CN106010795A - Tea tree essential oil extracting method and tea tree essential oil composition - Google Patents
Tea tree essential oil extracting method and tea tree essential oil composition Download PDFInfo
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- CN106010795A CN106010795A CN201610578364.7A CN201610578364A CN106010795A CN 106010795 A CN106010795 A CN 106010795A CN 201610578364 A CN201610578364 A CN 201610578364A CN 106010795 A CN106010795 A CN 106010795A
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- China
- Prior art keywords
- tea tree
- ethereal oil
- tree ethereal
- essential oil
- extracting method
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- 235000009024 Ceanothus sanguineus Nutrition 0.000 title claims abstract description 36
- 240000003553 Leptospermum scoparium Species 0.000 title claims abstract description 36
- 235000015459 Lycium barbarum Nutrition 0.000 title claims abstract description 36
- 239000000341 volatile oil Substances 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000000203 mixture Substances 0.000 title claims description 7
- 239000003814 drug Substances 0.000 claims abstract description 14
- 229940079593 drug Drugs 0.000 claims abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims description 13
- LKOJGSWUMISDOF-UHFFFAOYSA-N oroxylin A Chemical compound C=1C(=O)C2=C(O)C(OC)=C(O)C=C2OC=1C1=CC=CC=C1 LKOJGSWUMISDOF-UHFFFAOYSA-N 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 7
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 6
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 claims description 4
- IQPNAANSBPBGFQ-UHFFFAOYSA-N luteolin Chemical compound C=1C(O)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(O)C(O)=C1 IQPNAANSBPBGFQ-UHFFFAOYSA-N 0.000 claims description 4
- LRDGATPGVJTWLJ-UHFFFAOYSA-N luteolin Natural products OC1=CC(O)=CC(C=2OC3=CC(O)=CC(O)=C3C(=O)C=2)=C1 LRDGATPGVJTWLJ-UHFFFAOYSA-N 0.000 claims description 4
- 235000009498 luteolin Nutrition 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 4
- 235000019198 oils Nutrition 0.000 claims description 4
- ZNLQDZISIWGUNG-UHFFFAOYSA-L [Na+].C(CCCCCCCCCCCCCCC)C1=C(C(=C(C=C1)S(=O)(=O)[O-])OC1=CC=CC=C1)S(=O)(=O)[O-].[Na+] Chemical compound [Na+].C(CCCCCCCCCCCCCCC)C1=C(C(=C(C=C1)S(=O)(=O)[O-])OC1=CC=CC=C1)S(=O)(=O)[O-].[Na+] ZNLQDZISIWGUNG-UHFFFAOYSA-L 0.000 claims description 3
- 235000012343 cottonseed oil Nutrition 0.000 claims description 3
- 125000003074 decanoyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C(*)=O 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- JMGZBMRVDHKMKB-UHFFFAOYSA-L disodium;2-sulfobutanedioate Chemical compound [Na+].[Na+].OS(=O)(=O)C(C([O-])=O)CC([O-])=O JMGZBMRVDHKMKB-UHFFFAOYSA-L 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- 150000004665 fatty acids Chemical class 0.000 claims description 3
- 125000005456 glyceride group Chemical group 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- LISIOKIJVNSIGF-UHFFFAOYSA-N CCCN.CN(C)CC(O)=O Chemical compound CCCN.CN(C)CC(O)=O LISIOKIJVNSIGF-UHFFFAOYSA-N 0.000 claims description 2
- 235000019864 coconut oil Nutrition 0.000 claims description 2
- 239000003240 coconut oil Substances 0.000 claims description 2
- 239000012153 distilled water Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000344 soap Substances 0.000 abstract description 26
- 206010061218 Inflammation Diseases 0.000 abstract description 2
- 244000269722 Thea sinensis Species 0.000 abstract 1
- 230000004054 inflammatory process Effects 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000004898 kneading Methods 0.000 description 16
- 238000012360 testing method Methods 0.000 description 9
- 239000003153 chemical reaction reagent Substances 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 8
- 230000001580 bacterial effect Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 241000222122 Candida albicans Species 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 238000000227 grinding Methods 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 238000000465 moulding Methods 0.000 description 5
- 235000015097 nutrients Nutrition 0.000 description 5
- 235000013599 spices Nutrition 0.000 description 5
- 241000588724 Escherichia coli Species 0.000 description 4
- 241000191967 Staphylococcus aureus Species 0.000 description 4
- 229940095731 candida albicans Drugs 0.000 description 4
- 238000010790 dilution Methods 0.000 description 4
- 239000012895 dilution Substances 0.000 description 4
- 239000001963 growth medium Substances 0.000 description 4
- 241000194017 Streptococcus Species 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000002401 inhibitory effect Effects 0.000 description 3
- 239000002609 medium Substances 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- MPDGHEJMBKOTSU-YKLVYJNSSA-N 18beta-glycyrrhetic acid Chemical compound C([C@H]1C2=CC(=O)[C@H]34)[C@@](C)(C(O)=O)CC[C@]1(C)CC[C@@]2(C)[C@]4(C)CC[C@@H]1[C@]3(C)CC[C@H](O)C1(C)C MPDGHEJMBKOTSU-YKLVYJNSSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical class [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 2
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 241000193990 Streptococcus sp. 'group B' Species 0.000 description 2
- 244000309466 calf Species 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 235000013922 glutamic acid Nutrition 0.000 description 2
- 239000004220 glutamic acid Substances 0.000 description 2
- 230000002949 hemolytic effect Effects 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
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- 239000000126 substance Substances 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- PANIBUVGEJDJGE-UHFFFAOYSA-N 2-(2-sulfophenoxy)benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1OC1=CC=CC=C1S(O)(=O)=O PANIBUVGEJDJGE-UHFFFAOYSA-N 0.000 description 1
- 229920001817 Agar Polymers 0.000 description 1
- 238000009631 Broth culture Methods 0.000 description 1
- 206010007134 Candida infections Diseases 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- MPDGHEJMBKOTSU-UHFFFAOYSA-N Glycyrrhetinsaeure Natural products C12C(=O)C=C3C4CC(C)(C(O)=O)CCC4(C)CCC3(C)C1(C)CCC1C2(C)CCC(O)C1(C)C MPDGHEJMBKOTSU-UHFFFAOYSA-N 0.000 description 1
- 241001299553 Ilex chinensis Species 0.000 description 1
- 241001100935 Ilex purpurea Species 0.000 description 1
- 235000003366 Ilex purpurea Nutrition 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- 239000006159 Sabouraud's agar Substances 0.000 description 1
- 241000191940 Staphylococcus Species 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- WDJHALXBUFZDSR-UHFFFAOYSA-N acetoacetic acid Chemical compound CC(=O)CC(O)=O WDJHALXBUFZDSR-UHFFFAOYSA-N 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 201000003984 candidiasis Diseases 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- KKGXXVNMUUFEDZ-UHFFFAOYSA-L disodium;2-sulfonatododecanoate Chemical compound [Na+].[Na+].CCCCCCCCCCC(C([O-])=O)S([O-])(=O)=O KKGXXVNMUUFEDZ-UHFFFAOYSA-L 0.000 description 1
- 229960003720 enoxolone Drugs 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- -1 ethanol amide Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000006916 nutrient agar Substances 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 125000002730 succinyl group Chemical group C(CCC(=O)*)(=O)* 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- UZVUJVFQFNHRSY-OUTKXMMCSA-J tetrasodium;(2s)-2-[bis(carboxylatomethyl)amino]pentanedioate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CC[C@@H](C([O-])=O)N(CC([O-])=O)CC([O-])=O UZVUJVFQFNHRSY-OUTKXMMCSA-J 0.000 description 1
- 238000012549 training Methods 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0203—Solvent extraction of solids with a supercritical fluid
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2096—Heterocyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D2011/007—Extraction using a solvent in the gas phase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/123—Sulfonic acids or sulfuric acid esters; Salts thereof derived from carboxylic acids, e.g. sulfosuccinates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention provides a tea tree essential oil extracting method, comprising the steps: selecting fresh tea leaves and fresh tender shoots, adding to a CO2 supercritical extractor, using ethanol as an entrainer accounting for 4-6% by weight of a total extracting solvent, extracting under a pressure of 15-30 Mpa, at a temperature of 30-50 DEG C and at a CO2 flow of 1-3 ml/g raw drug per min, and extracting for 150-180 min to obtain the tea tree essential oil; soap made with the tea tree essential oil can diminish inflammation, is effective to use and is handy.
Description
Technical field
The present invention relates to extracting method and the tea tree ethereal oil compositions of a kind of tea tree ethereal oil, belong to chemical technology field.
Background technology
Along with the raising of people's living standard, the demand for fancy soap is more and more higher, extensively sells in the market
Fancy soap, major part utilizes chemicals to make, and easily causes skin allergy, also has other some side effect, Er Qie
The most costly, be not suitable for using in a large number, skin is had the less of protective effect, the fat even can secreted by skin
Fat protective ingredient washes, so that skin is the driest, and serious meeting injury skin.Many fancy soap skin comfort degree, moisten
Degree aspect effect is bad, does not has antiinflammation.
Summary of the invention
Goal of the invention: it is an object of the invention to provide extracting method and the tea tree ethereal oil compositions of a kind of tea tree ethereal oil.
Technical scheme: it is an object of the invention to by following scheme realization:
The extracting method of a kind of tea tree ethereal oil, step is: selects fresh leaf of tea tree and the fresh tender tip, joins
In CO2 supercritical extraction device, ethanol is as entrainer, and it is 4-6% that entrainer accounts for the percent by volume of total extractant, extraction pressure
Power 15-30MPa, temperature 30-50 DEG C, CO2 flow 1-3m1/g crude drug min, extraction time 150-180min, obtain tea tree ethereal oil.
The extracting method of described tea tree ethereal oil, described CO2 supercritical extraction entrainer accounts for the volume basis of total extractant
Ratio is 5%.
The extracting method of described tea tree ethereal oil, extracting pressure 20MPa of described CO2 supercritical extraction, temperature 40 DEG C, CO2
Flow 2ml/g crude drug min, extraction time 160min.
A kind of tea tree ethereal oil compositions, is prepared by the raw materials in: the tea tree ethereal oil that said method prepares
2-4 part, oroxylin 2-4 part, luteolin 1-3 part, cetyl sulfophenoxy benzenesulfonic acid disodium salt 10-20 part, Cortex cocois radicis
Fatty acid oil single ethanol amide 8-10 part, N-cocamidopropyl propyl amide-N, N-dimethylglycine inner salt 10-16 part, hydrogenated cotton seeds
Oil glyceride disodium sulfosuccinate salt 10-14 part, decanoyl/octanoyl glycerides 2-4 part, distilled water 20-30 part.
Tea tree ethereal oil compositions is fancy soap, preparation method, containing following steps:
(a) kneading spice: the various raw materials of said components are weighed in proportion in the kneading machine joining conventional soapmaking,
Kneading is uniformly mixed.B () grinds: the material after kneading being uniformly mixed, and enters in grinder, carries out soap body and grind
Mill.C () vacuum press strip: the soap body after grinding, enters vacuum plodder, carries out vacuum press strip.D () prints: plodder extrudes
Strip soap body be directly entered printer print, obtain the soap body of molding.
Tea tree ethereal oil is purchased from Guangdong Fuyang Biotechnology Co., Ltd., and oroxylin (90%), luteolin (85%) are purchased
From bio tech ltd of AOC, Shaanxi.
Cetyl sulfophenoxy benzenesulfonic acid disodium salt, CA registration number: 65143-89-7, molecular formula is
C28H42O7S2.2Na, English name: 51842Hexadecyl (sulfophenoxy) benzenesulfonic acid,
disodium salt。
Coconut oil fatty acid monoethanolamide CA registration number: 68140-00-1.
N-cocamidopropyl propyl amide-DMG inner salt, CA registration number: 86438-79-1, molecular formula is
C19H38N2O3。
Hydrogenated cotton seeds oil glyceride disodium sulfosuccinate salt, trade name: Emcol 4072Coemulsifier, the U.S.
Witco company produces.
Succinyl glycyrrhetinic acid disodium, cas number: 38841-48-4
Glutamic acid diacetic acid four sodium, cas number: 51981-21-6, molecular formula is C9H9NNa4O8, English name: 16896L-
Glutamic acid,N,N-bis(carboxymethyl)-,sodium salt(1:4)。
Decanoyl/octanoyl glycerides, cas number: 65381-09-1, English name: 45755Decanoyl/octanoyl-
glycerides。
Above-mentioned surfactant, antioxidant, chelating agen raw material are purchased from Shanghai Fei Ge Chemical Co., Ltd..
Beneficial effect: the fancy soap of the present invention, fine and smooth stable, performance is gentle, low to the zest of skin, is especially added with other
After extract, more can play antiinflammation, the feature of environmental protection is good, and using effect is good and convenient.
Detailed description of the invention
Form by the following examples, is described in further detail the foregoing of the present invention again, but should be by this
Being interpreted as that the scope of the above-mentioned theme of the present invention is only limitted to Examples below, all technology realized based on foregoing of the present invention are equal
Belong to the scope of the present invention.
1, combining detailed description of the invention, the present invention is further described as follows:
Table 1 various embodiments of the present invention needed raw material, unit: g
2, preparation embodiment
Embodiment 1: the preparation of tea tree ethereal oil: select fresh leaf of tea tree and fresh tender tip 10kg, joins CO2 and surpasses
In critical extractor, ethanol is as entrainer, and it is 5% that entrainer accounts for the percent by volume of total extractant, extracting pressure
20MPa, temperature 40 DEG C, CO2 flow 2m1/g crude drug min, extraction time 160min, obtain tea tree ethereal oil.
Embodiment 2: preparing raw material by upper table, preparation method, containing following steps: (a) kneads spice: by said components
Various raw materials (tea tree ethereal oil is prepared by above-described embodiment 1 method) weigh the kneading machine joining conventional soapmaking in proportion
In, kneading is uniformly mixed.B () grinds: the material after kneading being uniformly mixed, and enters in grinder, carries out soap body
Grind.C () vacuum press strip: the soap body after grinding, enters vacuum plodder, carries out vacuum press strip.D () prints: plodder pressure
The strip soap body gone out is directly entered printer and prints, and obtains the soap body of molding.
Embodiment 3: by upper table, prepares raw material, and preparation method, containing following steps: (a) kneads spice: by said components
Various raw materials (tea tree ethereal oil is prepared by above-described embodiment 1 method) weigh the kneading joining conventional soapmaking in proportion
In machine, kneading is uniformly mixed.B () grinds: the material after kneading being uniformly mixed, and enters in grinder, carries out soap
Body grinds.C () vacuum press strip: the soap body after grinding, enters vacuum plodder, carries out vacuum press strip.D () prints: plodder
The strip soap body extruded is directly entered printer and prints, and obtains the soap body of molding.
Embodiment 4: by upper table, prepares raw material, and preparation method, containing following steps: (a) kneads spice: by said components
Various raw materials (tea tree ethereal oil is prepared by above-described embodiment 1 method) weigh the kneading joining conventional soapmaking in proportion
In machine, kneading is uniformly mixed.B () grinds: the material after kneading being uniformly mixed, and enters in grinder, carries out soap
Body grinds.C () vacuum press strip: the soap body after grinding, enters vacuum plodder, carries out vacuum press strip.D () prints: plodder
The strip soap body extruded is directly entered printer and prints, and obtains the soap body of molding.
Embodiment 5: by upper table, prepares raw material, and preparation method, containing following steps: (a) kneads spice: by said components
Various raw materials (tea tree ethereal oil is prepared by above-described embodiment 1 method) weigh the kneading joining conventional soapmaking in proportion
In machine, kneading is uniformly mixed.B () grinds: the material after kneading being uniformly mixed, and enters in grinder, carries out soap
Body grinds.C () vacuum press strip: the soap body after grinding, enters vacuum plodder, carries out vacuum press strip.D () prints: plodder
The strip soap body extruded is directly entered printer and prints, and obtains the soap body of molding.
3, effect example
Test one: the present invention affects result of the test to staphylococcus aureus etc..
Test material: (1) medicine and reagent are by reagent: prepare tea tree ethereal oil combination by preparation embodiment 2-5 method
Thing；Sodium chloride: the long hundred million chemical reagent company limiteies in Shanghai, lot number: 00090130.Nutrient broth medium: upper marine section insecticide
Biotechnology development corporation, Ltd., lot number: 130616.Nutrient agar: Jiangsu Prov. Disease Preventing and Controlling Center's microorganism
Chemical reagent work, lot number: 130026.Improvement Martin's culture medium: sky, Hangzhou and microorganism reagent company limited, lot number: 130731.Improvement
Martin's culture medium: Beijing three medicine scientific and technological development company, lot number: 131023；Sabouraud's agar: CIQ science is ground
Jiu Yuan Beijing Luqiao Technology Co., Ltd., lot number: 1208156；Calf serum, Hangzhou Ilex purpurea Hassk.[I.chinensis Sims biological engineering material is limited
Company, lot number: 130808；De-fine Sheep Blood, purchased from Jiangning county epidemic prevention station, lot number: 130712 (2) bacterial strain reference cultures: golden yellow
Color staphylococcus (ATCC25923), escherichia coli (441490), beta hemolytic streptococcus (32210), Candida albicans
(98100) provided by Jiangsu Province Disease epizootic prevention center microorganism reagent factory.(3) instrument and equipment electronic balance, Beijing plug is many
Li Si balance company limited produces；Full-automatic high-pressure autoclave, Japan SANYO；Superclean bench, Suzhou Decontamination Equipment Plant；
SHP-80 biochemical cultivation case, Shanghai is gloomy reliable tests Instrument Ltd.
Experimental technique: (1) antibacterial culturing: take reference culture: staphylococcus aureus (ATCC25923), escherichia coli
(441490), beta hemolytic streptococcus (32210) bacterial strain a little, be inoculated in respectively in nutrient broth medium, 37 DEG C of cultivations
18h.(adding 20% calf serum in group B streptococcus broth bouillon) takes each bacterial strain nutrient broth culture that 18h cultivates, and uses
Nutrient broth makees 10-3Dilution is used for testing.Extracting waste candidiasis bacterial strain is a little, is inoculated in improvement Martin's culture medium, 35 DEG C of trainings
Support 24h.Take the Candida albicans culture that 24h cultivates, be used for testing with improvement Martin's culture medium 10-3 dilution.(2) two times dilute
Interpretation of the law (test tube method): take sterilizing test tubes 11, the 1st pipe adds nutrient broth fluid medium 1.6ml, remaining every pipe 1ml, respectively
Taking and added in the first pipe by reagent diluent 0.4ml, take 1ml to the 2nd pipe, dilute successively after mixing, the 10th pipe sucking-off 1ml abandons
Going, the 11st pipe is not added with medicinal liquid as comparison.Often pipe adds dilution bacterium solution 0.1ml, cultivates 24h for 37 DEG C.Take out and observe bacterial growth
Situation.As drug liquid tube is muddy, i.e. represent bacterial growth, for reagent thing without bacteriostasis；Then expression antibacterial as limpid in drug liquid tube is raw
Length is suppressed, the medicinal liquid of the greatest dilution of its energy bacteria growing inhibiting, is the minimal inhibitory concentration (MIC) of this medicine.
By limpid medicinal liquid meat soup each pipe transferred species broth agar plates, cultivating 24h and observe, still the minimum drug level without bacterial growth is
Bacteriocidal concentration for this medicine.
Experimental result: being shown in Table 2, antibacterial activity in vitro of the present invention (n=2), unit is: (g is raw for minimum inhibitory concentration (MIC)
Medicine/g).
Table 2 embodiment of the present invention 2-5 anti-inflammation test
| Sample source | Staphylococcus aureus | Escherichia coli | Group B streptococcus | Candida albicans |
| Embodiment 2 | 0.1 | 0.05 | 0.1 | 0.1 |
| Embodiment 3 | 0.4 | 0.5 | 0.6 | 0.5 |
| Embodiment 4 | 0.6 | 0.4 | 0.7 | 0.6 |
| Embodiment 5 | 0.7 | 0.3 | 0.2 | 0.4 |
Table 2 shows: embodiment 2-5 is to staphylococcus aureus (ATCC25923), escherichia coli (441490), B-mode molten
Courageous and upright streptococcus (32210), Candida albicans are respectively provided with stronger bacteriostasis；Wherein embodiment 2 is better than embodiment 3-5, says
Bright tea tree ethereal oil, oroxylin, luteolin compatibility using effect are more preferable.
Claims (4)
1. the extracting method of a tea tree ethereal oil, it is characterised in that step is: select fresh leaf of tea tree and fresh tender
The tip, joins CO2In supercritical extraction device, ethanol is as entrainer, and it is 4-that entrainer accounts for the percent by volume of total extractant
6%, extracting pressure 15-30MPa, temperature 30-50 DEG C, CO2Flow 1-3m1/g crude drug min, extraction time 150-180min,
Obtain tea tree ethereal oil.
The extracting method of tea tree ethereal oil the most according to claim 1, it is characterised in that described CO2Supercritical extraction entrainer accounts for
The percent by volume of total extractant is 5%.
The extracting method of tea tree ethereal oil the most according to claim 1, it is characterised in that described CO2The extraction pressure of supercritical extraction
Power 20MPa, temperature 40 DEG C, CO2Flow 2ml/g crude drug min, extraction time 160min.
4. a tea tree ethereal oil compositions, it is characterised in that be prepared by the raw materials in: claim 1 prepares
Tea tree ethereal oil 2-4 part, oroxylin 2-4 part, luteolin 1-3 part, cetyl sulfophenoxy benzenesulfonic acid disodium salt 10-
20 parts, coconut oil fatty acid monoethanolamide 8-10 part, N-cocamidopropyl propyl amide-N, N-dimethylglycine inner salt 10-16 part,
Hydrogenated cotton seeds oil glyceride disodium sulfosuccinate salt 10-14 part, decanoyl/octanoyl glycerides 2-4 part, distilled water 20-30 part.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106344476A (en) * | 2016-11-08 | 2017-01-25 | 全椒先奇医药科技有限公司 | Perfume and preparation method thereof |
| CN106929156A (en) * | 2017-04-12 | 2017-07-07 | 四川艾朗特生物科技有限公司 | A kind of Australia tea tree Essential oil extraction method |
| CN107812069A (en) * | 2017-11-08 | 2018-03-20 | 广州市桐晖药业有限公司 | Hexanicit topical composition and preparation method thereof |
| CN108034501A (en) * | 2017-12-30 | 2018-05-15 | 刘莹艳 | A kind of essential oil gel and preparation method thereof |
| CN108125876A (en) * | 2017-12-24 | 2018-06-08 | 宁国平衡健康管理有限公司 | A kind of Xuancheng's pawpaw mouthwash and preparation method thereof |
| WO2019056919A1 (en) * | 2017-09-25 | 2019-03-28 | 嘉必优生物技术（武汉）股份有限公司 | Microbial oil containing low chloropropanol and preparation method thereof |
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| CN104830538A (en) * | 2015-05-25 | 2015-08-12 | 江苏耐雀生物工程技术有限公司 | Method of extracting tea tree essential oil from tea trees |
| CN105062691A (en) * | 2015-09-28 | 2015-11-18 | 朱翠帮 | Extraction method of tea tree essential oil |
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| CN104830538A (en) * | 2015-05-25 | 2015-08-12 | 江苏耐雀生物工程技术有限公司 | Method of extracting tea tree essential oil from tea trees |
| CN105062691A (en) * | 2015-09-28 | 2015-11-18 | 朱翠帮 | Extraction method of tea tree essential oil |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106344476A (en) * | 2016-11-08 | 2017-01-25 | 全椒先奇医药科技有限公司 | Perfume and preparation method thereof |
| CN106929156A (en) * | 2017-04-12 | 2017-07-07 | 四川艾朗特生物科技有限公司 | A kind of Australia tea tree Essential oil extraction method |
| WO2019056919A1 (en) * | 2017-09-25 | 2019-03-28 | 嘉必优生物技术（武汉）股份有限公司 | Microbial oil containing low chloropropanol and preparation method thereof |
| CN107812069A (en) * | 2017-11-08 | 2018-03-20 | 广州市桐晖药业有限公司 | Hexanicit topical composition and preparation method thereof |
| CN108125876A (en) * | 2017-12-24 | 2018-06-08 | 宁国平衡健康管理有限公司 | A kind of Xuancheng's pawpaw mouthwash and preparation method thereof |
| CN108034501A (en) * | 2017-12-30 | 2018-05-15 | 刘莹艳 | A kind of essential oil gel and preparation method thereof |
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Application publication date: 20161012 |