CN102302512B - Multi-vitamin mineral tablet - Google Patents
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Abstract
The invention relates to the field of medicine, and discloses a multi-vitamin mineral tablet. The multi-vitamin mineral tablet is composed of a vitamin layer, an isolation layer and a mineral layer, wherein the isolation layer is positioned between the vitamin layer and the mineral layer, and has the thickness of 1-2mm; and the vitamin layer contains vitamin C. According to the invention, vitaminand mineral elements are isolated effectively by utilizing the isolation layer between the vitamin layer and the mineral layer, vitamin C is protected effectively, the use amount and variety of the auxiliary materials are not required to be increased additionally, and the production cost is lower.
Description
Technical field
The present invention relates to field of medicaments, relate in particular a kind of multi-vitamin mineral tablet.
Background technology
Vitamin and mineral element are to keep human normal physiological activity and the necessary nutrient of growth promoter, have the effect of the vision safeguarded, enhancing development such as vitamin A; Vitamin C has the effects such as treatment vitamin C deficiency, antioxidation, anti-cancer; Calcium constituent is the indispensable element of keeping the skeleton growth; Ferrum element has the prevention anemia, promotes the effect of Plumbum removing.The national nutrition survey of announcing according to Chinese Soclety of Nutrition shows China urban and rural residents famine vitamin A, vitamin B
2And calcium, B generally is deficient in vitamin
1, vitamin B
6With vitamin C etc., wherein, the middle-aged and elderly people C that is deficient in vitamin is more serious.In addition, the child is general zinc deficiency also, the general iron deficiency of women.
For replenish these nutrients comprehensively, usually multivitamin and several mineral materials are added simultaneously as raw material, be made into the product that contains multivitamin and mineral, be called for short the multi-vitamin mineral product, such as multi-vitamin mineral tablet, multi-vitamin mineral granule etc.The advantage of this series products is by once taking, just can reaching the effect that replenishes simultaneously multivitamin and mineral, and is convenient convenient, is subject to liking of more and more consumers.
At present, the process of making multi-vitamin mineral tablet or multi-vitamin mineral granule is that multivitamin and multi mineral raw material and molding adjuvant etc. are mixed together, granulate, and makes after drying the multi-vitamin mineral granule, or carries out tabletting again and do slabbing.In addition, also have the stock and adjuncts such as multivitamin and several mineral materials are mixed with soybean oil, add suspending agent and make the multi-vitamin mineral soft capsule.
But there is certain deficiency in the product that adopts above-mentioned process to make, because chemical property reason own, some vitamin contacts with mineral and can react, thereby makes the content of vitamin, and then causes product efficacy to reduce.Wherein, loss is vitamin C the most significantly, because vitamin C has very strong reproducibility, and very easy reacting with mineral element ions such as ferrum, copper, selenium and oxidized, thus reduce ascorbic content.
In order to make vitamin C can reach effect institute expense, the means that adopt at present have three kinds: (1) is by adding excessive vitamin C etc. to offset ascorbic loss; (2) first vitamin C is carried out embedding, again with granulate after other raw materials mix, make product; (3) adopt ascorbic derivant (such as sodium L-ascorbate-2-phosphate, sodium ascorbate, calcium ascorbate, vitamin C potassium and Magnesium L-Asacorbic Acid 2-O-Phosphate etc.) to replace vitamin C to use.
But, these three kinds of methods also exist certain technical disadvantages, at first be to add excessive vitamin C, although can increase Vitamin C content in the product, but ascorbic content is still wayward in the product, the vitamin C loss is still very large, also can greatly increase production cost by adding excessive vitamin C in addition;
Next is that vitamin C is carried out embedding, can isolate contacting of vitamin C and mineral element on this theoretical method.But vitamin C is carried out embedding, mix in the process of making product with other raw materials after granulating, the extruding of tablet machine during owing to compression molding can be squeezed the vitamin C granules compacting of embedding broken, still vitamin C can be exposed under the mineral environment, cause largely loss;
To adopt ascorbic derivant at last, although it is slightly stable that more ascorbic derivants are compared vitamin, but sodium L-ascorbate-2-phosphate wherein, sodium ascorbate, calcium ascorbate, vitamin C potassium still has good reproducibility, can react with mineral elements such as ferrum equally, and reduction content, although Magnesium L-Asacorbic Acid 2-O-Phosphate character very stable not can with the reaction of the mineral element such as ferrum, but in vivo must be by the effect of phosphate, the vitamin C enzymolysis is dissociated, the ascorbic physiological function of competence exertion, this has limited human body and has absorbed ascorbic.In addition, ascorbic content is relatively low in the ascorbic derivant, and expensive, easily increases production cost.
Summary of the invention
In view of this this multi-vitamin mineral tablet, the object of the present invention is to provide a kind of multi-vitamin mineral tablet, so that can reduce ascorbic loss.
For achieving the above object, the invention provides following technical scheme:
A kind of multi-vitamin mineral tablet is made of vitamin layer, isolation layer and mineral layer, and described isolation layer is between vitamin layer and mineral layer, and thickness is 1-2mm, and described vitamin layer comprises vitamin C.
Multivitamin and the several mineral materials of the present invention by will comprising vitamin C carried out special tabletting after granulating respectively; the centre separates with isolation layer; make the three-layer tablet form; in the multi-vitamin mineral three-layer tablet of making; have an isolation layer between multivitamin layer and the multi mineral prime element layer, rather than directly contact, vitamin C can not contact fully with mineral element like this; can not produce because reacting loss, protect ascorbic effect thereby play.
Thinner for fear of isolation layer, in the tabletting process so that contact surface appears in vitamin layer and mineral layer, then the situation that the vitamin C loss occurs, isolation layer thickness of the present invention is 1-2mm, be preferably 1.5mm, be made of in maltodextrin, white sugar, mannitol, starch and the microcrystalline Cellulose one or more, these several materials are the medicine typical additives, concrete ratio does not limit, and can determine according to the art technology experience.
Vitamin layer of the present invention and mineral layer select human body required and easy shortage commonly used nutrient and additive be raw material, wherein, in weight portion, described vitamin layer is by 0.2-2 weight portion vitamin A, 0.3-3 weight portion vitamin B
1, 0.3-3 weight portion vitamin B
2, 0.25-2.5 weight portion vitamin B
6, 0.6-6 weight portion vitamin B
12, 0.1-1 weight portion folic acid, 50-200 weight portion vitamin C, 0.002-0.02 weight portion vitamin D, 2-20 weight portion vitamin E, 100-400 weight portion starch, 100-400 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate consist of; In weight portion, described mineral layer is made of 50-200 weight portion calcium, 2-20 weight portion ferrum, 2-20 weight portion zinc, 0.008-0.08 weight portion selenium, 140-560 weight portion starch, 80-320 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate.
The present invention also provides a kind of preparation method of multi-vitamin mineral tablet, to include respectively ascorbic vitamin layer raw material and mineral layer raw material after mixing, soft material processed, granulation, drying, granulate, total mixing, obtain vitamin layer granule and mineral layer granule, then carry out three laminate with the isolation layer raw material and get final product, described isolation layer is between vitamin layer and mineral layer, and thickness is 1-2mm.
Wherein, described isolation layer thickness is preferably 1.5mm, is made of in maltodextrin, white sugar, mannitol, starch and the microcrystalline Cellulose one or more.
Vitamin layer raw material of the present invention and mineral layer raw material comprise multivitamin, mineral and typical additives.Wherein, described vitamin layer raw material is in weight portion, by 0.2-2 weight portion vitamin A, 0.3-3 weight portion vitamin B
1, 0.3-3 weight portion vitamin B
2, 0.25-2.5 weight portion vitamin B
6, 0.6-6 weight portion vitamin B
12, 0.1-1 weight portion folic acid, 50-200 weight portion vitamin C, 0.002-0.02 weight portion vitamin D, 2-20 weight portion vitamin E, 100-400 weight portion starch, 100-400 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate consist of.
Described mineral layer raw material is made of 50-200 weight portion calcium, 2-20 weight portion ferrum, 2-20 weight portion zinc, 0.008-0.08 weight portion selenium, 140-560 weight portion starch, 80-320 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate in weight portion.
The present invention adds the minerals and vitamins raw material of same amount, adopt respectively the direct mixing granulation tablet forming technique of vitamin and mineral, tablet forming technique after vitamin and mineral are separately granulated and always mixed, and employing embedding VC granule, the multi-vitamin mineral product of VC derivant (VC calcium and VC cetylate) technique preparation, compare with multi-vitamin mineral tablet of the present invention, the result is presented at and places same time in the equivalent environment, the ascorbic loss amount of multi-vitamin mineral tablet of the present invention is below 3.5%, and the vitamin C loss amount loss of the multi-vitamin mineral product of other technique preparations is more serious, is several times or tens times of multi-vitamin mineral tablet of the present invention.
By above technical scheme as can be known; multi-vitamin mineral tablet of the present invention utilizes the isolation layer between mineral layer and the vitamin layer, has effectively isolated vitamin and mineral element, has protected vitamin C; and used supplementary material consumption and kind do not need extra increase, and production cost is lower.
The specific embodiment
The invention discloses a kind of multi-vitamin mineral tablet, those skilled in the art can use for reference this paper content, suitably improve technological parameter and realize.Special needs to be pointed out is, all similarly replace and change apparent to those skilled in the art, and they all are deemed to be included in the present invention.Multi-vitamin mineral tablet of the present invention is described by preferred embodiment, the related personnel obviously can change or suitably change and combination methods and applications as herein described within not breaking away from content of the present invention, spirit and scope, realizes and use the technology of the present invention.
Below in conjunction with embodiment, further set forth the present invention.
Embodiment 1:
1, the vitamin layer is granulated
0.3 weight portion vitamin B of 80 mesh sieves will be crossed
1, 0.3 weight portion vitamin B
2, 0.25 weight portion vitamin B
6, 0.6 weight portion vitamin B
12, 0.1 weight portion folic acid, 50 weight portion vitamin C powder mix homogeneously, with 100 weight portion white sugars, 100 weight portion starch and the 50 weight portion maltodextrin mixings of crossing 80 eye mesh screens, obtain vitamin layer material again;
Add 20% alcoholic solution in vitamin layer material, the limit edged stirs, and makes soft material; Then soft material is granulated through 16 eye mesh screens, make wet granular and dry, dried granule is crossed 16 eye mesh screens carry out granulate, then mix with 0.2 weight portion vitamin A, 0.002 weight portion vitamin D and 2 weight portion vitamin E particle powders and 1.3 weight portion magnesium stearate, obtain always mixed granule of vitamin layer, for subsequent use.
2, the mineral layer is granulated
To cross 50 weight portion calcium, 2 weight portion ferrum, 2 weight portion zinc, the 0.008 weight portion selenium mix homogeneously of 80 mesh sieves, with 80 weight portion white sugars, 140 weight portion starch and the 50 weight portion maltodextrin mixings of crossing 80 eye mesh screens, obtain mineral layer material again;
Add 20% alcoholic solution in mineral layer material, the limit edged stirs, and makes soft material; Then soft material is granulated through 16 eye mesh screens, make wet granular and dry, dried granule is crossed 16 eye mesh screens carry out granulate, then mix with 1.3 weight portion magnesium stearate, obtain always mixed granule of mineral layer, for subsequent use.
3, tabletting
With vitamin layer granule and mineral layer granule, send into multilamellar tablet machine tabletting with the isolation layer raw material (100 weight portion white sugars and 50 weight portion maltodextrins) of crossing 80 mesh sieve mix homogeneously and get multi-vitamin mineral tablet, described isolation layer thickness is 1mm, is positioned in the middle of vitamin layer and the mineral layer.
Embodiment 2:
1, the vitamin layer is granulated
1.6 weight portion vitamin Bs of 90 mesh sieves will be crossed
1, 1.6 weight portion vitamin Bs
2, 1.4 weight portion vitamin Bs
6, 3.3 weight portion vitamin Bs
12, 0.6 weight portion folic acid, 125 weight portion vitamin C powder mix homogeneously, with 250 weight portion white sugars, 250 weight portion starch and the 125 weight portion maltodextrin mixings of crossing 90 eye mesh screens, obtain vitamin layer material again;
Add purified water in vitamin layer material, the limit edged stirs, and makes soft material; Then soft material is granulated through 20 eye mesh screens, make wet granular and dry, dried granule is crossed 20 eye mesh screens carry out granulate, then mix with 1.1 weight portion vitamin A, 0.011 weight portion vitamin D and 11 weight portion vitamin E particle powders and 3.9 weight portion magnesium stearate, obtain always mixed granule of vitamin layer, for subsequent use.
2, the mineral layer is granulated
To cross 125 weight portion calcium, 11 weight portion ferrum, 11 weight portion zinc, the 0.044 weight portion selenium mix homogeneously of 90 mesh sieves, with 350 weight portion white sugars, 200 weight portion starch and the 125 weight portion maltodextrin mixings of crossing 90 eye mesh screens, obtain mineral layer material again;
Add purified water in mineral layer material, the limit edged stirs, and makes soft material; Then soft material is granulated through 20 eye mesh screens, make wet granular and dry, dried granule is crossed 20 eye mesh screens carry out granulate, then mix with 3.9 weight portion magnesium stearate, obtain always mixed granule of mineral layer, for subsequent use.
3, tabletting
With vitamin layer granule and mineral layer granule, send into multilamellar tablet machine tabletting with the isolation layer raw material (100 weight portion starch and 50 weight portion mannitol) of crossing 90 mesh sieve mix homogeneously and get multi-vitamin mineral tablet, described isolation layer thickness is 1mm, is positioned in the middle of vitamin layer and the mineral layer.
Embodiment 3:
1, the vitamin layer is granulated
3 weight portion vitamin Bs of 100 mesh sieves will be crossed
1, 3 weight portion vitamin Bs
2, 2.5 weight portion vitamin Bs
6, 6 weight portion vitamin Bs
12, 1 weight portion folic acid, 200 weight portion vitamin C powder mix homogeneously, with 400 weight portion white sugars, 400 weight portion starch and the 200 weight portion maltodextrin mixings of crossing 100 eye mesh screens, obtain vitamin layer material again;
Add 40% alcoholic solution in vitamin layer material, the limit edged stirs, and makes soft material; Then soft material is granulated through 24 eye mesh screens, make wet granular and dry, dried granule is crossed 24 eye mesh screens carry out granulate, then mix with 2 weight portion vitamin A, 0.02 weight portion vitamin D and 20 weight portion vitamin E particle powders and 6.5 weight portion magnesium stearate, obtain always mixed granule of vitamin layer, for subsequent use.
2, the mineral layer is granulated
200 weight portion calcium, 20 weight portion ferrum, 20 weight portion zinc, the 0.08 weight portion selenium mix homogeneously of 100 mesh sieves will be crossed, with 560 weight portion white sugars, 320 weight portion starch and the 200 weight portion maltodextrin mixings of crossing 100 eye mesh screens, obtain mineral layer material again;
Add 40% alcoholic solution in mineral layer material, the limit edged stirs, and makes soft material; Then soft material is granulated through 24 eye mesh screens, make wet granular and dry, dried granule is crossed 24 eye mesh screens carry out granulate, then mix with 6.5 weight portion magnesium stearate, obtain always mixed granule of mineral layer, for subsequent use.
3, tabletting
With vitamin layer granule and mineral layer granule, send into multilamellar tablet machine tabletting with the isolation layer raw material (100 weight portion white sugars and 50 weight portion maltodextrins) of crossing 100 mesh sieve mix homogeneously and get multi-vitamin mineral tablet, described isolation layer thickness is 1mm, is positioned in the middle of vitamin layer and the mineral layer.
Embodiment 4:
Add the minerals and vitamins raw material of same amount, adopt respectively the direct mixing granulation tablet forming technique of vitamin and mineral, vitamin and mineral separately to granulate and always mix rear tablet forming technique, and the multi-vitamin mineral product that adopts embedding VC granule, the preparation of VC derivant (VC calcium and VC cetylate) technique, compare with the multi-vitamin mineral tablet of embodiment 2 preparations, contrast test is accelerated test, the results are shown in Table 1.
Table 1 change of vitamin C comparing result
Annotate: the accelerated test temperature is 40 ± 2 ℃, relative humidity 70 ± 5%.
As shown in Table 1, multi-vitamin mineral tablet of the present invention can effectively reduce ascorbic loss, and the increase along with natural law, this advantage is all the more obvious, and the product of other process preparations, ascorbic loss amount is very remarkable, is several times or tens times of multi-vitamin mineral tablet of the present invention.
The above only is preferred implementation of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (8)
1. multi-vitamin mineral tablet, it is characterized in that, consisted of by vitamin layer, isolation layer and mineral layer, described isolation layer is between vitamin layer and mineral layer, thickness is 1-2mm, described vitamin layer comprises vitamin C, and described isolation layer consists of by two kinds in maltodextrin, white sugar, mannitol, starch and the microcrystalline Cellulose.
2. described multi-vitamin mineral tablet according to claim 1 is characterized in that, described isolation layer thickness is 1.5mm.
3. described multi-vitamin mineral tablet according to claim 1 is characterized in that, in weight portion, described vitamin layer is by 0.2-2 weight portion vitamin A, 0.3-3 weight portion vitamin B
1, 0.3-3 weight portion vitamin B
2, 0.25-2.5 weight portion vitamin B
6, 0.6-6 weight portion vitamin B
12, 0.1-1 weight portion folic acid, 50-200 weight portion vitamin C, 0.002-0.02 weight portion vitamin D, 2-20 weight portion vitamin E, 100-400 weight portion starch, 100-400 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate consist of.
4. described multi-vitamin mineral tablet according to claim 1, it is characterized in that, in weight portion, described mineral layer is made of 50-200 weight portion calcium, 2-20 weight portion ferrum, 2-20 weight portion zinc, 0.008-0.08 weight portion selenium, 140-560 weight portion starch, 80-320 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate.
5. the preparation method of a multi-vitamin mineral tablet, it is characterized in that, to include respectively ascorbic vitamin layer raw material and mineral layer raw material after mixing, soft material processed, granulation, drying, granulate, total mixing, obtain vitamin layer granule and mineral layer granule, then carry out three laminate with the isolation layer raw material and get final product, described isolation layer is between vitamin layer and mineral layer, thickness is 1-2mm, and described isolation layer consists of by two kinds in maltodextrin, white sugar, mannitol, starch and the microcrystalline Cellulose.
6. described preparation method according to claim 5 is characterized in that, described isolation layer thickness is 1.5mm.
7. described preparation method according to claim 5 is characterized in that, in weight portion, described vitamin layer raw material is by 0.2-2 weight portion vitamin A, 0.3-3 weight portion vitamin B
1, 0.3-3 weight portion vitamin B
2, 0.25-2.5 weight portion vitamin B
6, 0.6-6 weight portion vitamin B
12, 0.1-1 weight portion folic acid, 50-200 weight portion vitamin C, 0.002-0.02 weight portion vitamin D, 2-20 weight portion vitamin E, 100-400 weight portion starch, 100-400 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate consist of.
8. described preparation method according to claim 5, it is characterized in that, in weight portion, described mineral layer raw material is made of 50-200 weight portion calcium, 2-20 weight portion ferrum, 2-20 weight portion zinc, 0.008-0.08 weight portion selenium, 140-560 weight portion starch, 80-320 weight portion white sugar, 50-200 weight portion maltodextrin and 1.3-6.5 weight portion magnesium stearate.
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| CN103349278A (en) * | 2013-06-14 | 2013-10-16 | 芜湖市诺康生物科技有限公司 | Vitamin mineral tablets |
| CN110403945B (en) * | 2018-04-28 | 2022-11-18 | 上海泽生科技开发股份有限公司 | Composite vitamin composition for promoting gastrointestinal system power and preparation method thereof |
| CN115581699A (en) | 2018-04-28 | 2023-01-10 | 上海泽生科技开发股份有限公司 | Composite vitamin composition for promoting gastrointestinal system power and preparation method thereof |
| CN110327303A (en) * | 2019-08-15 | 2019-10-15 | 威海百合生物技术股份有限公司 | A kind of iron vitamin C tablet and preparation method thereof |
| CN113180245A (en) * | 2021-06-07 | 2021-07-30 | 湖北人缘堂医药生物工程有限公司 | Production method of multi-vitamin mineral tablets |
| CN116548620A (en) * | 2023-04-23 | 2023-08-08 | 山东新硒望生态农业科技有限公司 | Novel K2 selenium multidimensional tablet and preparation method thereof |
| CN117582411A (en) * | 2023-11-21 | 2024-02-23 | 汤臣倍健股份有限公司 | Vitamin and mineral double-layer tablet and preparation method thereof |
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| KR100267576B1 (en) * | 1998-07-25 | 2000-11-01 | 허계성 | Chewable soft tablet comprising separated active ingredients and process for preparing the same |
| CN1864699A (en) * | 2005-05-20 | 2006-11-22 | 合肥安华药物研究有限责任公司 | Novel dosage form of multiple Vitamins |
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Patent Citations (3)
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| CN101138570A (en) * | 2006-09-08 | 2008-03-12 | 成都市金医生科技健康产业有限公司 | Multiple vitamin and mineral composition chewing tablet |
| CN101549151A (en) * | 2009-02-13 | 2009-10-07 | 新疆埃乐欣药业有限公司 | Alliin/alliinase dualistic drug-releasing multilayer tablet |
| CN101897442A (en) * | 2010-07-03 | 2010-12-01 | 王凯莹 | Vitamin and mineral matter nutrient supplement for adult men |
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