration, to the careful degree of foam of product, durable lather degree, cleannes, gentle degree, moisturizing degree and prevention powder
Thorn has an impact；The embodiment of the present invention 3 has higher average, illustrates hydrogenated starch hydrolysate and sugar compared with comparative example 3
The compound proportion of base trehalose is to the careful degree of foam of product, durable lather degree, cleannes, gentle degree, moisturizing degree and prevention powder
Thorn has an impact；The embodiment of the present invention 3 has higher average compared with comparative example 4, illustrates lythrum salucaria, arrow car
The careful degree of foam to product of chrysanthemum extract and the compound proportion of myrobalan berry extract three, durable lather degree, cleannes, temperature
Have an impact with degree, moisturizing degree and pre- anti-acne.
Claims (10)
- A kind of 1. no added synthetic surfactant face cleaning product of whole plant, it is characterised in that based on gross mass 100%, no trouble Seed extract 5-30%, foam stabilizer 10-30%, plant antiseptic agent 0.8-1.2%, surplus are water；Described foam stabilizer is by hydrogenating Glucidtemns and glycosyl trehalose are according to mass ratio 0.5:1.2-1.6 composition.
- 2. the no added synthetic surfactant face cleaning product of whole plant according to claim 1, it is characterised in that described Plant antiseptic agent is preservative compositions A or preservative compositions B or preservative compositions A and preservative compositions B mixture, the preservative compositions A by according to lythrum salucaria, cyani flos extract, myrobalan's berry extract according to mass ratio 3:2:3 compositions, the anti-corrosion group B is closed by long and thin hot pepper berry extract, Radix Pulsatillae extract, palpus extractive of usnea according to mass ratio 3:2:4 compositions.
- 3. the no added synthetic surfactant face cleaning product of whole plant according to claim 1, it is characterised in that described Soapberry extract passes sequentially through following step and is made：20-40 parts by weight soapberry pericarps are weighed, are placed in 150-280 parts by weight Soaked in plant fermented liquid, by the soapberry pericarp of soaking processing in 0 to 4 DEG C of low-temperature vacuum drying, by after freezing without trouble Sub- ultramicro grinding, 20-80% ethanol is added into soapberry fine powder, in 25 DEG C of ultrasonic extractions, filtering with microporous membrane, collect filter Liquid, then upper large pore resin absorption column, be washed to it is colourless after, it is then colourless to eluent with 20-80% ethanol elutions, collect ethanol and wash De- liquid, film concentration remove ethanol, spray drying, obtain soapberry extract.
- 4. the no added synthetic surfactant face cleaning product of whole plant according to claim 3, it is characterised in that the nothing Suffer from sub- pericarp and be placed in plant fermented liquid and soak 20 days.
- 5. the no added synthetic surfactant face cleaning product of whole plant according to claim 3, it is characterised in that the nothing The solid-liquid ratio for suffering from careful powder and ethanol is 1:40-60.
- 6. the no added synthetic surfactant face cleaning product of whole plant according to claim 3, it is characterised in that described The technological parameter of ultrasonic extraction is：Ultrasonic time is 20min, supersonic frequency 1.5-2.0MHz.
- 7. the no added synthetic surfactant face cleaning product of whole plant according to claim 3, it is characterised in that described Plant fermented liquid passes sequentially through following step and is made：Roselle flower 25-40 parts by weight are weighed, water hyacinth 30-50 parts by weight, are dried It is dry, crush, mix, obtain mixed-powder；The water of mixed-powder 40-50 times of volume of weight is added, it is overall then to add mixed liquor Product 10-30% Bacillus acidi lactici liquid, fermentation is filtered, centrifugation, takes supernatant, is concentrated in vacuo to the 1/4 of original volume, obtains plant Zymotic fluid.
- 8. the no added synthetic surfactant face cleaning product of whole plant according to claim 7, it is characterised in that described Roselle flower and water hyacinth cross 20-80 mesh sieves and mixed again after crushed.
- 9. the no added synthetic surfactant face cleaning product of whole plant according to claim 7, it is characterised in that described The technological parameter of fermentation is：Fermentation temperature is 25-30 DEG C, and fermentation time is 2-3 months.
- 10. the no added synthetic surfactant face cleaning product of whole plant according to claim 7, it is characterised in that described Bacillus acidi lactici liquid concentration be 105-108CFU/ml。
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| CN109620746A (en) * | 2018-12-06 | 2019-04-16 | 澳宝化妆品（惠州）有限公司 | A kind of Calyx Hibisci Sabdariffae extract and its application in facial-care composition |
| CN111110607A (en) * | 2020-02-26 | 2020-05-08 | 何军 | Mild moisturizing type foam facial cleanser and preparation method thereof |
| CN113214913A (en) * | 2021-04-29 | 2021-08-06 | 浙江吉叶生物科技有限公司 | Natural surfactant and preparation method thereof |
| CN113425661A (en) * | 2021-08-11 | 2021-09-24 | 广州睿森生物科技有限公司 | Plant composition with cleaning and repairing effects and application thereof |
| CN115998656A (en) * | 2023-02-09 | 2023-04-25 | 博贤实业(广东)有限公司 | A kind of shampoo containing natural surfactant and preparation method thereof |
| CN116077392A (en) * | 2023-01-18 | 2023-05-09 | 广州环亚化妆品科技股份有限公司 | Application of soapberry fermentation product in preparation of daily chemical products |
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