CN105919903A - Herbal preservative composition, freckle-removing facial mask and preparation method of freckle-removing facial mask - Google Patents
Herbal preservative composition, freckle-removing facial mask and preparation method of freckle-removing facial mask Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/985—Skin or skin outgrowth, e.g. hair, nails
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- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
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- A61Q19/00—Preparations for care of the skin
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses a herbal preservative composition. The composition is characterized by being prepared from a herbal active ingredient with butanediol and pentanediol which are synergized to achieve a bacterium inhibiting effect, wherein the herbal active ingredient comprises xanthoxylum piperitum fruit extract, pulsatilla koreana nakai extract and usnea barbata extract. The invention further discloses a freckle-removing facial mask and a preparation method thereof. The facial mask is prepared from the herbal preservative composition, polyvinyl alcohol crosslinked polymer, ethanol, papain, donkey-hide gelatin, ginseng root extract, herba leonuri extract, licorice root extract, radix sophorae extract, gingko leaf extract, scutellaria baicalensis extract, stephania tetrandra extract, carbomer and deionized water. The herbal preservative composition does not contain conventional chemical preservative, does not irritate human bodies, does not have toxic or side effect, cannot cause allergy, and has a good preservative effect. The herbal preservative composition has the effect of safely removing freckles and prolonging the preservation period of products when being applied to traditional Chinese medicine freckle-removing facial masks.
Description
Technical field
The invention belongs to cosmetics additive technical field, be specifically related to a kind of plant antiseptic agent compositions, freckle-removing mask
And freckle-removing mask preparation method.
Background technology
Containing abundant aminoacid, protein, collagen, vitamin, moisture etc. in cosmetics, these maintenance compositions are the most also
It is antibacterial, microbial growth " Nutrient medium ", it is therefore desirable in cosmetics, add preservative such that it is able to maintenance for a long time
The quality of cosmetic.In general, the moisture of cosmetics is the highest, and rotten probability is the biggest, more needs to add preservative.Face
Film is a kind of product that in cosmetics, water content is bigger, and therefore the interpolation of preservative is the most more.Owing to conventional chemosynthesis is prevented
Rotten agent has higher zest to skin, is favored the natural antiseptic agent that skin is non-stimulated by people.But natural antiseptic agent
The color is too dark and raw material is highly seasoned for a part for raw material, broad spectrum antibacterial relatively chemical preservative is poor, and the activity in plant extract
Composition to light, heat, oxygen physical stability low, can not fully keep its antiseptic activity during circulating, limit natural anti-
The use of rotten agent.
In numerous skin problems, the problem causing the biggest puzzlement to people is mottle.The producing cause of mottle
Have following several: life stress is big, hormone imbalance, metabolism are smooth, the ultraviolet radiation in daylight, cosmetics make
With improper etc..Present speckle dispelling product, based on chemical addition agent, is cured the symptoms, not the disease, easily bounce-back after disabling, and life-time service
Again can injured skin naturally elasticity and gloss.Some people there is also the phenomenon of skin allergy, skin ageing, to skin
Cause certain injury, bring painful and heavy financial burden to consumer.
Summary of the invention
One of the technical problem to be solved in the present invention is to provide a kind of plant antiseptic agent compositions, and this plant antiseptic agent combines
The main active of thing comes from natural plants, has been equipped with butanediol and the pentanediol of collaborative bacteriostasis, without routinizing
Learn preservative, non-stimulated to human body, have no side effect, it is not result in allergy, and promotes mutually between each composition, collaborative play
Effect, can effective bacteriostasis and sterilization；Another problem that the invention solves the problems that is to provide a kind of containing plant antiseptic agent compositions
Freckle-removing mask, this facial film be mainly composed of Chinese medicine extract, be possible not only to play safe freckle effect, also extend product
Shelf-life.
One aspect of the present invention provides a kind of plant antiseptic agent compositions, and described compositions has been equipped with by active components of plants
Butanediol and the pentanediol of collaborative bacteriostasis combine, and described active components of plants includes that prickly ash berries extract, Korea are white
Head father-in-law's extract, palpus extractive of usnea, described prickly ash berries extract, pasque flower extract, the weight of palpus extractive of usnea
Proportioning is 2:1～3:1～3；Described active components of plants, butanediol, the weight proportion of pentanediol be 0.03～3:5～10:3～
5；
Described prickly ash berries extract is prepared as follows: according to the ratio of every gram of prickly ash berries 25mL Extraction solvent,
Adding the ethanol extraction solvent that concentration is 80% in cleaning the prickly ash berries after drying, 80～85 ° are incubated reflux, extract, 1～2h,
Cooling, centrifugal, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described pasque flower extract is prepared as follows: according to every gram of pasque flower 25mL Extraction solvent
Ratio, adds the ethanol extraction solvent that concentration is 80% in cleaning the pasque flower after drying, and 80～85 ° of insulation backflows carry
Taking 1～2h, cool down, be centrifuged, filter, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described must be prepared as follows by extractive of usnea: according to every gram must the ratio of Usnea 25mL Extraction solvent,
Clean and the palpus Usnea after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cold
But, it is centrifuged, filters, the extracting solution concentrating under reduced pressure after filtration, lyophilization preservation；
Another aspect of the present invention provides a kind of freckle-removing mask, and containing plant antiseptic agent compositions, described compositions is by plant
Active component has been equipped with the butanediol of collaborative bacteriostasis and pentanediol combines, and described active components of plants includes prickly ash berries
Extract, pasque flower extract, palpus extractive of usnea, described prickly ash berries extract, pasque flower extract, palpus Usnea
The weight proportion of extract is 2:1～3:1～3；In terms of the gross weight of facial film, described active components of plants weight in facial film
Percentage ratio is 0.03～3%, and butanediol percentage by weight in facial film is 5～10%, pentanediol quality hundred in facial film
Proportion by subtraction is 3～5%；
Described prickly ash berries extract is prepared as follows: according to the ratio of every gram of prickly ash berries 25mL Extraction solvent,
Adding the ethanol extraction solvent that concentration is 80% in cleaning the prickly ash berries after drying, 80～85 ° are incubated reflux, extract, 1～2h,
Cooling, centrifugal, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described pasque flower extract is prepared as follows: according to every gram of pasque flower 25mL Extraction solvent
Ratio, adds the ethanol extraction solvent that concentration is 80% in cleaning the pasque flower after drying, and 80～85 ° of insulation backflows carry
Taking 1～2h, cool down, be centrifuged, filter, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described must be prepared as follows by extractive of usnea: according to every gram must the ratio of Usnea 25mL Extraction solvent,
Clean and the palpus Usnea after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cold
But, it is centrifuged, filters, the extracting solution concentrating under reduced pressure after filtration, lyophilization preservation；
Other components of described facial film and weight percentage are as follows:
Polyvinyl alcohol crosslinked polymer 10～15%
Ethanol 3～5%
Papain 0.6～1%
Colla Corii Asini 4～10%
Radix Ginseng extract 0.5～0.8%
Herba Leonuri extract 5～8%
Licorice root extract 5～8%
Radix sophorae extract 5～8%
Folium Ginkgo extract 0.5～5%
Radix Scutellariae extract 2～5%
Stephania tetrandra extract 0.1～1%
Carbomer 0.05～0.2%
Remaining is deionized water.
Said components effect in prescription is as follows:
Polyvinyl alcohol crosslinked polymer: film former；
Ethanol: antiinflammatory, convergence pore；
Papain: be called for short carase, extracts from Fructus Caricae fruit and obtains, and carase is prone to and forms the black of mottle
Copper ion in pigment forms complex, reduces melanic formation and removes the melanin of mottle, and the three of carase hydrolysis
Titanium material can directly suppress to form melanic TYR activity, eliminates Free Radical, thus reaches the effect of whitening and speckle dispelling；
Colla Corii Asini: can supplement skin collagen, suppresses melanic formation, moreover it is possible to stimulate body cell to produce glutathion
And superoxide dismutase, and superoxide dismutase can scavenging activated oxygen, there is antitumor, defying age, whitening, speckle dispelling
Effect；
Radix Ginseng extract: there is extremely strong oxidation resistance, and there is flat wrinkle of comforting, blood circulation promoting, strengthen skin
Skin nutrition, accelerates the multi-efficiency such as metabolism, can effectively nurse one's health skin, prevents skin dehydration, hardening, wrinkling, Radix Ginseng simultaneously
Active substance also has the melanic reducing property of suppression, makes skin pure white smooth；
Herba Leonuri extract: containing the trace element such as selenium and manganese, can antioxidation, anti-aging；
Licorice root extract: by multiple enzyme in suppression melanin forming process (such as tryrosinase and dopachrome change
Enzyme) activity, reach the effect of whitening, speckle dispelling；
Radix sophorae extract: whitening, antiinflammatory, anti-acne, antibacterial etc.；
Folium Ginkgo extract: the pyrite composition contained in Folium Ginkgo can hinder pigment in the formation of genuine piece layer with calm,
Reach the effect of skin whitening and preventing and treating mottle；And pyrite composition is the street cleaner of free radical, can protect skin corium cell, change
Kind blood circulation, prevents cell oxidized generation wrinkle；
Radix Scutellariae extract: the flavone compound contained in Radix Scutellariae extract can absorb ultraviolet, scavenging activated oxygen, again
Melanic generation can be suppressed, there is the effect of defying age, whitening, speckle dispelling；
Stephania tetrandra extract: antiallergic；
Carbomer: thickening agent.
Further, the pH value of described freckle-removing mask regulates to 5～6 with the potassium hydroxide solution of 10%, makes the acid of facial film
Basicity is close with skin.
Further, described Radix Ginseng extract, Herba Leonuri extract, licorice root extract, radix sophorae extract, Semen Ginkgo
Leaf extract, Radix Scutellariae extract raw material respectively with 80% ethanol insulation reflux, extract, 1～2h, be centrifuged, filter, filter after carry
Take liquid to be evaporated to 5 times of concentration and obtain extract.
Present invention also offers the preparation method of a kind of freckle-removing mask, comprise the following steps:
(1) polyvinyl alcohol crosslinked polymer is added in deionized water, is heated to 80 ° of dissolvings,；
(2) keep said temperature, carbomer is slowly added in (1) while stirring, to carbomer complete swelling, fully divides
Dissipate in (1)；
(3) with 10% potassium hydroxide solution regulation pH to 5～6, start cooling, when temperature is down to 40 °, ethanol is added
(2) in stirring, add subsequently Colla Corii Asini, Radix Ginseng extract, Herba Leonuri extract, licorice root extract, radix sophorae extract,
Folium Ginkgo extract, Radix Scutellariae extract, stephania tetrandra extract, plant antiseptic agent compositions, stir and i.e. obtain facial mask liquid.
It is an advantage of the current invention that:
1, the plant antiseptic agent compositions of the present invention uses natural plant active component to be equipped with butanediol and pentanediol combination
Form, without conventional chemical preservative, non-stimulated to human body, have no side effect, it is not result in allergy, wherein, prickly ash berries contains
There is multiple unsaturated fatty acid, there is local anesthesia and resist escherichia coli, dysentery bacterium, corynebacterium, dermatophytes etc.
Effect；Pasque flower have antitumor, strengthen immunologic function, antiinflammatory, resisting pathogenic microbes, parasiticide, protect the liver, toxicity and
The effects such as work such as treatment endotoxemia；Must Usnea be a kind of natural extract from lichens tree, its main component Usnea
Acid is considered as a kind of potent antibiotic and antibacterial, prevents carefully as natural antiseptic agent in cosmetics and personal care articles
Bacterium and fungus growth, it has broad-spectrum antiseptic effect, is believed to be effective against all of gram positive bacteria and pulmonary tuberculosis
Bacterium.By prickly ash berries extract, pasque flower extract, must combine by extractive of usnea, promote mutually between each composition,
Collaborative play effect, can effective bacteriostasis and sterilization.Although three of the above active components of plants can be with bacteriostasis and sterilization, but effect is not
The strongest, in the plant antiseptic agent compositions of the present invention, therefore compound butanediol and pentanediol, make bactericidal and bacteriostatic effect best.
2, described plant antiseptic agent compositions is applied in the freckle-removing mask that active ingredient of Chinese herbs develops by the present invention,
Do not only reach the effect of safe speckle dispelling, also made freckle effect be strengthened, and extend the shelf-life of product.
3, the freckle-removing mask of the present invention is by papain, Colla Corii Asini, Radix Ginseng extract, Herba Leonuri extract, licorice
Extract, radix sophorae extract, Folium Ginkgo extract, each active component of Radix Scutellariae extract configure by a certain percentage and form, to black
Pigment has coordinate repression, the most also has the effect of defying age, whitening.
Detailed description of the invention
Be below the non-limiting examples of the present invention, these embodiments be only given for illustrative purposes, not
It is understood that as limitation of the invention.Based on the embodiment in the present invention, those of ordinary skill in the art are not making creation
The every other embodiment obtained under property work premise, broadly falls into the scope of protection of the invention.
Embodiment one
A kind of plant antiseptic agent compositions, including prickly ash berries extract, pasque flower extract, palpus extractive of usnea,
Described prickly ash berries extract, pasque flower extract, the weight proportion of palpus extractive of usnea are 1:1:1；
Described prickly ash berries extract is prepared as follows: according to the ratio of every gram of prickly ash berries 25mL Extraction solvent,
Adding the ethanol extraction solvent that concentration is 80% in cleaning the prickly ash berries after drying, 80～85 ° are incubated reflux, extract, 1～2h,
Cooling, centrifugal, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described pasque flower extract is prepared as follows: according to every gram of pasque flower 25mL Extraction solvent
Ratio, adds the ethanol extraction solvent that concentration is 80% in cleaning the pasque flower after drying, and 80～85 ° of insulation backflows carry
Taking 1～2h, cool down, be centrifuged, filter, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described must be prepared as follows by extractive of usnea: according to every gram must the ratio of Usnea 25mL Extraction solvent,
Clean and the palpus Usnea after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cold
But, it is centrifuged, filters, the extracting solution concentrating under reduced pressure after filtration, lyophilization preservation.
Embodiment two
A kind of plant antiseptic agent compositions, has been equipped with butanediol and the pentanediol of collaborative bacteriostasis by active components of plants
Combining, described active components of plants includes prickly ash berries extract, pasque flower extract, palpus extractive of usnea, described
Prickly ash berries extract, pasque flower extract, palpus extractive of usnea, butanediol, the weight proportion of pentanediol are 1:1:1:6:
4；
Described prickly ash berries extract, pasque flower extract, the preparation method of palpus extractive of usnea and embodiment one phase
With.
Embodiment three
A kind of freckle-removing mask, containing plant antiseptic agent compositions, described compositions includes prickly ash berries extract, towards Common Squill Bulb
Father-in-law's extract, palpus extractive of usnea, in terms of the gross weight of facial film, prickly ash berries extract percentage by weight in facial film is 1%,
Pasque flower extract percentage by weight in facial film is 1%, must extractive of usnea percentage by weight in facial film be
1%；
Described prickly ash berries extract is prepared as follows: according to the ratio of every gram of prickly ash berries 25mL Extraction solvent,
Clean and the prickly ash berries after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cold
But, it is centrifuged, filters, the extracting solution concentrating under reduced pressure after filtration, lyophilization preservation；
Described pasque flower extract is prepared as follows: according to every gram of pasque flower 25mL Extraction solvent
Ratio, adds the ethanol extraction solvent that concentration is 80% in cleaning the pasque flower after drying, and 80～85 ° of insulation backflows carry
Taking 1～2h, cool down, be centrifuged, filter, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described must be prepared as follows by extractive of usnea: according to every gram must the ratio of Usnea 25mL Extraction solvent,
Clean and the palpus Usnea after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cold
But, it is centrifuged, filters, the extracting solution concentrating under reduced pressure after filtration, lyophilization preservation；
Other components of described facial film and weight percentage are as follows:
Polyvinyl alcohol crosslinked polymer 10～15%
Ethanol 3～5%
Papain 0.6～1%
Colla Corii Asini 4～10%
Radix Ginseng extract 0.5～0.8%
Herba Leonuri extract 5～8%
Licorice root extract 5～8%
Radix sophorae extract 5～8%
Folium Ginkgo extract 0.5～5%
Radix Scutellariae extract 2～5%
Stephania tetrandra extract 0.1～1%
Carbomer 0.05～0.2%
Remaining is deionized water.
The pH value of described freckle-removing mask regulates to 5～6 with the potassium hydroxide solution of 10%.
Described Radix Ginseng extract, Herba Leonuri extract, licorice root extract, radix sophorae extract, Folium Ginkgo extract,
The raw material of Radix Scutellariae extract respectively with 80% ethanol insulation reflux, extract, 1～2h, be centrifuged, filter, filter after extracting solution decompression
It is concentrated into 5 times of concentration and obtains extract.
Embodiment four
A kind of freckle-removing mask, containing plant antiseptic agent compositions, described compositions has been equipped with collaborative by active components of plants
Butanediol and the pentanediol of bacteriostasis combine, and described active components of plants includes prickly ash berries extract, pasque flower
Extract, palpus extractive of usnea, in terms of the gross weight of facial film, prickly ash berries extract percentage by weight in facial film is 1%, court
Common Squill Bulb father-in-law's extract percentage by weight in facial film is 1%, must extractive of usnea percentage by weight in facial film be
1%, butanediol percentage by weight in facial film is 6%, and pentanediol mass percent in facial film is 4%；
Described prickly ash berries extract, pasque flower extract, must extractive of usnea preparation method and embodiment one or
Embodiment three is identical, and other components and the weight percentage of described facial film are identical with embodiment three；
The pH value of described freckle-removing mask regulates to 5～6 with the potassium hydroxide solution of 10%.
Radix Ginseng extract, Herba Leonuri extract, licorice root extract, radix sophorae extract, Folium Ginkgo extract, Radix Scutellariae
The raw material of extract respectively with 80% ethanol insulation reflux, extract, 1～2h, be centrifuged, filter, filter after extracting solution concentrating under reduced pressure
Extract is obtained to 5 times of concentration.
Embodiment five
The preparation method of a kind of freckle-removing mask, comprises the following steps:
(1) polyvinyl alcohol crosslinked polymer is added in deionized water, is heated to 80 ° of dissolvings,；
(2) keep said temperature, carbomer is slowly added in (1) while stirring, to carbomer complete swelling, fully divides
Dissipate in (1)；
(3) with 10% potassium hydroxide solution regulation pH to 5～6, start cooling, when temperature is down to 40 °, ethanol is added
(2) in stirring, add subsequently Colla Corii Asini, Radix Ginseng extract, Herba Leonuri extract, licorice root extract, radix sophorae extract,
Folium Ginkgo extract, Radix Scutellariae extract, stephania tetrandra extract, plant antiseptic agent compositions, stir and i.e. obtain facial mask liquid.
Embodiment six
Bacteriostatic experiment
1, experiment material
Sample 1: the freckle-removing mask prepared according to the method for embodiment five, it contains polyvinyl alcohol crosslinked polymer 12%,
Ethanol 3%, papain 1%, Colla Corii Asini 10%, Radix Ginseng extract 0.8%, Herba Leonuri extract 5%, licorice root extract
5%, radix sophorae extract 6%, Folium Ginkgo extract 3%, Radix Scutellariae extract 4%, stephania tetrandra extract 0.8%, carbomer
0.1%, surplus is deionized water；
Sample 2: the freckle-removing mask prepared according to the method for embodiment five, its whole compositions containing sample 1 contain with percentage
Amount, possibly together with prickly ash berries extract 1%, pasque flower extract 1%, palpus extractive of usnea 1%；
Sample 3: the freckle-removing mask prepared according to the method for embodiment five, its whole compositions containing sample 1 contain with percentage
Outside amount, possibly together with butanediol 6%, pentanediol 4%；
Sample 4: the freckle-removing mask prepared according to the method for embodiment five, its whole compositions containing sample 1 contain with percentage
Outside amount, possibly together with prickly ash berries extract 1%, pasque flower extract 1%, palpus extractive of usnea 1%；Butanediol 6%, penta 2
Alcohol 4%.
2, experimental technique
Antibacterial (staphylococcus aureus, escherichia coli) is inoculated into lecithin Tween 80-nutrient agar respectively
Inclined-plane, cultivates 24h under 37 °；Mycete (candida albicans bacterium, aspergillus niger) inoculation Cha Shi fluid medium, cultivates under 25 °
5d.The appropriate four kinds of bacterium colonies of picking, are diluted to certain density bacteria suspension with physiological saline solution respectively, and bacterial suspension concentration is
1.0×106cfu/g。
Respectively above-mentioned four kinds of bacteria suspensions are coated on nutrient agar panel with aseptic cotton carrier and make lawn, then cut-off footpath
For the sterilizing filter paper dick of 3cm, after the most uniformly picking the facial film that 3 kinds of samples are made, then it is attached to four kinds of different bacteria suspensions respectively
On the flat board made, antibacterial and mycotic culture 7d, observed result.
3, evaluation methodology
Paper disk method bacteriostatic diameter >=10mm is that effectively bacteriostatic diameter ＜ 10mm is invalid.
4, experimental result is shown in Table 1
Table 1 paper disk method fungistatic effect
As shown in Table 1, without anticorrosive composite in sample 1, therefore fungistatic effect is worst；Sample 2, sample 3 and sample 4 add
Enter antiseptic composition, all show preferable bactericidal and bacteriostatic effect.By comparing discovery, add active components of plants
Prickly ash berries extract, pasque flower extract, sample 2 ratio of palpus extractive of usnea add the sample of butanediol and pentanediol
3 fungistatic effects are the most notable；And add prickly ash berries extract, pasque flower extract, must extractive of usnea, butanediol and
Sample 4 fungistatic effect of pentanediol is best, illustrate butanediol, pentanediol there was added collaborative fungistatic effect, make the plant of composition
Active component compounds the plant antiseptic agent compositions fungistatic effect of butanediol and pentanediol and reaches optimal.
Embodiment seven
Facial film speckle dispelling is tested
1, object select: choose age 25～40 years old, face has the women of the pigments such as chloasma in various degree, butterfly spot
200 examples, wherein 25～30 years old 100 example, 30～35 years old 50 example, 35～40 years old 50 example.
2, film sample: use the sample that the sample 1 in embodiment six and sample 4 are tested as this facial film speckle dispelling.
3, experimental technique: before sleep every night after cleaning skin, by the facial film uniform application of about 5g on the face, keep
20 minutes, now facial film film forming, throw off the facial film of film forming, clean residual liquor with clear water, use 6 months continuously.
4, curative effect determinate standard: be almost recovered: naked eyes disappear substantially depending on mottle；Effective: naked eyes depending on mottle disappear 60% with
On；Effective: naked eyes disappear more than 20% depending on mottle；Invalid: naked eyes disappear less than 20% depending on mottle.
Cure rate=recovery from illness number/total number of cases
Effective percentage=(recovery from illness number of cases+effective number of cases+effective number of cases)/total number of cases
5, therapeutic effect is shown in Table 2
Table 2 freckle-removing mask using effect statistical table
As can be seen from Table 2, sample 1 and sample 4 are respectively provided with preferable freckle effect to the women of 25～40 age brackets, have
Efficiency all reaches more than 84%.The freckle-removing mask effect of the age women application present invention between 25～30 years old is best, cures
Rate and effective percentage are above age women between 30～40 years old.Comparative sample 1 and sample 4, find containing plant antiseptic agent
The facial film freckle effect of compositions is more preferable, this some composition being likely due in plant antiseptic agent compositions and its in facial film
The coefficient result of his composition.
The above, be only presently preferred embodiments of the present invention, and the present invention not makees any pro forma restriction, every depends on
Any simple modification of being made above example according to the technical spirit of the present invention, equivalent variations, each fall within the protection of the present invention
Within the scope of.
Claims (5)
1. a plant antiseptic agent compositions, it is characterised in that described compositions has been equipped with collaborative antibacterial by active components of plants
Butanediol and the pentanediol of effect combine, and described active components of plants includes that prickly ash berries extract, pasque flower are extracted
Thing, palpus extractive of usnea, described prickly ash berries extract, pasque flower extract, the weight proportion of palpus extractive of usnea are 2:1
～3:1～3；Described active components of plants, butanediol, the weight proportion of pentanediol are 0.03～3:5～10:3～5；
Described prickly ash berries extract is prepared as follows: according to the ratio of every gram of prickly ash berries 25mL Extraction solvent, washing
Only the prickly ash berries after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cool down,
Centrifugal, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described pasque flower extract is prepared as follows: according to the ratio of every gram of pasque flower 25mL Extraction solvent
Example, adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, in cleaning the pasque flower after drying
1～2h, cool down, be centrifuged, filter, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described palpus extractive of usnea is prepared as follows: according to the ratio of every gram of palpus Usnea 25mL Extraction solvent, cleaning
After drying Usnea must add the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cooling, from
The heart, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves.
2. a freckle-removing mask, it is characterised in that containing plant antiseptic agent compositions, described compositions is joined by active components of plants
Combining with the butanediol and pentanediol playing collaborative bacteriostasis, described active components of plants includes prickly ash berries extract, court
Common Squill Bulb father-in-law's extract, must extractive of usnea, described prickly ash berries extract, pasque flower extract, must extractive of usnea
Weight proportion is 2:1～3:1～3；In terms of the gross weight of facial film, described active components of plants percentage by weight in facial film is
0.03～3%, butanediol percentage by weight in facial film is 5～10%, pentanediol mass percent in facial film be 3～
5%；
Described prickly ash berries extract is prepared as follows: according to the ratio of every gram of prickly ash berries 25mL Extraction solvent, washing
Only the prickly ash berries after drying adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cool down,
Centrifugal, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described pasque flower extract is prepared as follows: according to the ratio of every gram of pasque flower 25mL Extraction solvent
Example, adds the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, in cleaning the pasque flower after drying
1～2h, cool down, be centrifuged, filter, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Described palpus extractive of usnea is prepared as follows: according to the ratio of every gram of palpus Usnea 25mL Extraction solvent, cleaning
After drying Usnea must add the ethanol extraction solvent that concentration is 80%, 80～85 ° of insulation reflux, extract, 1～2h, cooling, from
The heart, filtration, the extracting solution concentrating under reduced pressure after filtration, lyophilization preserves；
Other components of described facial film and weight percentage are as follows:
Polyvinyl alcohol crosslinked polymer 10～15%
Ethanol 3～5%
Papain 0.6～1%
Colla Corii Asini 4～10%
Radix Ginseng extract 0.5～0.8%
Herba Leonuri extract 5～8%
Licorice root extract 5～8%
Radix sophorae extract 5～8%
Folium Ginkgo extract 0.5～5%
Radix Scutellariae extract 2～5%
Stephania tetrandra extract 0.1～1%
Carbomer 0.05～0.2%
Remaining is deionized water.
Freckle-removing mask the most according to claim 2, it is characterised in that the pH value of described freckle-removing mask with 10% hydroxide
Potassium solution regulates to 5～6.
Freckle-removing mask the most according to claim 2, it is characterised in that described Radix Ginseng extract, Herba Leonuri extract, sweet
Grass roots extract, radix sophorae extract, Folium Ginkgo extract, the raw material of Radix Scutellariae extract carry with 80% ethanol insulation backflow respectively
Take 1～2h, be centrifuged, filter, filter after extracting solution be evaporated to 5 times of concentration and obtain extract.
5. the preparation method of a freckle-removing mask, it is characterised in that comprise the following steps:
(1) polyvinyl alcohol crosslinked polymer is added in deionized water, be heated to 80 ° of dissolvings；
(2) keep said temperature, carbomer is slowly added in (1) while stirring, to carbomer complete swelling, is well dispersed in
(1) in；
(3) with 10% potassium hydroxide solution regulation pH to 5～6, start cooling, when temperature is down to 40 °, ethanol is added (2)
Middle stirring, adds Colla Corii Asini, Radix Ginseng extract, Herba Leonuri extract, licorice root extract, radix sophorae extract, silver subsequently
Folium Pruni extract, Radix Scutellariae extract, stephania tetrandra extract, plant antiseptic agent compositions, stir and i.e. obtain facial mask liquid.
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| CN110151660A (en) * | 2019-07-08 | 2019-08-23 | 北京书路一品文化发展有限公司 | A kind of eye-care condensation and preparation method thereof |
| CN110151660B (en) * | 2019-07-08 | 2022-07-12 | 北京书路一品文化发展有限公司 | Eye care gel and preparation method thereof |
| CN110279599A (en) * | 2019-07-10 | 2019-09-27 | 中山卡丝生物科技有限公司 | A kind of lightening compositions, suit containing lightening compositions and preparation method thereof |
| CN110279599B (en) * | 2019-07-10 | 2022-04-01 | 中山卡丝生物科技有限公司 | Whitening composition, set containing whitening composition and preparation method of set |
| CN111888307A (en) * | 2020-07-17 | 2020-11-06 | 重庆珂蓝健康管理集团有限公司 | Composition for repairing and healing face and application thereof |
| CN115487125A (en) * | 2022-01-28 | 2022-12-20 | 山西海博贝马生物科技有限公司 | Bactericidal composition and application thereof |
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